Preparation method of enveloping acidulant for feeds
A technology for coating acidulants and feeds, which is applied in the field of preparation of coating acidulants for feeds, can solve the problems of reducing the application efficiency of acidulants, premature oxidation of coatings, and elevated fat levels, and achieves delaying lipid peroxidation. reaction, excellent antibacterial properties, effect of preventing proliferation
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example 1
[0021] According to the mass ratio of 1:5, mix the natural zeolite with the mass fraction of 5% ammonium chloride solution, heat it in a water bath at 75°C for 6h, filter and collect the filter cake, wash it with deionized water for 3 times, and then heat it at 550°C. Calcined in a furnace for 100 minutes, after the calcination was completed, let it stand and cool to room temperature, collected the calcined particles and mixed the calcined particles with 5% hydrochloric acid in a mass ratio of 1:8, stirred and mixed for 6 hours, filtered to obtain a filter cake, and used Rinse with deionized water until the pH of the washing solution reaches 7.0, and dry in vacuum to obtain modified zeolite particles; mix β-cyclodextrin with deionized water at a mass ratio of 1:5, heat and stir in a water bath at 45°C to obtain a mixed solution, adjust the pH to 8.5 with a mass fraction of 3% sodium hydroxide solution to obtain an alkalized solution, and then add 2,3-epoxypropyltrimethylammoniu...
example 2
[0023] According to the mass ratio of 1:5, mix natural zeolite with 5% ammonium chloride solution by mass fraction, heat in a water bath at 77°C for 7 hours, filter and collect the filter cake, wash it with deionized water for 4 times, and then heat it at 600°C Calcined in a furnace for 110 minutes, after the calcination was completed, let it stand and cool to room temperature, collected the calcined particles and mixed the calcined particles with 5% hydrochloric acid in a mass ratio of 1:8, stirred and mixed for 7 hours, filtered to obtain a filter cake, and used Rinse with deionized water until the pH of the washing solution reaches 7.0, and dry in vacuum to obtain modified zeolite particles; mix β-cyclodextrin with deionized water at a mass ratio of 1:5, heat and stir in a water bath at 47°C to obtain a mixed solution, adjust the pH to 8.5 with a mass fraction of 3% sodium hydroxide solution to obtain an alkalized solution, and then add 2,3-epoxypropyltrimethylammonium chlor...
example 3
[0025]According to the mass ratio of 1:5, mix the natural zeolite with the mass fraction of 5% ammonium chloride solution, heat it in a water bath at 85°C for 8h, filter and collect the filter cake, wash it with deionized water for 5 times, and then heat it at 650°C. Calcined in a furnace for 120 minutes. After the calcination was completed, let it stand and cool to room temperature. Collect the calcined particles and mix the calcined particles with 5% hydrochloric acid in a mass ratio of 1:8. After stirring and mixing for 8 hours, filter to obtain a filter cake. Rinse with deionized water until the pH of the washing solution reaches 7.0, and dry in vacuum to obtain modified zeolite particles; mix β-cyclodextrin with deionized water at a mass ratio of 1:5, heat and stir in a water bath at 50°C to obtain a mixed solution, adjust the pH to 8.5 with a mass fraction of 3% sodium hydroxide solution to obtain an alkalized solution, and then add 2,3-epoxypropyltrimethylammonium chlori...
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