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Preparation method of metal-based shape memory composite

A composite material and metal-based technology, applied in metal rolling and other directions, can solve the problems of high equipment requirements, plate thickness particle loss, uneven dispersion, etc., and achieve simple preparation process, improved damping performance, and small particle loss. Effect

Active Publication Date: 2017-12-29
XI'AN UNIVERSITY OF ARCHITECTURE AND TECHNOLOGY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

But there are big problems. On the one hand, under high temperature conditions, the shape memory effect is destroyed, and intermetallic compounds with brittle phases are easily formed at the interface, which reduces the bonding effect of the material; on the other hand, it is easy to make the shape memory alloy Particles are agglomerated and cannot be uniformly dispersed in the matrix, and the test period is long, requiring high equipment
Ma Zongyi and others tried to make aluminum matrix composites by drilling and slotting in the center of the plate, adding shape memory particles, and preparing aluminum matrix composites through friction stir processing, but the thickness of the available plate was thin and the particles were lost to a certain extent, which limited the use

Method used

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  • Preparation method of metal-based shape memory composite
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  • Preparation method of metal-based shape memory composite

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preparation example Construction

[0031] A method for preparing a metal matrix shape memory composite material, comprising the steps of:

[0032] (1) First, put the NiTi metal powder in a beaker and vibrate in the ultrasonic vibrator for about 40 minutes. The purpose of using the ultrasonic vibrator to vibrate is to eliminate possible errors caused by the agglomeration of the NiTi metal powder and ensure the uniform dispersion of the NiTi metal powder.

[0033] (2) Place the uniformly dispersed NiTi metal powder between two prefabricated metal plates (such as magnesium plates), add the NiTi metal powder in a tiled manner for rolling, and finish rolling in the first pass. Cut the rolled plate, continue to add NiTi metal powder to the two sheared plates, and then roll, repeating this step.

[0034] Among them, the thickness ratio of the metal plate is 1:1, and the same metal can be used for rolling, and different metals can also be selected for rolling. In addition to the above magnesium plates, the metal plate...

Embodiment 1

[0046] Large particle, integral NiTi particle reinforced same-material lamination welding manufacturing process: clean the overlapping surface of two AZ31 plates with a size of 80mm×80mm×2mm with ethanol and a steel brush, and add a diameter of 106 in the middle of the tile. ~150um NiTi particles, the number of particles added is about 1.36×10 3 ~1.91×10 3 piece / cm 2 , and fastened with rivets. Then heated at 350°C for 400s and taken out. Rolling is carried out on a Φ170×300 two-roll mill, the reduction rate is 50%, and the rolling speed is 0.4m / s. Cut from the middle after rolling. Repeat the above steps, take out after rolling for 5 passes, the final thickness of AZ31 plate is 4mm. Single-pass FSP processing was carried out under the condition of rotating speed of 750r / min and traveling speed of 118mm / min. The NiTi particles of the obtained composite material are basically lossless and very uniformly distributed, and are well combined with the matrix. No adverse inter...

Embodiment 2

[0048] Small particle, overall NiTi particle reinforced same-material lamination welding manufacturing process: clean the overlapped surface of two AZ31 plates with a size of 80mm×80mm×2mm with ethanol and a steel brush, and add a diameter of 2 -50um NiTi particles, the number of particles added is about 0.41×10 4 ~1.02×10 5 piece / cm 2 , and fastened with rivets. Then heated at 350°C for 400s and taken out. Rolling is carried out on a Φ170×300 two-roll mill with a reduction rate of 45% and a rolling speed of 0.4m / s. Cut from the middle after rolling. Repeat the above steps, take out after rolling for 6 passes, the final thickness of AZ31 plate is 2.1mm. Single-pass FSP processing was carried out under the condition of rotating speed of 750r / min and traveling speed of 118mm / min. The NiTi particles of the obtained composite material are basically lossless and very uniformly distributed, and are well combined with the matrix. No adverse interface reactions occurred.

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Abstract

The invention discloses a preparation method of a metal-based shape memory composite. The preparation method comprises the steps that NiTi metal powder layers are laid between to-be-prepared adjacent metal plates to obtain laminated plates, the laminated plates are subjected to accumulative ply rolling treatment to obtain a composite plate, it is guaranteed that the corresponding NiTi metal powder layer is laid between any two adjacent metal plates in the accumulative ply rolling treatment process, and the composite plate is subjected to friction stirring processing treatment to obtain the metal-based shape memory composite. The reduction rate of each pass of accumulative ply rolling ranges from 40% to 55%, and the number of the rolling passes of accumulative ply rolling ranges from 2 to 8; and the rotating speed of friction stirring processing ranges from 375 r / min to 1,180 r / min, the advancing speed of friction stirring processing ranges from 75 mm / min to 235 mm / min, and the reduction rate of friction stirring processing ranges from 0.2 mm to 0.5 mm. Through the adoption of the laminating welding deformation method, the metal plates on different layers are changed, SMAs different in particle size and content are evenly and flatly laid between the plates, metal materials with different structures and properties can be prepared out, and the novel functional material in different service environments is met.

Description

technical field [0001] The invention belongs to the field of material preparation, and in particular relates to a preparation method of a metal matrix shape memory composite material. Background technique [0002] With the development of science and technology, there is an increasing demand for materials with special properties in many fields such as aerospace, electronics and automobile industries. Therefore, as a functional material, smart materials have great application prospects, and shape memory alloys (SMAs) are the most important components of smart composite materials due to their shape memory effect, high damping performance and pseudoelasticity. At present, the research on SMAs composite materials is very active, and NiTi shape memory alloy, as a typical representative of SMAs, not only has excellent shape memory effect and superelasticity, but also has good biocompatibility, and can be used to make vascular stents, lumens, etc. Medical devices such as endotrache...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B22F3/18B22F7/02B22F1/00B21B1/38
CPCB21B1/38B21B2001/386B22F1/0003B22F3/18B22F7/02B22F2007/042
Inventor 王快社席小鹏王文乔柯张兵张婷张志娟
Owner XI'AN UNIVERSITY OF ARCHITECTURE AND TECHNOLOGY
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