Modified treatment process of kudzuvine root powder
A kudzu root and modification technology, which is applied in the processing technology field of kudzu root powder, can solve the problems of poor storage and absorption effect, and achieve the effects of simple and controllable production method, improved taste, and less dosage
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Embodiment 1
[0023] The modification process of Pueraria lobata powder includes the following steps:
[0024] (1) Cut the pueraria root into pieces, put the lumpy pueraria root in a 90% ethanol solution by mass concentration for 1.5 hours, filter and dry, and grind the pueraria root into powder particles with a particle size of 0.08-0.12mm;
[0025] (2) Weigh the dried powder particles into the reaction vessel, keep the temperature in the reaction vessel between 35-37℃, add 45% sodium hydroxide aqueous solution and 90% ethanol solution with mass concentration to the reaction at the same time In the container, stir for 10 minutes and then filter; the weight ratio between the sodium hydroxide aqueous solution and the ethanol solution is 1:1.5;
[0026] (3) The solid material obtained by filtration is repeatedly washed with ethanol solution with a mass concentration of 90%, and the temperature in the reaction vessel is increased to between 50-55°C, and then 0.5 times the weight of the powdered parti...
Embodiment 2
[0029] The difference between this embodiment and embodiment 1 is only that the process parameters of each step are different, and the specific settings are as follows:
[0030] In step (1), the size of the powdery particles is 0.12-0.2mm; after the water cooking time is 30min, the ethanol solution concentration is 95%, and the soaking time is 2h;
[0031] In step (2), the concentration of the ethanol solution is 95%, the concentration of the sodium hydroxide aqueous solution is 50%, the stirring time is 15 minutes, and the weight ratio between the sodium hydroxide aqueous solution and the ethanol solution is 1:1;
[0032] Step (3) The haloalkane RX is 0.3 times the weight of the powdered particles, the X is Cl, and the R is hydroxyethyl.
Embodiment 3
[0034] The difference between this embodiment and embodiment 1 is only that the process parameters of each step are different, and the specific settings are as follows:
[0035] In step (1), the size of the powdery particles is 0.01-0.08mm; the water cooking time is 10min, the ethanol solution concentration is 90%, and the soaking time is 1h;
[0036] In step (2), the concentration of the sodium hydroxide aqueous solution is 40%, the ethanol solution concentration is 85%, the stirring time is 5 min, and the weight ratio between the sodium hydroxide aqueous solution and the ethanol solution is 1:1.8;
[0037] Step (3) The haloalkane RX is 0.6 times the weight of the powdered particles, the X is Cl, and the R is methyl.
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