The invention provides an efficient method for pretreating, degrading and recycling thermosetting
epoxy resin based on a mixed
reaction type solvothermal method. The efficient method comprises the following steps: S1, providing cured
epoxy resin; s2, adding the cured
epoxy resin into double solvents for pre-soaking so as to provide a pre-treated sample; the double
solvent is selected from halogenated
alkane and
aliphatic amine; and S3, carrying out
reflux on the pretreated sample in a low-temperature interval, cooling to
room temperature, carrying out first suction
filtration to obtain a first filtrate, mixing the first filtrate with water to separate out a precipitate or form a dispersion liquid, carrying out second suction
filtration on the precipitate, further separating the dispersion liquid, and recovering to obtain the epoxy resin degradation micromolecules or oligomers. According to the present invention, the halogenated
alkane-
aliphatic amine mixed
reaction type double solvents with different proportions are subjected to pre-soaking and low-temperature interval
reflux, and the obtained mixture and the original
solvent molecule have the synergistic effect, such that the thermosetting epoxy resin can be efficiently degraded, the
environmental protection is achieved, and the cost is low.