Method and device for preparing uniform-particle-diameter metal powder through quantitative centrifugal atomization method

A centrifugal atomization and metal powder technology, applied in the field of metal spherical powder preparation, can solve the problems of high manufacturing schedule requirements, difficult processing, affecting the performance of spherical metal powder, etc., and achieve the effect of high powder preparation efficiency

Inactive Publication Date: 2018-01-12
张家港创博金属科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Among them, the remelting method is to make metal raw materials into filaments and cut them into uniform small pieces, and then immerse them in hot oil at an appropriate temperature to melt and solidify them into spherical particles. This method is simple in principle, but requires high manufacturing progress, and for small Materials with poor particle size or plasticity are difficult to process, and the production efficiency is low; the uniform droplet injection method is to melt the metal raw material, and extrude the liquid metal from the bottom of the crucible with holes through vibration extrusion to form a liquid pellet, thereby solidifying into Spherical metal powder, the spherical powder prepared by this method has uniform size and good quality, but the preparation process must adopt the method of vibration extrusion, which will have a certain impact on the stability of the liquid raw material in the crucible, especially as the liquid raw material decreases, its stability The performance will become worse and worse, and the preparation efficiency of this method is low, which is not suitable for industrial mass production; the atomization method is mainly divided into gas atomization

Method used

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  • Method and device for preparing uniform-particle-diameter metal powder through quantitative centrifugal atomization method
  • Method and device for preparing uniform-particle-diameter metal powder through quantitative centrifugal atomization method

Examples

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Embodiment 1

[0013] Embodiment 1: Prepare spherical powder of metal aluminum, the particle size of the powder is 100 μm, the diameter of the small hole of the crucible is 80 μm, and the rotation speed of the crucible is 3000 rpm, the specific steps are as follows:

[0014] Open the deflation valve (9), and after the deflation is completed, open the door (19), put the powder collector (20) directly under the crucible, close the door (19), open the door (1), and place the powder in the crucible Put metal aluminum into the crucible, the amount of metal aluminum put in does not exceed 2 / 3 of the volume of the crucible, cover the crucible cover (3) and fix it, close the door (1), close the air release valve (9), turn on the mechanical pump (10 ) to pump the pressure in the chamber to 1Pa, then use the diffusion pump (11) to further pump the pressure in the chamber to 0.01Pa, fill the chamber with high-purity inert gas through the intake pipe (2), so that the pressure inside and outside the chamb...

Embodiment 2

[0015] Example 2: Preparation of spherical powder of superalloy Inconel 718, the particle size of the powder is 50 μm, the diameter of the small hole of the crucible is 60 μm, and the rotation speed of the crucible is 1800 rpm. The specific steps are:

[0016] Open the deflation valve (9), and after the deflation is completed, open the door (19), put the powder collector (20) directly under the crucible, close the door (19), open the door (1), and place the powder in the crucible Put superalloy Inconel 718 into the crucible, the volume of which should not exceed 2 / 3 of the volume of the crucible, cover the crucible lid (3) and fix it, close the door (1), close the vent valve (9), and turn on the mechanical pump (10) Pump the pressure in the chamber to 1Pa, then use the diffusion pump (11) to further pump the pressure in the chamber to 0.01Pa, fill the chamber with high-purity inert gas through the intake pipe (2), so that the pressure inside and outside the chamber is balanced,...

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Abstract

The invention discloses a method and a device for preparing uniform-particle-diameter metal powder through a quantitative centrifugal atomization method. According to the method, a perforated crucibleis driven by a motor to rotate, and then a molten metal liquid in the crucible is jetted from tiny holes in the crucible under the action of centrifugal force; after being jetted from the tiny holes,the metal liquid is atomized into metal liquid drops under the action of centrifugal force; under the action of gravity and surface tension, spherical metal liquid drops are formed; and during the falling process, uniform-particle-diameter metal spheres are formed. The method is matched with different crucible tiny-hole diameters and crucible rotation speeds, so that metal powder of different types can be prepared; the particle diameters are controllable; and the metal powder prepared according to the method has the characteristics being controllable in particle diameter, high in sphericity and uniform in particle size.

Description

technical field [0001] The invention belongs to the technical field of metal spherical powder preparation, in particular to a method and device for preparing metal powder with uniform particle size by quantitative centrifugal atomization method. Background technique [0002] With the development of material science, the position of spherical metal powder in material processing has been increasing day by day. At present, spherical metal powders have been widely used in solar cells, semiconductor integrated circuits, electronic packaging, precision manufacturing, chemical catalysis, biomaterials and other fields. The size, sphericity and particle size uniformity of spherical powders have become the key factors affecting product quality. [0003] At present, the methods for preparing spherical metal powder at home and abroad mainly include remelting method, uniform droplet spraying method and atomization method. Among them, the remelting method is to make metal raw materials ...

Claims

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Application Information

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IPC IPC(8): B22F9/10
Inventor 李小宝朱俊
Owner 张家港创博金属科技有限公司
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