Composite non-woven fabric suitable for oil-water separation and preparation method thereof

A technology of oil-water separation and non-woven fabrics, which is applied in the field of material chemistry, can solve the problems of lack of in-depth research on the dynamic oil-water separation performance of non-woven fabrics, and achieve the effects of low resistance, high oil phase breakdown pressure, and high retention rate

Inactive Publication Date: 2018-01-26
苏州市苏真床垫有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, there is a lack of in-depth research on the dyna

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] A composite non-woven fabric suitable for oil-water separation, said non-woven fabric comprising: 28 parts of polypropylene non-woven fabric, 12 parts of acetone, 10 parts of acrylic acid, 12 parts of benzophenone, 13 parts of dichloroethane, chlorine Calcium 8 parts, sodium carbonate 8 parts, calcium carbonate 19 parts, n-hexadecane 15 parts, sodium periodate 17 parts, ethylenediamine 7 parts, dimethyl sulfoxide 23 parts.

[0024] A preparation method for a composite non-woven fabric suitable for oil-water separation, comprising the following steps:

[0025] (1) Cut the polypropylene non-woven fabric into a 10cm×10cm sample, wash it with absolute ethanol, dry it at 25°C, roll it into a cylinder around the glass rod, and tie it up;

[0026] (2) Under the condition of 15°C, dissolve benzophenone and acetone in n-hexadecane, add acrylic acid dropwise thereto, mix well and store in a sealed container at 4°C;

[0027] (3) Submerge the polypropylene non-woven fabric bundled...

Embodiment 2

[0032] A composite non-woven fabric suitable for oil-water separation, said non-woven fabric comprising: 42 parts of polypropylene non-woven fabric, 23 parts of acetone, 22 parts of acrylic acid, 21 parts of benzophenone, 18 parts of dichloroethane, chlorine Calcium 15 parts, sodium carbonate 14 parts, calcium carbonate 26 parts, n-hexadecane 24 parts, sodium periodate 24 parts, ethylenediamine 16 parts, dimethyl sulfoxide 32 parts.

[0033] A preparation method for a composite non-woven fabric suitable for oil-water separation, comprising the following steps:

[0034] (1) Cut the polypropylene non-woven fabric into a 10cm×10cm sample, wash it with absolute ethanol, dry it at 32°C, wrap it around a glass rod into a cylindrical shape, and tie it up;

[0035] (2) Under the condition of 22°C, dissolve benzophenone and acetone in n-hexadecane, add acrylic acid dropwise therein, mix well and store in a sealed container at 4°C;

[0036] (3) Submerge the polypropylene non-woven fabr...

Embodiment 3

[0041]A composite non-woven fabric suitable for oil-water separation, said non-woven fabric comprising: 50 parts of polypropylene non-woven fabric, 26 parts of acetone, 25 parts of acrylic acid, 25 parts of benzophenone, 19 parts of dichloroethane, chlorine Calcium 19 parts, sodium carbonate 19 parts, calcium carbonate 32 parts, n-hexadecane 28 parts, sodium periodate 27 parts, ethylenediamine 20 parts, dimethyl sulfoxide 39 parts.

[0042] A preparation method for a composite non-woven fabric suitable for oil-water separation, comprising the following steps:

[0043] (1) Cut the polypropylene non-woven fabric into a 10cm×10cm sample, wash it with absolute ethanol, dry it at 35°C, roll it into a cylinder around the glass rod, and tie it up;

[0044] (2) Under the condition of 25°C, dissolve benzophenone and acetone in n-hexadecane, add acrylic acid dropwise thereto, mix well and store in a sealed container at 4°C;

[0045] (3) Submerge the polypropylene non-woven fabric bundl...

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Abstract

The invention discloses a composite non-woven fabric suitable for oil-water separation and a preparation method thereof. The non-woven fabric comprises: 28-50 parts of polypropylene non-woven fabric,12-26 parts of acetone, 10-25 parts of acrylic acid, 12-25 parts of benzophenone, 13-19 parts of dichloroethane, 8-19 parts of calcium chloride, 8-19 parts of sodium carbonate, 19-32 parts of calciumcarbonate, 15-28 parts of n-hexadecane, 17-27 parts of sodium periodate, 7-20 parts of ethylenediamine, and 23-39 parts of dimethylsulfoxide. According to the method, a co-radiation method is employedfor grafting of acrylic acid to the polypropylene non-woven fabric and then mineralization is carried out, in a solid-water-oil three-phase system, a mineral layer on the non-woven fabric surface plays a role of rigid and stable moisture retention layer, and a mineralized membrane shows the underwater superoleophobic and oil drop adhesion layer effects. The composite non-woven fabric suitable foroil-water separation provided by the invention has the advantages of high oil phase disruptive pressure, small transmembrane resistance, and high retention rate of large-size emulsion droplets.

Description

technical field [0001] The invention belongs to the field of material chemistry and relates to a functional nonwoven fabric material, in particular to a composite nonwoven fabric suitable for oil-water separation and a preparation method thereof. Background technique [0002] With the rapid development of society and the steady advancement of industrialization, people use more and more oil products. While meeting the needs of human material production and life, it also brings great challenges to environmental protection worldwide. On the one hand, oil-intensive industries such as oil refining, textiles, and food industries produce a large amount of oily wastewater every year, which seriously threatens water quality safety; on the other hand, oil spills from drilling platforms or ocean-going cruise ships have occurred frequently in recent years. When a large amount of crude oil is leaked into the seawater, the clean oil components will form a thin film on the ocean surface, h...

Claims

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Application Information

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IPC IPC(8): D06M14/28D06M11/155D06M11/76D06M11/30D06M13/08D06M13/332D06M13/268B01D17/022C02F1/40D06M101/20
Inventor 张俊武姚仟锋
Owner 苏州市苏真床垫有限公司
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