Preparation method of microalgae biodiesel with high caloric heat

A technology of microalgae biology and high calorific value, which is applied in the fields of bioengineering and clean energy preparation, which can solve the problems of low oil production efficiency and low calorific value, so as to improve oil production efficiency, promote the accumulation of oil in algae cells, and improve oil production efficiency. quality effect

Inactive Publication Date: 2018-03-02
雷春生
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The main technical problem to be solved by the present invention is to provide a method for preparing high calorific value microalgae biodiesel,

Method used

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  • Preparation method of microalgae biodiesel with high caloric heat

Examples

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Effect test

example 1

[0026]Take 0.5kg of river bottom sludge and put it in a beaker, add 800mL of distilled water into the beaker, seal the mouth of the beaker with a ventilating plug, move it into a water bath, heat up to 90°C, cook for 2 hours, cool naturally to room temperature, and let it stand for 10 minutes. , filtered to remove the lower layer of sediment, to obtain a supernatant, sterilized distilled water was added to the supernatant to a total volume of 900mL, to obtain a soil extract; Inoculate the inoculation density of / mL into the soil extract solution, control the temperature of the culture solution at 26°C, and the intensity of visible light irradiation at 2000Lx, and cultivate for 4 days; add 70mL biogas slurry, 50g shell powder, and 20g Nile Red to the above-mentioned conical flask, And place a beaker filled with potassium permanganate solution with a mass fraction of 65% between the air pump and the Erlenmeyer flask, connect the air pump, beaker, and Erlenmeyer flask with a glass...

example 2

[0028] Take 0.6kg of river bottom sludge and put it in a beaker, add 900mL of distilled water into the beaker, seal the mouth of the beaker with a ventilating plug, move it into a water bath, heat up to 95°C, cook for 2.5h, cool naturally to room temperature, and let it stand for stratification After 13 minutes, remove the lower layer of sediment by filtration to obtain a supernatant, add sterilized distilled water to the supernatant to a total volume of 950mL, and obtain a soil extract; The inoculation density of cells / mL was inoculated into the soil extract solution, the temperature of the culture solution was controlled at 27°C, and the intensity of visible light irradiation was 2100Lx, and cultured for 4.5 days; 75mL of biogas slurry, 55g of shell powder, and 25g of Nile Red were added to the above-mentioned Erlenmeyer flask , and place a beaker filled with potassium permanganate solution with a mass fraction of 65% between the air pump and the Erlenmeyer flask. Air was in...

example 3

[0031] Take 0.7kg of river bottom sludge and put it in a beaker, add 1000mL of distilled water into the beaker, seal the mouth of the beaker with a ventilating plug, move it into a water bath, heat up to 100°C, cook for 3 hours, cool naturally to room temperature, and let it stand for 15 minutes. , filtered to remove the lower sediment, to obtain the supernatant, sterilized distilled water was added to the supernatant to a total volume of 1000mL, to obtain the soil extract; Inoculate the inoculation density of / mL into the soil extract solution, control the temperature of the culture solution at 28°C, and the intensity of visible light irradiation at 2200Lx, and cultivate for 5 days; add 80mL biogas slurry, 60g shell powder, and 30g Nile Red to the above-mentioned conical flask, And place a beaker filled with potassium permanganate solution with a mass fraction of 65% between the air pump and the Erlenmeyer flask, connect the air pump, beaker, and Erlenmeyer flask with a glass ...

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Abstract

The invention relates to the technical field of biological engineering and preparation of clean energy sources, in particular to a preparation method of microalgae biodiesel with high caloric heat. The preparation method comprises the following steps of using chlorella as a raw material to prepare chlorella grease; esterifying the chlorella grease, and centrifugally delaminating, so as to obtain alower biodiesel crude product; continuing to distill, so as to obtain the microalgae biodiesel with high caloric heat. The preparation method has the advantages that the microalgae is promoted to quickly grow under the conditions of relatively moderate light radiation and light quality, highly-concentrated soil extracting solution as culture liquid, proper temperature and the like, so that the diesel production efficiency is improved; the chlorella is single cell pyrenoid chlorella, the pyrenoid chlorella has stable suitability to the environment, the rich nitrogen and phosphor elements and the inorganic elements in biogas slurry can be absorbed, the function of promoting accumulation of chlorella cell grease is realized, the production efficiency of the biodiesel is improved, the maximumcontent of grease is obtained, the content of carbon in the grease is increased, and the purpose of improving the caloric heat of the biodiesel is realized.

Description

technical field [0001] The invention relates to the technical fields of bioengineering and clean energy preparation, in particular to a method for preparing high calorific value microalgae biodiesel. Background technique [0002] With the rapid development of the world economy, fossil fuels can no longer meet the needs of world economic development. Especially in recent years, the international oil price has soared sharply, which has an increasing impact on the economies of various countries. Biodiesel is an excellent renewable new energy. As a renewable energy project that is being actively promoted in the world, it will become the main energy source of human beings in the 21st century together with clean nuclear energy, wind energy, and photovoltaic power generation. [0003] The most common way to produce biodiesel is esterification, which is the process of adding a certain amount of methanol to vegetable oil, heating it to a certain temperature, and reacting with a cata...

Claims

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Application Information

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IPC IPC(8): C12P7/64C12R1/89
CPCC12P7/649Y02E50/10
Inventor 谷春芽何少雄张建初
Owner 雷春生
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