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Hot melt adhesive and production method thereof

An adhesive and hot-melt technology, applied in the directions of adhesives, adhesive additives, adhesive types, etc., can solve the problems of poor use effect and high production cost, and achieve simple production, low cost and good adhesion. Effect

Inactive Publication Date: 2018-03-16
GUILIN AONISITE ENERGY SAVING & ENVIRONMENT PROTECTION TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

There are many classification methods of adhesives, which can be divided into thermosetting type, hot melt type, room temperature curing type, pressure sensitive type, etc. according to the application method; according to the application object, it can be divided into structural type, non-configuration or special adhesive; the connection form can be divided into Water-soluble, water-emulsion, solvent-based, and various solid-state types; traditional adhesives are expensive to produce and use poorly

Method used

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  • Hot melt adhesive and production method thereof

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Experimental program
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Effect test

Embodiment 1

[0020] The hot-melt adhesive of this embodiment is composed of the following raw materials: 10 kg of dibutyl phthalate, 10 kg of triethanolamine, 4 kg of propylene oxide phenyl ether, 8 kg of benzisothiazolone, 2 kg of polyurethane resin, Propyl distarch phosphate 9kg, N-methylpyrrolidone 2kg, hydroxydicumyl peroxide 9kg, furfuryl alcohol resin 1kg, vitamin E oil 10kg and glyoxal 2kg.

[0021] The preparation method of above-mentioned hot-melt adhesive comprises the steps:

[0022] (1) Weigh the following raw materials: dibutyl phthalate 10kg, triethanolamine 10kg, propylene oxide phenyl ether 4kg, benzisothiazolone 8kg, polyurethane resin 2kg, hydroxypropyl distarch phosphate 9kg , N-methylpyrrolidone 2kg, hydroxydicumyl peroxide 9kg, furfuryl alcohol resin 1kg, add to the reaction kettle, gradually heat up, and stir slowly, start timing when the temperature rises to 95°C, keep warm for 10min, and carry out uniform stirring at the same time , until reaching the end of the re...

Embodiment 2

[0025] The hot-melt adhesive of this embodiment is made up of raw materials with the following weight: 15kg of dibutyl phthalate, 7kg of triethanolamine, 7kg of propylene oxide phenyl ether, 5kg of benzisothiazolone, 6kg of polyurethane resin, hydroxy Propyl distarch phosphate 7kg, N-methylpyrrolidone 6kg, hydroxydicumyl peroxide 6kg, furfuryl alcohol resin 3kg, vitamin E oil 7kg and glyoxal 4kg.

[0026] The preparation method of above-mentioned hot-melt adhesive comprises the steps:

[0027] (1) Weigh the following raw materials: dibutyl phthalate 15kg, triethanolamine 7kg, propylene oxide phenyl ether 7kg, benzisothiazolone 5kg, polyurethane resin 6kg, hydroxypropyl distarch phosphate 7kg , 6kg of N-methylpyrrolidone, 6kg of hydroxydicumyl peroxide, and 3kg of furfuryl alcohol resin were added to the reaction kettle, and the temperature was gradually raised, and stirred slowly. When the temperature rose to 95°C, the timing was started, and the temperature was kept for 20 mi...

Embodiment 3

[0030] The hot-melt adhesive of this embodiment is composed of the following raw materials: 20 kg of dibutyl phthalate, 5 kg of triethanolamine, 10 kg of propylene oxide phenyl ether, 2 kg of benzisothiazolone, 10 kg of polyurethane resin, Propyl distarch phosphate 5kg, N-methylpyrrolidone 10kg, hydroxydicumyl peroxide 3kg, furfuryl alcohol resin 5kg, antioxidant 4kg and crosslinking agent 6kg.

[0031] The preparation method of above-mentioned hot-melt adhesive comprises the steps:

[0032] (1) Weigh the following raw materials: dibutyl phthalate 20kg, triethanolamine 5kg, propylene oxide phenyl ether 10kg, benzisothiazolone 2kg, polyurethane resin 10kg, hydroxypropyl distarch phosphate 5kg , 10kg of N-methylpyrrolidone, 3kg of hydroxydicumyl peroxide, and 5kg of furfuryl alcohol resin were added to the reaction kettle, and the temperature was gradually raised, and stirred slowly. When the temperature rose to 95°C, the timing was started, and the temperature was kept for 30 m...

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Abstract

The invention discloses a hot melt adhesive and a production method thereof, and belongs to the technical field of chemical industry. The hot melt adhesive is prepared from, by weight, 10-20 parts ofdibutyl phthalate, 5-10 parts of triethanolamine, 4-10 parts of epoxy propane phenyl ether, 2-8 parts of benzisothiazolone, 2-10 parts of polyurethane resin, 5-9 parts of hydroxypropyl distarch phosphate, 2-10 parts of N-methylpyrrolidone, 3-9 parts of peroxide hydroxyl diisopropylbenzene, 1-5 parts of Furfuryl alcohol resin, 4-10 parts of antioxidants and 2-6 parts of cross-linking agents. The hot melt adhesive has excellent hot melt performances and cohesiveness, can be normally used at the high temperature and is simple to product, low in cost and excellent in performance.

Description

technical field [0001] The invention relates to a hot-melt adhesive and a preparation method thereof, belonging to the technical field of chemical industry. Background technique [0002] Adhesive refers to the technology of connecting the surfaces of homogeneous or heterogeneous objects with adhesive, which has the characteristics of continuous stress distribution, light weight and low process temperature. Gluing is especially suitable for the connection of different materials, different thicknesses, ultra-thin specifications and complex components. Glue is developing the fastest in modern times and has a wide range of application industries. There are many classification methods of adhesives, which can be divided into thermosetting type, hot melt type, room temperature curing type, pressure sensitive type, etc. according to the application method; according to the application object, it can be divided into structural type, non-configuration or special adhesive; the connect...

Claims

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Application Information

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IPC IPC(8): C09J103/04C09J103/06C09J103/08C09J175/04C09J171/14C09J11/06
CPCC09J103/04C08L2205/03C09J11/06C09J103/06C09J103/08C09J175/04C08L75/04C08L71/14C08K5/12C08K5/14C08L3/04
Inventor 郑波何星基何星存
Owner GUILIN AONISITE ENERGY SAVING & ENVIRONMENT PROTECTION TECH
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