Forming method adopting infiltration method to make reactive sintering silicon carbide ceramic and die

A technology for sintering silicon carbide and silicon carbide ceramics, applied in the field of materials science, can solve the problems of reducing yield and quality, organic matter removal process defects, silicon carbide body defects, etc. The effect of trimming process and uniform particle distribution

Pending Publication Date: 2018-03-23
朱胜利
View PDF4 Cites 8 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Carrying out the two at the same time is likely to cause defects in the silicon carbide body, and the removal of organic matter is also likely to cause further defects
In addition, due to air bubbles, pouring molding is also prone to produce pores in the green body, which reduces the yield and quality

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Forming method adopting infiltration method to make reactive sintering silicon carbide ceramic and die

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0065] This embodiment is mainly used to make ceramic products such as grinding buckets, slurry pumps or sandblasting nozzles.

[0066] 1), material preparation

[0067] 1.1), select silicon carbide powder with a mesh number of 40, a ratio of 60%, a mesh number of 240, a ratio of 10%, a mesh number of 1000, a ratio of 20%, a mesh number of 3000, a ratio of 3%, and a maximum particle size of less than 0.5 The micron ratio is 7% carbon material;

[0068] 1.2), select cotton cloth as the resin diffusion channel material, and the size and shape of the cotton cloth are made according to the design requirements in the mould;

[0069] 1.3), select an appropriate amount of thermosetting phenolic resin (strong base is catalyst) as binding agent; Select mixed acid as curing agent, the consumption of curing agent is 5% of resin;

[0070] 2) Pre-production work

[0071] 2.1), prepare the mould, spray the release agent on the inner surface of the mould, and do the demoulding treatment; ...

Embodiment 2

[0088] This embodiment is a method for making a silicon carbide ceramic sealing ring.

[0089] The friction coefficient of the "self-lubricating" sealing ring made of silicon carbide powder and graphite material is much lower than that of the sealing ring made of alumina ceramics and various hard alloys. Silicon carbide ceramics and graphite The abrasion resistance of sealing rings made of materials is much higher than that of graphite materials. Combined with the characteristics of corrosion resistance, high strength and high hardness of silicon carbide ceramics, the sealing rings made of silicon carbide ceramics and graphite materials are used in many harsh environments. It can also be used normally under the working conditions.

[0090] At present, the manufacturing process of silicon carbide ceramic sealing rings is mainly based on the use of nano-scale ultra-fine silicon carbide powder to sinter at normal pressure to make the seal ring, and the use of nano-scale ultra-fin...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

The invention belongs to the technical field of materialogy, and particularly relates to a forming method adopting an infiltration method to make reactive sintering silicon carbide ceramic and a die.The forming method includes following steps: 1), filling a mixture formed by uniform mixing into the die with a resin diffusion passage, and continuously vibrating the die in the process of filling the mixture, wherein the mixture comprises silicon carbide powder and a carbon material; 2), filling the die with the mixture, compacting, and then sealing the die, wherein compacting refers to compacting or pressurizing for compacting; 3), injecting resin serving as a binder into the die to enable the resin to infiltrate into gaps inside the mixture; 4), heating to enable the resin in the die to becured to obtain a silicon carbide ceramic blank; 5), putting the silicon carbide ceramic blank into a sintering furnace for reactive sintering to obtain the silicon carbide ceramic. The infiltrationmethod is adopted to make the reactive sintering silicon carbide ceramic, so that limitation caused by particle size of the silicon carbide powder is avoided, and requirements on using quality of various silicon carbide products can be met.

Description

technical field [0001] The invention belongs to the technical field of materials science, and in particular relates to a molding method and a mold for making reaction-sintered silicon carbide ceramics by adopting an infiltration method. Background technique [0002] Silicon carbide ceramic materials have excellent properties such as high temperature strength, high temperature oxidation resistance, good wear resistance, good thermal stability, small thermal expansion coefficient, high thermal conductivity, high hardness and chemical corrosion resistance. Protection, space technology, information electronics, energy and other fields have increasingly wide applications. [0003] At present, there are many silicon carbide ceramic blank forming processes and sintering process technologies. Although the silicon carbide ceramics produced by most of the process technologies have excellent performance, they are different due to the complex manufacturing process of the products, stric...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
IPC IPC(8): C04B35/573C04B35/622B28B7/00B28B7/16B28B7/42
CPCC04B35/573C04B35/622B28B7/0002B28B7/16B28B7/42C04B2235/616C04B2235/656
Inventor 关小芬朱胜利朱宏吴中民强军锋郭庆功刘振宇王晓辉
Owner 朱胜利
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products