Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

High-temperature-resisting and low-temperature-resisting extreme pressure lubricating grease with long service life and preparation method thereof

An extreme pressure grease and extreme pressure lubrication technology, applied in the field of grease, can solve problems such as poor product stability, affecting product low temperature performance, complex production process, etc., achieve good extreme pressure and wear resistance, and is beneficial to large-scale The effect of production and production process safety and environmental protection

Active Publication Date: 2018-03-23
JIANGSU LOPALTECH
View PDF9 Cites 22 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

CN105087108A discloses a high and low temperature resistant lubricating grease and its preparation method, which is formed by thickening polyalphaolefin with composite calcium sulfonate soap and adding additives such as extreme pressure and oxidation. Not only the preparation process is complicated, but the product stability is poor , and the product is prone to hardening problems after being placed for a long time
CN102286306A also proposes a high-temperature, water-resistant, long-life complex lithium-calcium-based grease and its preparation method, which uses the mixture of complex calcium sulfonate soap and complex lithium-calcium soap as the thickener, the production process is complicated, and the dropping point of the prepared product is Below 300°C, at the same time, the addition of complex calcium sulfonate soap will affect the low-temperature performance of the product, which cannot better meet the requirements of low-temperature use
In addition, the low-temperature lubricating greases reported in other related patents are mostly made of polyalphaolefin or ester oil thickened with lithium soap and lithium complex soap. There are problems such as the need for prefabricated soap or the poor compatibility of the grease with additives, which will cause problems accordingly. Increase production difficulty or reduce product performance

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • High-temperature-resisting and low-temperature-resisting extreme pressure lubricating grease with long service life and preparation method thereof
  • High-temperature-resisting and low-temperature-resisting extreme pressure lubricating grease with long service life and preparation method thereof
  • High-temperature-resisting and low-temperature-resisting extreme pressure lubricating grease with long service life and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] Get polyalphaolefin oil PAO10 92.88kg and alkylnaphthalene Synesstic12 30.96kg to mix as mixed base oil (40 ℃ kinematic viscosity of mixed base oil is 78mm 2 / s, the viscosity index is 123). Take 82.2kg of mixed base oil, 10.5kg of 12-hydroxystearic acid, and 3.54kg of sebacic acid and add them to the saponification reaction kettle in sequence, start stirring and raise the temperature to 82°C, then add 4.92kg of lithium hydroxide oil solution, after the addition is completed, put Saponification reaction at 95-105°C for 90 minutes, then heat up to 135°C for 30 minutes, add 0.45kg of antioxidant Irganox L57 and 0.75kg of structure improver Lubrizol2002D, continue to heat up to 215°C and keep it warm for 5 minutes, and finally transfer the material to the blending Add the remaining 41.64kg of mixed base oil to the kettle to lower the temperature. After the temperature drops below 90°C, add 1.5kg of molybdenum dialkyldithiocarbamate, 1.5kg of zinc dialkyldithiophosphate, an...

Embodiment 2

[0020] Get polyalphaolefin oil PAO40 37.8kg, PAO10 70.33kg and alkylnaphthalene Synesstic12 12.01kg to mix as mixed base oil (40 ℃ kinematic viscosity of mixed base oil is 115mm 2 / s, the viscosity index is 138). Take 80kg of mixed base oil, 13.5kg of 12-hydroxystearic acid, and 4.55kg of sebacic acid and add them to the saponification reactor in sequence, start stirring and raise the temperature to 82°C, then add in turn the emulsion containing 0.80kg of calcium hydroxide, 4.86kg of hydrogen Lithium oxide oil solution, saponification reaction at 105°C for 75 minutes after feeding, then heat up to 140°C for 40 minutes, add 0.075kg of antioxidant Irganox L57 and 0.75kg of structure improving agent Lubrizol 2002D, continue to heat up to 220°C and keep warm for 5 Minutes, finally transfer the material to the blending kettle, add the remaining 40.14kg of mixed base oil to cool down, and add 3kg of molybdenum dialkyldithiophosphate and 1.5kg of zinc dialkyldithiophosphate in sequen...

Embodiment 3

[0022] Get polyalphaolefin oil PAO10 103.29kg and alkyl naphthalene SynNaph23 19.4kg to mix as mixed base oil (40 ℃ kinematic viscosity of mixed base oil is 80mm 2 / s, the viscosity index is 129). Take 86kg of mixed base oil, 10.5kg of 12-hydroxystearic acid, and 4.23kg of sebacic acid and add them to the saponification reaction kettle in sequence, and start stirring to raise the temperature to 82°C, then add 5.08kg of lithium hydroxide oil solution, and after the addition is completed, the temperature rises at 95°C. ~105°C saponification reaction for 90 minutes, then heat up to 135°C for 30 minutes, add 0.25kg of antioxidant Irganox L135, 0.5kg of Irganox L57 and 1.5kg of structure improver Lubrizol 2002D, continue to heat up to 210°C and hold for 5 minutes, and finally Transfer the material to the blending kettle, add the remaining 36.69kg of mixed base oil to cool down, and then add 2.25kg of molybdenum dialkyldithiocarbamate, 1.5kg of thiadiazole derivatives, and dinonylnap...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
Kinematic viscosityaaaaaaaaaa
Kinematic viscosityaaaaaaaaaa
Kinematic viscosityaaaaaaaaaa
Login to View More

Abstract

The invention discloses high-temperature-resisting and low-temperature-resisting extreme pressure lubricating grease with long service life and a preparation method thereof. The lubricating grease isprepared from the following components in percentage by weight: 80 percent to 85 percent of mixed basic oil, 9 percent to 16 percent of a thickening agent, 0.5 percent to 1.5 percent of a structure improver, 1.0 percent to 3.0 percent of an extreme pressure anti-wear agent, 0.5 percent to 1.5 percent of a metal deactivating agent, 0.05 percent to 1.5 percent of an anti-rust agent and 0.3 percent to 1.5 percent of an antioxidant, wherein the mixed basic oil contains alkyl naphthalene and the alkyl naphthalene accounts for 10 weight percent to 30 weight percent of the mixed basic oil. The high-temperature-resisting and low-temperature-resisting extreme pressure lubricating grease has the advantages that the product has excellent high temperature performance, water resistance, extreme pressure resistance and anti-wear performance and has a stable structure; the production is safe and environmentally friendly and the technology is simple; the high-temperature-resisting and low-temperature-resisting extreme pressure lubricating grease is suitable for various lubricating occasions with high-temperature-resisting and low-temperature-resisting requirements and extreme pressure anti-wear requirements, such as fields including automobile hub bearings, equal-speed universal joints and high-temperature bearings.

Description

technical field [0001] The invention belongs to the field of lubricating grease, and in particular relates to a high-low temperature resistant long-life extreme-pressure lubricating grease and a preparation method thereof. Background technique [0002] Under the current situation of global economic slowdown, equipment owners and operators hope to reduce equipment maintenance costs, which makes people look for equipment that can still perform well under high temperature, low temperature, heavy load and other conditions, and has long grease change intervals. Long-life greases create greater demands. The high dropping point grease mainly includes calcium complex grease, lithium complex grease, aluminum complex grease, calcium sulfonate complex grease, polyurea grease and bentonite grease, among which lithium complex grease It has the advantages of safety and environmental protection in the production process, advanced production technology, good compatibility with additives, a...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
IPC IPC(8): C10M169/00C10N50/10C10N30/08
CPCC10M169/00C10M2201/062C10M2203/065C10M2205/0206C10M2207/127C10M2207/128C10M2215/223C10M2219/044C10M2219/068C10M2219/106C10M2223/045C10N2030/08C10N2050/10C10N2030/26C10N2010/12C10N2020/02C10N2010/04
Inventor 杨操朱国靖
Owner JIANGSU LOPALTECH
Features
  • Generate Ideas
  • Intellectual Property
  • Life Sciences
  • Materials
  • Tech Scout
Why Patsnap Eureka
  • Unparalleled Data Quality
  • Higher Quality Content
  • 60% Fewer Hallucinations
Social media
Patsnap Eureka Blog
Learn More