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Quality Control Method of Intermittent Vacuum Evaporation of Sodium Chloride Aqueous Solution

A sodium chloride aqueous solution and a control method technology, applied in the field of evaporation and crystallization in chemical industry, can solve the problems of unfavorable production of high-quality sodium chloride products, rough control precision, etc.

Inactive Publication Date: 2021-03-16
TIANJIN UNIV
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  • Claims
  • Application Information

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Problems solved by technology

[0004] At present, the control of the evaporation rate of water quality in the industrial production process of sodium chloride is often based on the evaporation experience accumulated in a large number of small or pilot experiments. The control accuracy is often rough, which is not conducive to the production of high-quality sodium chloride products.

Method used

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  • Quality Control Method of Intermittent Vacuum Evaporation of Sodium Chloride Aqueous Solution
  • Quality Control Method of Intermittent Vacuum Evaporation of Sodium Chloride Aqueous Solution
  • Quality Control Method of Intermittent Vacuum Evaporation of Sodium Chloride Aqueous Solution

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Embodiment 1

[0052] The sodium chloride evaporating crystallizer is cylindrical, with a diameter of 200mm, an initial height of sodium chloride solution of 150mm, a constant evaporation temperature of 40°C (at this temperature, the saturated mass fraction of sodium chloride is 0.267936), and a constant operating pressure of 5000Pa. The mass fraction of salt is 0.10, and the evaporation process adopts batch operation.

[0053] Since the initial salt concentration is 0.10, which is less than the saturation concentration of 0.267936 at 40°C, the sodium chloride aqueous solution in the previous vacuum evaporation process belongs to the concentration process of salt. At this time, the quality control method of water vacuum evaporation is as follows:

[0054] Step 1: Calculate the evaporation temperature difference

[0055] According to the evaporation temperature, operating pressure and salt concentration, the temperature difference is calculated by the following formula

[0056]

[0057] ...

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Abstract

The invention relates to a method for controlling the intermittent vacuum evaporation mass of a sodium chloride aqueous solution, which is mainly applied to the intermittent vacuum evaporation and concentration of the sodium chloride aqueous solution as well as crystallization process design, computer simulation and process control thereof, and belongs to the field of chemistry and chemical engineering evaporation and crystallization. The method for controlling the vacuum evaporation mass of the sodium chloride aqueous solution provided by the invention uses a numerical method to carry out design calculation mainly according to a novel evaporation model and a temperature difference model, so as to achieve the purpose of accurately controlling the water evaporation mass in the vacuum evaporation process of the sodium chloride aqueous solution; the method for controlling the intermittent vacuum evaporation mass of the sodium chloride aqueous solution has wide laboratory and industrial application prospect, is beneficial to the design and control of the evaporation, concentration and crystallization process of the sodium chloride aqueous solution, can be applied to the processes of waste water desalination, sea water desalination and sodium chloride industrial crystallization, and is in favor of the promotion of the technological level in the environmental protection and resourcerecycling and utilizing in China.

Description

technical field [0001] The invention relates to a method for controlling the water evaporation quality in the intermittent vacuum evaporation process of sodium chloride aqueous solution, and is of great significance to the design, computer simulation and control of the sodium chloride evaporation concentration and crystallization process. The invention can be used in waste water desalination, seawater desalination and salt industrial production process, and belongs to the field of evaporation and crystallization in chemical industry. Background technique [0002] As an important chemical raw material and food flavoring agent, sodium chloride is mainly produced by evaporative crystallization because its solubility in water changes little with temperature. Evaporation technology mainly includes traditional sun drying method and vacuum evaporation technology. Sea salt, lake salt and well salt with a long history are generally obtained by drying. However, the production of sod...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01D1/00B01D9/02
CPCB01D1/00B01D9/0018B01D9/0063Y02A20/124
Inventor 刘勇罗琼那平王国栋赵思源
Owner TIANJIN UNIV
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