482results about "Crystallization regulation/control" patented technology

The invention relates to the technical field of parameter adjustment, and discloses a low-temperature evaporative crystallization machine parameter adjustment method, device and equipment and a storage medium, and the method comprises the steps: collecting M groups of temperature sensor data and N groups of pressure sensor data of a low-temperature evaporative crystallization machine, calculating a first uncertainty representation of temperature parameter measurement and a second uncertainty representation of pressure parameter measurement; performing data fusion to obtain an optimal estimated value of a temperature state and an optimal estimated value of a pressure state; parallel prediction is carried out through the thermodynamic equilibrium model, the crystallization kinetic model and the system response model, and a crystallization process prediction result is obtained; according to the technical scheme of the invention, the interference of the feeding fluctuation, the environmental change and the like can be effectively handled, and the real-time updating of the control strategy and the accurate adjustment of the temperature and pressure parameters can be realized.

The invention relates to the technical field of grease production control, in particular to a grease product production control method and system based on intelligent digitization. The method comprises the following steps: monitoring temperature, viscosity and turbidity data in a grease crystallization process in real time, and generating grease crystallization state snapshot data; performing crystallization state prediction according to the grease crystallization state snapshot data, and performing reaction kettle cooling rate adjustment to obtain a target control cooling rate; performing real-time stirring rotating speed adjustment fuzzy reasoning on the grease crystallization state snapshot data to generate a corrected grease stirring speed; and performing control instruction conversion on the target control cooling rate and the corrected grease stirring speed, executing a production control instruction, and generating a grease crystallization process control report. By accurately controlling the cooling rate and the stirring speed, intelligent control over the grease crystallization process is achieved, and the quality and stability of grease products are remarkably improved.

The invention provides a sulfamic acid continuous crystallization production device and process, the sulfamic acid continuous crystallization production device comprises a filter box and a production box, the production box is fixedly connected to the upper surface of the filter box through bolts, the top end of the production box is provided with a feeding pipe, the middle part of the interior of the production box is provided with a partition plate, and the middle part of the partition plate is provided with a conveying pipe; a discharging pipe, a production reaction module and a filtering and cleaning module are arranged between the production box and the filtering box. According to the sulfamic acid continuous crystallization production device and the sulfamic acid continuous crystallization production process, in the sulfamic acid continuous crystallization production process, when sulfamic acid crystals are filtered out from mother liquor through the filter cartridge, purified water is sprayed into the filter cartridge through the spray head; and the sulfamic acid crystals can be quickly and uniformly washed to remove impurities through the filter cartridge which continuously shakes in a reciprocating manner in the rotating process, so that the continuous crystallization production efficiency of the sulfamic acid can be effectively improved.

The invention relates to the technical field of equipment management and control, in particular to an evaporative crystallization equipment operation management and control system and method based on multi-modal perception, and the system comprises a raw material characteristic analysis module, a temperature regulation and control module, a heating time adjustment module and an equipment maintenance management module. According to the method, the energy utilization efficiency and the raw material conversion rate are optimized by analyzing the characteristics of the raw materials and adjusting the heating temperature in the evaporative crystallization process, the energy utilization efficiency is improved by monitoring the time change of the quality of the raw materials, evaluating the evaporation rate of the raw materials and dynamically adjusting the heating time, and meanwhile, the energy consumption of equipment is reduced; by monitoring the power consumption, voltage and current data of equipment operation and combining the maintenance history of the equipment, the operation stability of the equipment can be accurately evaluated, the maintenance requirements of the equipment can be identified in time, faults can be prevented in advance, the long-term stable operation of the equipment is ensured, and the continuity and safety of the production process are ensured.

The invention relates to a continuous oscillatory flow crystallization device with a V-shaped connecting pipe structure. According to the technical scheme, the device specifically comprises a tubular crystallizer assembly of a V-shaped connecting pipe structure, an oscillatory flow pump driving mechanism, a feeding mechanism, a discharging mechanism, a circulating cooling mechanism and an intelligent control system. Through the structural design of the V-shaped connecting pipe, periodic circulation can be formed in the chamber, the radial mixing strength is remarkably enhanced, the impact force of fluid on the wall surface is increased, and a heat transfer boundary layer is thinned, so that the technical bottleneck of non-uniform crystal suspension at a high solid-to-liquid ratio is effectively solved, and heat transfer and mass transfer in the continuous crystallization process can be enhanced; no stirring paddle or moving mechanical part is arranged inside, so that suspended crystal particles are effectively prevented from being broken and nucleated; and in the nucleation dominant area, through alternate cooling crystallization and heating dissolution operation, crystal scales on the pipe wall and fine grains in the mother liquor can be dissolved, and the number of crystal nucleuses in the crystallization mother liquor can be regulated and controlled, so that controllable production of expected particle size distribution of a crystallization product is realized, and the problem of scaling on the pipe wall is effectively solved.

The invention relates to the technical field of automatic control, in particular to a monitoring method and system for synthesizing ceramide based on alpha-hydroxy fatty acid, and the monitoring system for synthesizing ceramide based on alpha-hydroxy fatty acid comprises a raw material feeding module, a reaction control module, a quenching-crystallization joint control module and a data integration module; carrying out dynamic weighing monitoring on the raw materials based on the received synthesis instruction, and starting a reaction kettle according to weighing data; performing multi-dimensional data acquisition in real time according to the set reaction data, and performing dynamic feeding control according to the set reaction data; when the TLC detection substrate reaction is completed, the cooling process and the crystallization process are regulated and controlled in real time according to the reaction data until the end point judgment standard is met; according to a received synthesis completion instruction, product quality data is obtained, a monitoring data packet is generated, the synthesis instruction is marked and then stored, process control is accurately monitored and controlled, and the purity and crystal form of the product are ensured.

The invention belongs to the technical field of freeze concentration, and relates to a freeze concentration method, which comprises the following steps: freezing a dilute solution to obtain a solid or a solid-liquid mixture, crushing the solid or solid-liquid mixture obtained by freezing, or firstly separating the solid-liquid mixture and then crushing the solid, and adopting dry gas as an energy medium, and penetrating the crushed solid and transferring heat, and staged reserving the solution to realize freezing concentration of the dilute solution. The method improves the efficiency of freeze concentration and separation purification, is simple to operate, and can be conveniently applied to the fields of food, cosmetics, biological medicine, petrochemical industry, environment-friendly treatment and the like.

The invention provides a system and a method for producing high-purity electronic-grade carbonic ester, and the system comprises a heterogeneous reaction section, a separation section and a crystallization section along the material flow direction, the heterogeneous reaction section is used for carrying out heterogeneous reaction on ethylene oxide and carbon dioxide to prepare carbonic ester; the separation section is used for separating materials from the heterogeneous reaction section and comprises a flash evaporation unit and a rectification unit in the material flow direction, and the flash evaporation unit comprises at least one flash evaporation tank; the rectification unit comprises at least one rectification tower, and the side-draw of the rectification unit is communicated with the feed port of the crystallization section; and the crystallization section is used for crystallizing and purifying the material mainly containing carbonic ester from the separation section. According to the method, high-purity ethylene carbonate used as a power battery can be obtained from the crystallization section, and crystallization mother liquor can be selectively returned to the separation section to be concentrated. The method can effectively improve product purity, reduce product chromaticity and reduce energy consumption, and can be applied to industrial production of carbonic ester.

The invention provides an intelligent dynamic flow rate regulation and double-effect crystallization evaporation device which comprises a feeding system, a double-effect evaporation system, a crystallization system, a circulating pump and a flow rate regulation system, the feeding system is connected to the double-effect evaporation system through a pipeline, the double-effect evaporation system is connected to the crystallization system through the circulating pump, and the flow rate regulation system is connected to the crystallization system through a pipeline. The flow rate adjusting system is connected with the circulating pump and the double-effect evaporation system, and the device realizes intelligent dynamic flow rate adjustment through the circulating closed-loop control system, so that the evaporation efficiency and the crystallization quality are optimized. The circulating closed-loop control system comprises a data acquisition unit, a data processing unit, a flow velocity adjusting system, a feedback optimization unit and an abnormity early warning unit, a flow velocity adjusting strategy is optimized based on real-time data, historical data and machine learning, scaling is reduced through disturbance flow velocity control, and the system stability is improved. The evaporation and crystallization efficiency is improved, the energy consumption is reduced, different working condition requirements are met, and the method is suitable for the field of industrial evaporation and crystallization.

The invention belongs to the technical field of sugar alcohol preparation, and relates to a preparation method of anhydrous lactitol crystals with controllable granularity, which comprises the following steps: putting a lactitol concentrated solution with the refraction of 80-82% and the temperature of 75-80 DEG C into a crystallizer, and then cooling at the cooling rate of 0.5-1 DEG C / min; when the temperature is reduced until crystals are separated out, cooling is stopped, the current temperature is maintained for 1-4 h, then the cooling rate is adjusted to be 1-1.5 DEG C / min, and cooling continues; when the temperature is reduced to 20-30 DEG C, stopping cooling, and maintaining the current temperature to grow the crystal for 1-3 hours to obtain massecuite; centrifuging the massecuite to obtain wet sugar; feeding the wet sugar into an air dry oven, drying for 1 hour with hot air at the temperature of 50-60 DEG C, slowly heating to 85-90 DEG C at the speed of 5-10 DEG C / h, staying for 1 hour, slowly heating to 105-115 DEG C at the speed of 5-10 DEG C / h, and staying for 1 hour again, so as to obtain the anhydrous lactitol crystal. The anhydrous lactitol is prepared by adopting gradient cooling crystallization and gradient heating drying modes, the anhydrous lactitol crystal with controllable particle size distribution is obtained, and the production difficulty is greatly reduced.

A method of forming lithium carbonate from a lithium-bearing solution including:evaporating the lithium-bearing solution to precipitate a first group of impurities;removing the first group of impurities to form a first purified solution; andperforming a flash crystallisation step within a predetermined temperature range to crystallise a second group of impurities from the first purified solution;removing the second group of impurities from the first solution to form a second purified solution, wherein at least 90 wt % of lithium is recovered from the first purified solution; andreacting the second purified solution with a metal carbonate to form lithium carbonate of at least 90 wt % purity.

The invention provides a cooling rate optimization control method and system for continuous cooling crystallization, and the method comprises the steps: collecting crystal slurry concentration data and temperature data of each stage of crystallization tank in real time; the crystal slurry concentration data, the temperature data and the feeding flow data are input into a deep learning model, and a prediction result is obtained; based on the prediction result and crystal mush concentration data, dynamically adjusting the cooling rate of each stage of crystallizing tank and the addition amount of a co-crystallizing solvent; and feeding back an outlet crystal mush concentration signal of the last-stage crystallizing tank to the solid-liquid separation unit, and adjusting the running rotating speed of the solid-liquid separation unit in a linkage manner. According to the cooling rate optimization control method and system for continuous cooling crystallization, prospective correction of the cooling rate is carried out by using the predicted supersaturation degree, and adjustment of the additive amount of the auxiliary crystallization solvent is carried out by using the predicted crystal particle size distribution; and finally, an outlet concentration signal of the last-stage crystallizing tank is fed back to the solid-liquid separation unit in real time to adjust the separation rotating speed in a linkage manner, so that the crystal particle size deviation is reduced, and the triazole crystallization recovery rate is improved.

The invention belongs to the technical field of biological medicine, and particularly relates to sterile cefepime hydrochloride and a direct preparation method thereof. The method comprises the following steps: firstly, carrying out condensation reaction on a 7-MPCA solution and an AE active ester solution through a solid base catalyst column at the same time; then, carrying out extraction phase separation, two times of pH regulation crystallization, activated carbon decoloration and sodium sulfite reduction on the condensation liquid to obtain a cefepime hydrochloride liquid to be crystallized; and then taking a part of the cefepime hydrochloride to-be-crystallized liquid to prepare a seed crystal mixed liquid, and adding the rest of the cefepime hydrochloride to-be-crystallized liquid and the crystallization solvent into the seed crystal mixed liquid at a specific speed to obtain the sterile cefepime hydrochloride. According to the method disclosed by the invention, the continuous production of the sterile cefepime hydrochloride is realized, the preparation period of the sterile cefepime hydrochloride is greatly shortened, side reactions and product degradation are reduced, the quality and yield of the obtained cefepime hydrochloride product are relatively high and stable, and industrial production is facilitated.

The invention provides an ultrasonic-assisted gamma-aminobutyric acid crystallization particle size regulation and control method, which comprises the following steps: removing impurities and decolorizing gamma-aminobutyric acid-containing feed liquid, heating, stirring and concentrating to a nearly saturated state, then carrying out ultrasonic-assisted crystallization, cooling, aging and suction filtration to obtain coarse crystals, and finally washing and drying to obtain target crystals. According to the method, a synergistic process of raw material liquid pretreatment, evaporation concentration-ultrasonic-cooling coupling crystallization, aging and post-treatment is adopted, an ultrasonic cavitation effect is utilized to reduce a nucleation barrier, and a supersaturation degree precise control and gradient cooling strategy is combined, so that grain size refinement, obvious narrowing of distribution and effective inhibition of agglomeration of crystals are realized; the median particle size of the crystal can be controlled to be smaller than or equal to 200 microns, the particle size distribution span is smaller than or equal to 1.5, the agglomeration phenomenon is remarkably inhibited, the crystal form is kept stable, the crystal habit is complete and smooth, the crystal product quality and the process efficiency are remarkably improved, and the method has important industrial application value.

The invention belongs to the technical field of energy storage batteries, and particularly relates to a desalting, dehumidifying and cooling integrated thermal management device and method for a marine environment energy storage battery. The device is composed of an energy storage battery module, an air inlet dehumidification and desalination module, an air return reprocessing module, a salt crystallization and separation module, a cold source heat exchanger and a heat source heat exchanger. Wherein the inlet air dehumidification and desalination module cools inlet air by utilizing a first solvent and inlet air cross flow heat exchange mode, meanwhile, the first solvent dissolves salt mist ions in inlet sea wind, and the purposes of reducing the dew point temperature and dehumidifying the inlet sea wind are further achieved; in order to ensure water-salt concentration balance of the first solution, a salt crystallization precipitation module and a return air retreatment module are adopted to jointly adjust the concentration of the first solution. A solution is provided for safe and reliable operation of the energy storage battery system under the ocean high-temperature, high-humidity and high-salt links.

A method of making colloidal kagome superlattices can include functionalizing a plurality of metal nanoparticles with a plurality of oligonucleotides to produce programmable atom equivalents; and cooling the programmable atom equivalents to induce crystallization of the programmable atom equivalents. The cooling process can include cooling the PAEs from a first temperature to a second temperature at a first cooling rate, cooling the PAEs from the second temperature to a third temperature at a second cooling rate, and cooling the PAEs from the third temperature to a fourth temperature at a third cooling rate. The kagome superlattices can have a rhombohedral unit cell formed by alternating chiral layers of PAEs organized in 2-dimensional distorted kagome layers. The colloidal superlattices can have anisotropic light emission, Purcell factors of at least 25 and birefringent properties.

The invention relates to a one-way valve and static crystallization equipment. The one-way valve comprises a valve body and a valve cover which are hinged, a second rack and a first rack which are meshed with each other are arranged on the valve body and the valve cover respectively, and when the one-way valve is opened, a gap is formed between the second rack and the first rack. The valve body and the valve cover which are hinged are arranged, the second rack and the first rack which are meshed with each other are arranged on the valve body and the valve cover correspondingly, when the one-way valve is opened, a gap is formed between the second rack and the first rack, and the valve body can be sealed through cooperation of the second rack and the first rack; under the impact action of airflow, the valve cover and the valve body are repeatedly opened and closed, at the moment, a small gap is formed between the first rack and the second rack, gas overflows from the gap, the gap between the racks assists the gas in further reducing bubbles formed by the gas, more small bubbles are formed, the number and dispersity of the bubbles are increased, the crystallization time is shortened, and the crystallization efficiency is improved; the energy consumption is reduced and the finished product purity is improved.

The invention relates to a liquid level control device of a vacuum crystallizer. Relates to the technical field of vacuum crystallization. The device comprises a flash tank arranged below a crystallization pot, the flash tank is provided with an overflow port, and the bottom end of a discharge pipe extends into the flash tank and is lower than the overflow port, so that feed liquid and liquid level in the flash tank automatically flow out of the overflow port when reaching the height of the overflow port. The overflow port is formed in the overflow groove, the bottom end of the discharge pipe extends to the position below the overflow port in the overflow groove, when the liquid level of feed liquid in the overflow groove reaches the height where the overflow port is located, the feed liquid automatically flows out of the overflow port, liquid level control over the feed liquid in the overflow groove is achieved, and therefore the liquid level of the feed liquid in the overflow groove is controlled. The liquid level control device is simple in structure, reliability of liquid level control in the vacuum crystallizer can be improved, and then the effect of liquid level control in the vacuum crystallizer is guaranteed.

The invention discloses a crystallization system, a crystallization method and application thereof. The crystallization system comprises a crystallizer, a wet grinder and a liquid level control module, the crystallizer is externally connected with a circulation loop, and the wet grinder is arranged on the circulation loop; a liquid discharge pipeline is arranged on the crystallizer, and a liquid discharge pump is arranged on the liquid discharge pipeline; the liquid level control module comprises an ultrasonic liquid level measurement signal transmission and conversion unit and a PID (Proportion Integration Differentiation) control unit; the PID control unit comprises a signal processing element and a feedback element, and the feedback element is connected with the liquid discharge pump. The crystallization system and the crystallization method have the advantages of high yield and high yield, and crystal grains with excellent uniformity can be obtained.

The invention provides a production device and process for increasing the content of magnesium citrate crystals. The problems that in the prior art, the impurity co-crystallization rate is high, and crystal forms are difficult to control are solved. The device comprises a gradient temperature control multi-stage crystallization device and a crystal form directional regulation and self-adaptive separation system. The gradient temperature control multi-stage crystallization device is composed of a main crystallizer, a gradient temperature control system, an ultrasonic-assisted system and a liquid phase partition circulating system, and the crystallization environment is accurately controlled through the temperature gradients of five independent temperature zones. The crystal form directional regulation and self-adaptive separation system is composed of a seed crystal dynamic inoculation device, an electric field auxiliary directional crystallization system, a real-time crystal morphology analysis system and a self-adaptive separation system, and the crystal morphology and particle size distribution can be accurately controlled. According to the process disclosed by the invention, the main content of magnesium citrate is increased to 98.8 + / -0.3%, heavy metal impurities and organic impurities are respectively reduced by 70% and 75%, the crystal form consistency is increased to 96 + / -2%, the production period is shortened by 33%, and the process has remarkable economic benefits and social benefits.

The invention relates to the technical field of mixing equipment, and discloses a mixing preparation device and method for a plant growth regulator containing a silicon element. The mixing preparation device of the silicon-containing plant growth regulator comprises a stirring main kettle, an online monitoring unit, a solid-liquid separation unit and a control unit, the stirring main kettle is used for carrying out a liquid-phase chemical reaction and separating out a solid product in situ, and is provided with a stirring piece; and the on-line monitoring unit is used for acquiring a reaction process signal and a crystallization state signal in the main stirring kettle in real time. The online monitoring unit, the solid-liquid separation unit and the control unit are arranged and cooperatively used, dynamic optimization management of the reaction crystallization process is achieved, the solid-liquid separation unit moves out crystals in time and circularly supplements materials, the problem that the crystals are secondarily wrapped is solved, meanwhile, reaction balance is pushed to move rightwards, and the reaction efficiency is improved. The conversion rate and the yield are improved.

The invention provides a p-xylene crystallization tower. The p-xylene crystallization tower comprises a tower body, a cooling structure and a scraper structure, mixed xylene is contained in the tower body; the cooling structure comprises a sealing plate and liquid conveying pipes arranged at the upper end and the lower end of the sealing plate respectively, and the sealing plate surrounds the periphery of the tower body; the sealing plate is wavy; the sealing plate comprises a plurality of wave trough parts and a plurality of wave crest parts which are alternately arranged, the wave trough parts are tightly connected with the periphery of the tower body, and the sealing plate and the periphery of the tower body define a circulation channel extending in the vertical direction between any two adjacent wave trough parts; the liquid conveying pipes are arranged on the periphery of the tower body in a surrounding mode, and the two liquid conveying pipes communicate with the multiple circulation channels correspondingly. And the refrigerating medium is input into the circulation channel through the liquid conveying pipe. And the mixed xylene is cooled under the action of the refrigerating medium, and paraxylene is crystallized and separated out on the inner circumferential wall of the tower body. And the scraper structure scrapes crystals on the tower body. According to the p-xylene crystallization tower, a refrigerating medium is in close contact with the tower body, so that the dissipation of cold energy is effectively reduced, and the refrigerating effect is improved.

The invention provides a production device and process for recovering electronic-grade phosphoric acid from waste etching liquid. The device comprises a raw material storage tank, a multi-stage filtration system, a phosphoric acid evaporation kettle, a purification system, a mixed acid storage tank and a neutralization reaction and crystallization system. The waste etching liquid enters an evaporation kettle after being subjected to multi-stage filtration to remove suspended solid particles, and phosphoric acid is separated from volatile nitric acid and acetic acid; and condensing the volatile acid into mixed acid for storage, and removing metal ions from the semi-finished phosphoric acid through a purification system to obtain the electronic-grade phosphoric acid. The mixed acid reacts with alkali to generate a mixed solution of sodium acetate and nitric acid, sodium acetate crystals are separated out through evaporation and concentration, a solid product is obtained after separation, nitric acid is obtained by condensing gas, and suspended particles and metal impurities are subjected to incineration treatment. Through the steps of filtering, negative-pressure evaporation, neutralization and crystallization and the like, the process realizes efficient recovery of electronic-grade phosphoric acid and byproducts of sodium acetate and nitric acid, and has the characteristics of high resource recovery rate and low pollution emission.

The invention relates to the field of calcium gluconate evaporative crystallization equipment, in particular to a crystallizing tank for calcium gluconate crystallization production and a using method thereof.The crystallizing tank comprises an evaporative crystallization tank body, the evaporative crystallization tank body comprises a tank body, a stirring and uniform heating assembly is arranged on the inner edge of the tank body, and an adaptive adjusting assembly is installed on one side of the stirring and uniform heating assembly; a crystal transfer assembly is arranged at the middle part in the tank body; the stirring and uniform heating assembly is used for stirring the to-be-crystallized solution in the tank body to uniformly disperse heat; the adaptive adjusting assembly is used for adaptively adjusting the stirring and heat uniformizing assembly according to the evaporation progress; according to the crystal stirring device, the situation that the stirring work is easily affected in the later period that the crystals are continuously accumulated at the bottom in the tank body and become high can be avoided, and meanwhile the situation that the crystals are likely to collide with a stirring component along with flowing of a solution, and consequently the crystals are broken can be effectively reduced.

The invention relates to the field of chemical application, and discloses a device for preparing large-particle ammonium sulfate crystals through reduced-speed crystallization. Comprising a neutralization reactor, a settling separation tank, a pre-crystallization solution tank, a first-stage intermittent jacket crystallizer, a second-stage intermittent jacket crystallizer, a filter powder sieving device, an ammoximation tert-butyl alcohol tower reboiler, a heat exchanger group, a stirrer group and a centrifugal pump group, wherein the centrifugal pump group consists of a centrifugal pump I, a centrifugal pump II, a centrifugal pump III, a centrifugal pump IV and a centrifugal pump V; the invention further discloses a process for preparing the large-particle ammonium sulfate crystals through speed-reducing crystallization. The process comprises the following steps: adding rearrangement liquid from a caprolactam rearrangement system and gas ammonia into the neutralization reactor through an external circulation pipeline. By fully utilizing heat in a neutralization reaction and crystallization process and combining with a compound additive, a seed crystal and a speed reduction crystallization technology, an efficient two-stage series crystallization mode is realized, the generation of large-particle ammonium sulfate crystals is promoted, the crystal quality is optimized, the energy consumption is reduced and the production efficiency is improved.

The invention relates to the technical field of insecticides, and discloses an indoxacarb finished product crystallization device and method.The indoxacarb finished product crystallization device comprises a supporting bracket, a stirring tank is arranged at the top of the supporting bracket, an opening plate is arranged on one side of the stirring tank, a mounting frame is arranged at the top of the stirring tank, a driving source is arranged on the mounting frame, and a rotating shaft is arranged at the output end of the driving source; a fixing frame is arranged at the bottom of the inner wall of the stirring tank, and a homogenizing assembly is arranged on the fixing frame; the fixing frame is further provided with a vibration assembly. The homogenizing assembly is used for uniformly mixing the indoxacarb finished product solution in the stirring tank; the vibration assembly is used for reducing the phenomenon of local supersaturation of liquid in the stirring tank through vibration. Compared with the prior art, crystal agglomeration can be reduced, the particle distribution uniformity can be improved, the wall surface scaling risk can be reduced, the cleaning and maintenance frequency can be reduced, and the production efficiency and the product quality can be improved.

According to the low-energy-consumption evaporating crystallizer, a single driving motor is adopted, a rotating shaft rod is used for simultaneously driving a scale scraping assembly arranged in an evaporating cylinder to conduct dynamic scale scraping and solution stirring, one end of the rotating shaft rod passes through a first transmission mechanism and a linkage shaft, and the other end of the rotating shaft rod is driven by a second transmission mechanism. A spiral separation assembly in the gas-liquid separation tank is driven by the direction conversion mechanism to rotate at a high speed so as to strengthen gas-liquid separation; and the other end of the discharging pipe drives a discharging assembly in the discharging pipe to rotate through a second transmission mechanism, so that discharging blockage prevention and negative-pressure deslagging are realized. Through a single power source, cooperative linkage of five functions of scale scraping, stirring, separation, blocking prevention and slag discharging is achieved, the structure is compact, the problems that traditional equipment is serious in scaling, poor in gas-liquid separation effect and prone to blockage during discharging are effectively solved, and meanwhile energy consumption of the equipment is remarkably reduced.

The invention discloses a diiodosilane purification method and a purification processing system, relating to the technical field of diiodosilane. A driving component is provided on a mounting shell, an inner liner is clamped on an output end of the driving component, the driving component is slidably connected to a sliding groove provided on the mounting shell, the inner liner is located in a sliding cavity in the mounting shell, the sliding cavity is communicated with the sliding groove, a limiting component is installed on the mounting shell, a notch is provided on the mounting shell, the limiting component is tilted toward the notch, and the crystals can be quickly taken out by taking out the inner liner, thereby enhancing work efficiency, facilitating the rapid removal of the crystals, and enabling the next crystallization to be carried out quickly. Moreover, by arranging a filter screen and a railing on the inner liner, the residual liquid in the inner liner can be quickly discharged, thereby preventing the residual liquid from affecting the purity of the diiodosilane.

The invention relates to the technical field of ammonium dihydrogen phosphate preparation, and discloses a high-purity ammonium dihydrogen phosphate crystallization device and a method thereof.The high-purity ammonium dihydrogen phosphate crystallization device comprises a first-stage crystallization system, a first-stage centrifugal separation system, a second-stage crystallization system and a second-stage centrifugal separation system which are connected in series. The primary crystallization system comprises a crystal elimination heater, a crystal elimination mixer, a bag filter and a DTB flash cooling crystallizer which are connected in sequence, and is used for primarily purifying a concentrated solution; the primary centrifugal separation system is used for separating primary crystals; the second-stage crystallization system comprises a crystal dissolving tank, an OSLO cooling crystallizer and the like, and deep crystallization is carried out after the first-stage crystal is dissolved; the secondary centrifugal separation system is used for separating secondary crystals; through two-stage crystallization coupling, mother liquor graded circulation, a unique gradient washing process and active impurity control, efficient and continuous production of battery-grade ammonium dihydrogen phosphate with wet-process phosphoric acid as a raw material is realized, the product purity is high, the process flow is simplified, the cost is low, and the system operation is stable.