Polyimide film
A polyimide film and film technology, applied in the directions of lamination, printed circuits, electrical components, etc., can solve the problems of uneven coating, wrinkles or twists, and reduced yield, and achieve excellent electrical insulation and performance improvement. Effect
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[0153] Prepare pyromellitic dianhydride (molecular weight 218.12) / 4,4'-diaminodiphenyl ether (molecular weight 200.24) according to the molar ratio of 1:1, in DMAc (N,N-dimethylacetamide ) to prepare a 23.7% by weight solution and perform polymerization to obtain a 4000 poise polyamic acid solution.
[0154] On the other hand, inorganic particles (with a particle diameter ranging from 0.01 μm to 6.0 μm, an average particle diameter of 0.87 μm, and particles with a particle diameter of 0.5 μm to 2.5 μm, 81.5% by volume of phosphoric acid in all particles were obtained. Hydrogen calcium particles) N,N-dimethylacetamide slurry.
[0155] Add the slurry to the polyamic acid solution so that when the polyimide is formed, the calcium hydrogen phosphate is 0.15% by weight per 1 weight of the polyimide resin, and stir at room temperature for 30 minutes to disperse the inorganic particles in the polyimide. amic acid solution.
[0156] A conversion agent containing acetic anhydride (mo...
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