Modifier mother liquor and road asphalt, and preparation methods thereof

A technology of road asphalt and modifier, applied in building components, building insulation materials, buildings, etc., can solve the problems of poor thermal storage stability, large power consumption, large grinding volume, etc., and improve thermal storage stability. , The effect of high and low temperature performance enhancement, reasonable colloidal structure

Inactive Publication Date: 2018-05-22
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In this method, the proportion of coal tar pitch is relatively high (50-30 parts of coal tar pitch), and the proportion of petroleum pitch is relatively small (10-20 parts of petroleum pitch). , leading to too high content of asphaltene in the asphalt colloidal structure, unreasonable asphalt colloid composition matching, which will lead to poor flexibility of asphalt, poor low temperature performance and thermal storage stability
In addition, adding 5-35 parts of waste rubber powder to asphalt will lead to too high mixing temperature of asphalt and poor thermal storage stability
The preparation process is to pre-mix petroleum pitch, coal tar pitch and co-solvent with SBS, and then grind through a colloid mill. Large size, high power consumption

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] Add 84 parts of anthracene oil with a distillation range of 320~360°C into the reactor, add 0.9 parts of polyphosphoric acid (the concentration of polyphosphoric acid is 110wt%, the same below), heat to about 110°C, and stir for 2 hours. Continue to raise the temperature to about 160°C, then add 1.8 parts of polyphosphoric acid, and stir for 1 hour to obtain modified anthracene oil A1.

[0037] Add 12 parts of SBS (star structure, molecular weight 150,000, the same below) to modified anthracene oil A1, heat to 150°C, and stir for 5 hours to obtain modifier mother liquid A2.

Embodiment 2

[0039] Add 81 parts of anthracene oil with a distillation range of 320~360°C into the reaction kettle, add 0.6 parts of polyphosphoric acid, heat to about 100°C, and stir for 2 hours. Continue to heat up to about 150°C, then add 2.1 parts of polyphosphoric acid, and stir for 1 hour to obtain modified anthracene oil A3.

[0040] Add 14 parts of SBS to modified anthracene oil A3, heat to 155°C, and stir for 6 hours to obtain modifier mother liquor A4.

Embodiment 3

[0042] Add 84 parts of anthracene oil with a distillation range of 320~360°C into the reaction kettle, add 0.9 parts of polyphosphoric acid, heat to about 110°C, and stir for 2 hours. Continue to raise the temperature to about 160°C, then add 2.1 parts of polyphosphoric acid, and stir for 1 hour to obtain modified anthracene oil A5.

[0043] Add 10 parts of SBS to modified anthracene oil A5, heat to 150°C, and stir for 6 hours to obtain modifier mother liquor A6.

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Abstract

The invention discloses a modifier mother liquor and a road asphalt, and preparation methods thereof. The modifier mother liquor comprises, by weight, 78-94 parts of anthracene oil, 0.4-3.2 parts of polyphosphoric acid and 4-20 parts of SBS. The modifier mother liquor is used for the condensation modification of the anthracene oil by using PPA, especially the modification of the anthracene oil through a two-step technology in order to make the anthracene oil reach a suitable condensation degree, so the aroma degree of the anthracene oil is improved, and the content of suitable colloids is increased. The modifier mother liquor is combined with petroleum asphalt and coal pitch to prepare the road asphalt, so the colloidal structure of the road asphalt product is reasonable, the high and lowtemperature performances of the asphalt are enhanced, and the heat storage stability of the product is improved.

Description

technical field [0001] The invention belongs to the technical field of chemical industry, and mainly relates to a modifier mother liquid, road asphalt and a preparation method thereof, in particular to a preparation method of road asphalt produced from coal tar pitch and petroleum pitch as raw materials. Background technique [0002] With the continuous expansion of road construction scale, the market demand for road asphalt is also growing at a high speed. At present, oil resources are increasingly scarce, and the processing value of coal tar pitch (coal tar pitch) is low, and the market price is only about half of that of petroleum pitch. For this reason, researchers are constantly exploring whether coal tar pitch can be used as a raw material for the production of road pitch . Coal tar pitch produced by traditional methods has disadvantages such as poor heat sensitivity, easy aging, and poor ductility, which cannot meet the needs of road construction. Aiming at the shor...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L91/00C08L53/02C08L95/00C08K3/32
CPCC08L91/00C08L95/00C08L2201/08C08L2205/025C08L2205/035C08L53/02C08K2003/329
Inventor 徐青柏陈杰宁爱民李志军程国香
Owner CHINA PETROLEUM & CHEM CORP
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