Preparation method of tin ion enriched materials
A tin ion and enrichment technology, which is applied in the field of preparation of tin ion enrichment materials, can solve problems such as slow speed, and achieve the effects of large capacity, uniform adsorption effect and reasonable component distribution.
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Embodiment 1
[0031] Step 1. prepare detinning auxiliary unsaturated monomer combination liquid, each part represents 1Kg quality, and its composition is:
[0032] Component Parts by weight
[0033] Solvent oil 50 parts
[0034] 2-Aminobutenoic acid ethyl ester 3.5 parts 8
[0035] 1 part Ethoxymethyl cyanate ethyl ether
[0036] 1,5-di(p-hydroxy)-3-carbonyl-1,4-pentadiene 0.6 parts
[0037] Neopentyl glycol 2-cyano-3,3-diphenylacrylate 0.2 parts
[0038] 2,5-dimethoxy-4-ethylthio-β-nitrostyrene 0.05 parts
[0039] Step 2. prepare tin ion enrichment material, each represents 1Kg quality, and its composition is:
[0040] Component Parts by weight
[0041] ABS foam resin 30 parts
[0042] Acrylic 70 parts
[0043] Detinning auxiliary unsaturated monomer combination liquid 30 parts
[0044] Benzoyl peroxide 1.4 parts
[0045] 0.7 parts of gelatin
[0046] 450 parts of water
[0047] Polyethylene glycol 40 parts
[0048] Mix the following components evenly, raise the temperature to...
Embodiment 2
[0050] Step 1. prepare detinning auxiliary unsaturated monomer combination liquid, each part represents 1Kg quality, and its composition is:
[0051] Component Parts by weight
[0052] Solvent oil 50 parts
[0053] 2 parts of ethyl 2-aminobutyrate
[0054] Ethoxymethyl cyanate ethyl ether 0.5 parts
[0055] 0.3 parts of 1,5-di(p-hydroxy)-3-carbonyl-1,4-pentadiene
[0056] Neopentyl glycol 2-cyano-3,3-diphenylacrylate 0.1 parts
[0057] 2,5-dimethoxy-4-ethylthio-β-nitrostyrene 0.01 parts
[0058] Step 2. prepare tin ion enrichment material, each represents 1Kg quality, and its composition is:
[0059] Component Parts by weight
[0060] ABS foam resin 30 parts
[0061] Acrylic 70 parts
[0062] Detinning auxiliary unsaturated monomer combination liquid 20 parts
[0063] 1 part benzoyl peroxide
[0064] 0.4 parts of gelatin
[0065] 350 parts of water
[0066] Polyethylene glycol 30 parts
[0067] Mix the following components evenly, raise the temperature to 90° C., ...
Embodiment 3
[0069] Step 1. prepare detinning auxiliary unsaturated monomer combination liquid, each part represents 1Kg quality, and its composition is:
[0070] Component Parts by weight
[0071] Solvent oil 50 parts
[0072] 5 parts of ethyl 2-aminobutyrate
[0073] Ethoxymethylene cyanate ether 1.5 parts
[0074] 0.9 parts of 1,5-di(p-hydroxy)-3-carbonyl-1,4-pentadiene
[0075] Neopentyl glycol 2-cyano-3,3-diphenylacrylate 0.3 parts
[0076] 2,5-dimethoxy-4-ethylthio-β-nitrostyrene 0.1 parts
[0077] Step 2. prepare tin ion enrichment material, each represents 1Kg quality, and its composition is:
[0078] Component Parts by weight
[0079] ABS foam resin 30 parts
[0080] Acrylic 70 parts
[0081] Detinning auxiliary unsaturated monomer combination liquid 40 parts
[0082] Benzoyl peroxide 1.8 parts
[0083] 1 part gelatin
[0084] 550 parts of water
[0085] Polyethylene glycol 50 parts
[0086] Mix the following components evenly, raise the temperature to 10° C., and react...
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