Method for preparing dustproof carpet caring agent
A technology for a care agent and a carpet, applied in the field of preparation of a dust-proof carpet care agent, can solve the problems of carpet fiber corrosion, easy growth of fleas, mites, bacteria, etc., and achieves good spreading, good water and oil repellency, good Affinity effect
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[0024] A preparation method of a dustproof carpet care agent, comprising the steps of:
[0025] (1) Take allyl alcohol and perfluorooctanoic acid in a mass ratio of 5:2 and mix evenly. 2 Stirring for 30~40min under the protection of the mixture, adding H to the mixture at a mass ratio of 6:1 2 SO 4 Solution, heated up to 100~130°C, kept for 2~3h, cooled to room temperature, distilled to remove allyl alcohol, collected fractions at 95~98°C, obtained distillate, extracted, obtained extract;
[0026] (2) Take the extract and add tetrahydrofuran and hydrogen-containing silicone oil at a mass ratio of 8:4:3. 2 Stir for 30~45min under the protection of the catalyst, raise the temperature to 110~135℃ and keep for 2~4h, then add isopropanol and chloroplatinic acid according to the mass ratio of 1:50, react for 1~3h, cool down to room temperature, filter, take the filtrate, and distill off Tetrahydrofuran, to obtain distillate, add solvent laurane and solubilizer Tween-80 to the dis...
example 1
[0031] Pretreatment of lavender and dill seeds: Take the green peel and dill seeds according to the mass ratio of 1:1:9, add distilled water to soak for 2 hours, dry at 40°C, and crush through an 80-mesh sieve to obtain pretreated green peel particles and dill seed particles.
[0032]A preparation method of a dustproof carpet care agent, comprising the steps of:
[0033] (1) Take allyl alcohol and perfluorooctanoic acid in a mass ratio of 5:2 and mix evenly. 2 Stirring for 30min under the protection of the mixture, adding H 2 SO 4 Solution, heated up to 100°C, kept for 2h, cooled to room temperature, distilled off allyl alcohol, collected fractions at 95°C to obtain distillate, extracted to obtain extract;
[0034] (2) Take the extract and add tetrahydrofuran and hydrogen-containing silicone oil at a mass ratio of 8:4:3. 2 Stir for 30min under the protection of the environment, raise the temperature to 110°C and keep it for 2h, then add isopropanol and chloroplatinic acid a...
example 2
[0039] Pretreatment of lavender and dill seeds: take the green peel and dill seeds according to the mass ratio of 1:1:9, add distilled water to soak for 4 hours, dry at 50°C, and crush through an 80-mesh sieve to obtain pretreated green peel particles and dill seed particles.
[0040] A preparation method of a dustproof carpet care agent, comprising the steps of:
[0041] (1) Take allyl alcohol and perfluorooctanoic acid in a mass ratio of 5:2 and mix evenly. 2 Stirring for 40min under the protection of the mixture, adding H 2 SO 4 Solution, heated up to 130°C, kept for 3h, cooled to room temperature, distilled off allyl alcohol, collected fractions at 98°C to obtain distillate, extracted to obtain extract;
[0042] (2) Take the extract and add tetrahydrofuran and hydrogen-containing silicone oil at a mass ratio of 8:4:3. 2 Stir for 45min under the protection of 135°C, heat up to 135°C and keep for 4h, then add isopropanol and chloroplatinic acid at a mass ratio of 1:50, re...
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