One-pot liquefaction process of biomass

A biomass and biomass pretreatment technology, applied in the field of one-pot liquefaction of biomass, can solve the problems of high energy consumption, low amount of biomass transported by pumps, and unstable transportation, so as to achieve volume reduction and achieve stable Operation and transportation, to achieve the effect of smooth flow

Active Publication Date: 2018-06-29
BEIJING SJ ENVIRONMENTAL PROTECTION & NEW MATERIAL CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] Therefore, the technical problem to be solved by the present invention is to overcome the shortcomings of the existing biomass cracking catalytic process, such as the small amount of biomass transported by the pump, unstable transportation, and high energy consumption, and to provide a one-pot process for biomass Liquefaction process

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  • One-pot liquefaction process of biomass

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Experimental program
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Effect test

Embodiment 1

[0045] A one-pot liquefaction process of biomass, comprising the steps of:

[0046] Biomass Pretreatment

[0047] Put the palm oil residue into the drier and dry at 80°C for 5 hours until the water content is lower than 2wt%, and then send it into the superfine pulverizer for primary crushing. The median particle size after primary crushing is 100 μm, and then the primary crushing The palm oil residue is sent to the plodder for compression extrusion molding at a temperature of 50 °C and a pressure of 5 MPa, and then for secondary crushing. The median particle size after the secondary crushing is 30 μm. After the secondary crushing The bulk density of palm oil residue is 1600kg / m 3 ,spare.

[0048] Catalyst preparation

[0049] S1. After the biochar is acidified, a biochar carrier is obtained;

[0050] S2. Vibrating and grinding the oxide of Mo and the above-mentioned biomass carbon carrier to obtain the biomass carbon loaded with Mo oxide with a particle size of 400-500...

Embodiment 2

[0059] A one-pot liquefaction process of biomass, comprising the steps of:

[0060] Biomass Pretreatment

[0061] Send the linseed oil residue and peanut oil residue into a drier and dry at 110°C for 6 hours until the water content is lower than 2wt%, and then send them into an ultrafine pulverizer for primary crushing. The median particle size after primary crushing is 300 μm, and then The primary crushed linseed oil residue and peanut oil residue are sent to the plodder for compression extrusion molding at a temperature of 58°C and a pressure of 3MPa, and then secondary crushing is performed. The median particle size after the secondary crushing is 50 μm. The bulk density of linseed oil residue and peanut oil residue after secondary crushing is 1500kg / m 3 ,spare.

[0062] Catalyst preparation

[0063] S1. After the biochar is acidified, a biochar carrier is obtained;

[0064] S2. After the oxides of W, the oxides of Fe and the above-mentioned biomass charcoal carrier ...

Embodiment 3

[0073] A one-pot liquefaction process of biomass, comprising the steps of:

[0074] Biomass Pretreatment

[0075] Put saponin oil residue and rapeseed oil residue into a drier, dry at 100°C for 2 hours until the water content is lower than 2wt%, and then send it to an ultrafine pulverizer for primary crushing. The median particle size after primary crushing is 210 μm, Then the saponin oil residue and rapeseed oil residue after primary crushing are sent to a briquetting machine for compression extrusion molding at a temperature of 40°C and a pressure of 4MPa, and then secondary crushing is carried out. The particle size is 40 μm, and the bulk density of saponin oil residue and rapeseed oil residue after secondary crushing is 1561kg / m 3 ,spare.

[0076] Preparation of biochar loaded with Mo oxide and Pd oxide

[0077] S1. After the biochar is acidified, a biochar carrier is obtained;

[0078] S2. Vibrating and grinding Mo oxides, Pd oxides, and the above-mentioned biomass...

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Abstract

The invention relates to the field of biological energy sources, in particular to a one-pot liquefaction process of biomass. The process comprises the following steps: firstly, preparing slurry containing a catalyst, a vulcanizing agent and biomass, and then introducing hydrogen into the slurry for carrying out a reaction. The slurry is prepared by the steps of sequentially carrying out drying, primary crushing, compressing and secondary crushing on plant oil residue, and then mixing the product with the catalyst and the vulcanizing agent to obtain a mixture; adding the obtained mixture into an oil product, and grinding to prepare slurry, wherein the prepared slurry is biomass slurry with a plant oil residue concentration of 50-65wt%. According to the one-pot liquefaction process of the biomass, a treatment process of first compressing and then secondary crushing is carried out on the plant oil residue for the first time, so that the volume of the plant oil residue is greatly reduced,the plant oil residue is more easily dispersed in the oil product, the content of the plant oil residue in the oil product is increased, and the concentration of a reaction material is increased; theone-pot liquefaction process increases the biomass conveying capacity of a pump within unit time, and guarantees the smooth operation and transportation of the pump.

Description

technical field [0001] The invention relates to the technical field of bioenergy conversion, in particular to a one-pot liquefaction process of biomass. Background technique [0002] Coal, crude oil, natural gas, oil shale and other fossil non-renewable energy sources are becoming increasingly exhausted with the rapid development of social economy, and the CO produced after their combustion 2 , SO 2 , NO x The increasingly serious environmental pollution caused by such pollutants has forced human beings to seriously consider ways to obtain energy and methods to improve the environment. Biomass is a kind of renewable energy, which has huge potential and advantages in meeting energy demand, reducing environmental pollution, and improving energy structure. In a broad sense, biomass refers to all directly or indirectly available green plants formed by photosynthesis. Biomass in the narrow sense includes plant oil residues such as palm oil residues and plant straws such as ric...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10G1/06C10G1/08B01J23/28B01J23/34B01J23/755B01J23/888B01J23/89
CPCB01J23/28B01J23/34B01J23/755B01J23/888B01J23/8993C10G1/06C10G1/086
Inventor 林科李林郭立新
Owner BEIJING SJ ENVIRONMENTAL PROTECTION & NEW MATERIAL CO LTD
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