Flame-retardant type glue for mirror surface
A flame-retardant, raw material technology, applied in the direction of adhesives, adhesive additives, non-polymer adhesive additives, etc., can solve the problems of low bonding strength, fire, easy to burn, etc., to improve safety performance and not easy to fall off , good flame retardant effect
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Embodiment 1
[0024] Flame-retardant mirror glue, its raw material components include:
[0025]
[0026]
[0027] Its preparation method is:
[0028] Weigh the components of hydroxyl-terminated polydimethylsiloxane, silicone polysiloxane, dimethicone, talc, monoammonium phosphate, KH550 coupling agent, dioctyl phthalate, dibutyltin Dilaurate and ketoamine antioxidants;
[0029] Add hydroxyl-terminated polydimethylsiloxane, organosilicon polysiloxane and dimethyl silicone oil into the reaction kettle, turn on the stirrer, the stirring speed is 220r / min, and heat the reaction kettle at the same time, the heating rate is is 5°C, and the temperature rises to 55°C;
[0030] After stirring for 12 minutes, add dibutyltin dilaurate and KH550 coupling agent, adjust the stirring speed to 280r / min, and react for 20 minutes;
[0031] After the reaction time, stop heating, then add talcum powder, monoammonium phosphate, dioctyl phthalate and ketone amine antioxidant, and stir for 50 minutes to ...
Embodiment 2
[0035] Flame-retardant mirror glue, its raw material components include:
[0036]
[0037] Its preparation method is:
[0038] Weigh the components of polydimethylsiloxane, silicone polysiloxane, dimethyl silicone oil, graphite, diammonium phosphate, KH560 coupling agent, butyl benzyl phthalate, stannous octoate and ketamine class of antioxidants;
[0039] Add polydimethylsiloxane, organosilicon polysiloxane and dimethyl silicone oil into the reaction kettle, turn on the stirrer, the stirring speed is 210r / min, and heat the reaction kettle at the same time, the heating rate is 4°C , heating up to 67°C;
[0040] After stirring for 9 minutes, add stannous octoate and KH560 coupling agent, adjust the stirring speed to 270r / min, and react for 23 minutes;
[0041] After the reaction time, stop heating, then add graphite, diammonium phosphate, butyl benzyl phthalate and ketone amine antioxidants, stir for 76 minutes, and obtain the adhesive;
[0042] The adhesive is passed th...
Embodiment 3
[0045] Flame-retardant mirror glue, its raw material components include:
[0046]
[0047] Its preparation method is:
[0048] Weigh the components of polyhydroxy-terminated polydimethylsiloxane, silicone polysiloxane, dimethyl silicone oil, carbon black, ammonium chloride, KH570 coupling agent, dibutyl phthalate, dimethicone (Lauryl sulfide) dibutyl tin and antioxidant;
[0049] Add polyhydroxy-terminated polydimethylsiloxane, silicone polysiloxane and dimethyl silicone oil into the reaction kettle, turn on the stirrer, the stirring speed is 160r / min, and heat the reaction kettle at the same time, The rate is 3°C, and the temperature rises to 70°C;
[0050] After stirring for 8 minutes, add dibutyltin di(dodecylsulfide) and KH570 coupling agent, adjust the stirring speed to 240r / min, and react for 30 minutes;
[0051] After the reaction time, stop heating, then add carbon black, ammonium chloride, dibutyl phthalate and antioxidant, after stirring for 80min, obtain adhes...
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