Fast curing EMI heat-conducting and conductive material and preparation method thereof
A conductive material and rapid curing technology, applied in the field of shielding materials, can solve the problems of poor shielding effect, difficult manufacturing process, and low reproducibility, and achieve good electrical and thermal conductivity, excellent curing performance, and high reproducibility Effect
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Embodiment 1
[0025] The present invention proposes a fast-curing EMI thermally and electrically conductive material, comprising the following raw materials in parts by weight: 70 parts of bisphenol A epoxy resin, 15 parts of butadiene-styrene copolymer, 0.4 part of trimethylolpropane, 4, 1.2 parts of 4′-diphenylmethane diisocyanate, 1.2 parts of xylene diisocyanate, 1 part of dibutyltin dilaurate, 1 part of azobisisobutyronitrile, 4 parts of composite alloy powder, bisphenol A epoxy resin diluted 50 doses;
[0026] Its preparation method comprises the following steps:
[0027] S1. Preparation of composite alloy powder: Add copper powder and iron-based alloy powder into the ball mill according to the mass ratio of 1:3, and add 2 times the mass of grinding body and 1 times the mass of ethanol for ball milling for 6 hours, and then Dried to obtain composite alloy powder for subsequent use;
[0028] S2. According to 70 parts of bisphenol A epoxy resin, 15 parts of butadiene-styrene copolymer...
Embodiment 2
[0032] The present invention proposes a fast-curing EMI thermally and electrically conductive material, comprising the following raw materials in parts by weight: 80 parts of bisphenol A epoxy resin, 20 parts of butadiene-styrene copolymer, 0.6 part of trimethylolpropane, 4, 1.5 parts of 4′-diphenylmethane diisocyanate, 1.5 parts of xylene diisocyanate, 0.5 parts of dibutyltin dilaurate, 0.5 parts of azobisisobutyronitrile, 6 parts of composite alloy powder, diluted with bisphenol A epoxy resin 40 doses;
[0033] Its preparation method comprises the following steps:
[0034] S1. Preparation of composite alloy powder: Add copper powder and iron-based alloy powder into the ball mill according to the mass ratio of 1:4, and add 3 times the mass of grinding body and 0.5 times the mass of ethanol for ball milling for 5 hours, and then Dried to obtain composite alloy powder for subsequent use;
[0035] S2. According to 80 parts of bisphenol A epoxy resin, 20 parts of butadiene-styren...
Embodiment 3
[0039] The present invention proposes a fast-curing EMI thermally and electrically conductive material, comprising the following raw materials in parts by weight: 60 parts of bisphenol A epoxy resin, 10 parts of butadiene-styrene copolymer, 0.2 part of trimethylolpropane, 4, 1 part of 4'-diphenylmethane diisocyanate, 1 part of xylene diisocyanate, 1.5 parts of dibutyltin dilaurate, 1.5 parts of azobisisobutyronitrile, 3 parts of composite alloy powder, diluted with bisphenol A epoxy resin 60 doses;
[0040] Its preparation method comprises the following steps:
[0041] S1. Preparation of composite alloy powder: Add copper powder and iron-based alloy powder into the ball mill according to the mass ratio of 1:2, and add 2 times the mass of grinding body and 1 times the mass of ethanol for ball milling for 8 hours, and then Dried to obtain composite alloy powder for subsequent use;
[0042] S2. According to 60 parts of bisphenol A epoxy resin, 10 parts of butadiene-styrene copo...
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