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Medium-plasticity high energy absorption magnesium alloy and deeply cold-bending tubular product preparation device and method

A magnesium alloy and intermediate alloy technology, applied in the direction of metal extrusion dies, etc., can solve the problems of poor secondary processing formability, small-diameter thin-walled tubes that cannot maintain the uniformity of the hole diameter at the bending deformation, and achieve reduced extrusion force and good Deep cold formability, low cost effect

Active Publication Date: 2018-08-03
NORTHEASTERN UNIV LIAONING
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0007] Aiming at the current problems of magnesium alloys and their pipes, and overcoming the poor formability of secondary processing of existing magnesium alloy pipes, the small-diameter thin-walled pipes cannot maintain the uniformity of the aperture at the bending deformation without adding a mandrel, and the like. The present invention provides a medium A plastic high-energy-absorbing magnesium alloy and a deep cold-bending pipe preparation device and method, the method provides a high-energy-absorbing magnesium alloy with medium plasticity, and provides a deep cold-bending pipe corresponding to the magnesium alloy Preparation device and method

Method used

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  • Medium-plasticity high energy absorption magnesium alloy and deeply cold-bending tubular product preparation device and method
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  • Medium-plasticity high energy absorption magnesium alloy and deeply cold-bending tubular product preparation device and method

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Embodiment 1

[0061] A kind of high energy-absorbing magnesium alloy, which is Mg-Zn-Ce-La-Mn-Zr-Ca series magnesium alloy; its composition contains by mass percentage: Zn: 1.5%, Ce: 0.4%, La: 0.2%, Mn: 0.5%, Zr: 0.2%, Ca: 0.2%, the balance is Mg and impurities; among them, in terms of mass percentage, Ce:La=2:1, Mn:Zr=2.5:1, and Fe<0.003% as impurities.

[0062] The preparation method of the deep cold-formed high-energy-absorbing magnesium alloy pipe of this embodiment specifically includes the following steps:

[0063] Step 1, Smelting:

[0064] (1) The magnesium metal is heated to 730℃ under the protection of No. 5 flux, calculated according to the ratio of medium plasticity and high energy absorption magnesium alloy, first add Zn, after all Zn is melted, add Mg-Zr master alloy and MnCl 2 Particles

[0065] (2) After cooling the melt to 710℃, add Mg-Ca master alloy, Mg-Ce master alloy and Mg-La master alloy according to the ratio of medium plasticity and high energy absorption magnesium alloy, a...

Embodiment 2

[0078] A high-energy-absorbing magnesium alloy, which is Mg-Zn-Ce-La-Mn-Zr-Ca series magnesium alloy; its composition contains by mass percentage: Zn: 2.2%, Ce: 0.7%, La: 0.1%, Mn: 0.3%, Zr: 0.06%, Ca: 0.3%, the balance is Mg and impurities; among them, according to mass percentage, Ce:La=7:1, Mn:Zr=5:1, and Fe<0.003%.

[0079] The preparation method of the deep cold-formed high-energy-absorbing magnesium alloy pipe of this embodiment specifically includes the following steps:

[0080] Step 1, Smelting:

[0081] (1) The magnesium metal is heated to 730℃ under the protection of No. 5 flux, calculated according to the ratio of medium plasticity and high energy absorption magnesium alloy, first add Zn, after all Zn is melted, add Mg-Zr master alloy and MnCl 2 Particles

[0082] (2) After cooling the melt to 710℃, add Mg-Ca master alloy, Mg-Ce master alloy and Mg-La master alloy according to the ratio of medium plasticity and high energy absorption magnesium alloy, among which: Mg-Ca mast...

Embodiment 3

[0095] A high-energy-absorbing magnesium alloy, which is Mg-Zn-Ce-La-Mn-Zr-Ca series magnesium alloy; its composition contains by mass percentage: Zn: 1.7%, Ce: 0.4%, La: 0.2%, Mn: 0.4%, Zr: 0.1%, Ca: 0.2%, the balance is Mg and impurities; among them, in terms of mass percentage, Ce:La=2:1, Mn:Zr=4:1, and Fe<0.003% as impurities.

[0096] The preparation method of the deep cold-formed high-energy-absorbing magnesium alloy pipe of this embodiment specifically includes the following steps:

[0097] Step 1, Smelting:

[0098] (1) The magnesium metal is heated to 730℃ under the protection of No. 5 flux, calculated according to the ratio of medium plasticity and high energy absorption magnesium alloy, first add Zn, after all Zn is melted, add Mg-Zr master alloy and MnCl 2 Particles

[0099] (2) After cooling the melt to 710℃, add Mg-Ca master alloy, Mg-Ce master alloy and Mg-La master alloy according to the ratio of medium plasticity and high energy absorption magnesium alloy, among which...

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Abstract

The invention discloses medium-plasticity high energy absorption magnesium alloy and a deeply cold-bending tubular product preparation device and method and belongs to the technical field of metallicmaterial technology and metallurgy. The medium-plasticity high energy absorption magnesium alloy comprises the following components in percent by mass: 1.5%-2.2% of Zn, 0.2%-0.7% of Ce, 0.1%-0.2% of La, 0.3%-0.9% of Mn, 0.06%-0.6% of Zr, 0.1%-0.3% of Ca and the balance of Mg and impurities, wherein the mass ratio of Ce to La is (2-7):1; the mass ratio of Mn to Zr is (1.5-5):1; and the mass percentof the impurity Fe is less than 0.003%. The deeply cold-bending tubular product preparation device comprises a hollow extruding rod, a flow distribution extruding upper die, a flow distribution extruding lower die, an extruding cylinder, an extruding gasket and a turbocharging cooling system. The magnesium alloy tubular product preparation method comprises the following steps: 1, smelting the rawmaterial and carrying out purification treatment on the melt; 2, lowering the temperature of the melt to 680-700 DEG C and then carrying out semicontinuous casting; and 3, carrying out flow distribution extrusion on a magnesium alloy bar subjected to homogenization treatment and pretreatment to obtain a deeply cold-bending high energy absorption magnesium alloy tubular product.

Description

Technical field [0001] The invention belongs to the field of metal material technology and metallurgical technology, and specifically relates to a device and method for preparing a medium-plasticity high-energy-absorbing magnesium alloy and a pipe capable of deep cold bending. Background technique [0002] Magnesium alloy has the advantages of low density, high specific strength, excellent vibration damping, electromagnetic shielding and machining performance. It is an ideal material for lightweight structure. Magnesium alloy extrusion pipe is an important bulk product form for the production of wrought magnesium alloy structural parts. It can be widely used in civilian fields such as bicycles, wheelchairs, beach chairs, outdoor furniture, sports equipment, etc., and can also be widely used in aerospace and military industries. However, in the production of pipe members, secondary plastic forming processes such as bending and diameter reduction (diameter expansion or reduction) o...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C23/04C22C1/03C22F1/06B22D11/00B21C37/06B21C25/02B21C29/00
Inventor 乐启炽胡克李春雨赵大志贾永辉宝磊
Owner NORTHEASTERN UNIV LIAONING