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415results about How to "Improve detergency" patented technology

Technological process for producing high concentration nitric-phosphate fertilizer

The invention discloses a technique method for producing high-concentration nitric phosphate, which comprises the following steps of: adding nitric acid into phosphorus ore for acidolysis, depositing and separating acid non-soluble substance, freezing and crystallizing calcium nitrate, filtering the calcium nitrate, neutralizing the mother liquid, vaporization, pelleting and drying. The invention is characterized in that: a step of thoroughly removing the calcium of the mother liquid is arranged between the steps of filtering the calcium nitrate, and neutralizing the mother liquid. The steps comprise the following steps of: I) thoroughly removing the calcium of the mother liquid and adding sulfuric acid or ammonium sulfate; the calcium ions and the sulfate ions in the mother liquid generate dihydrate calcium sulfate crystal; II) the grading processing of reaction slurry: employing a grading device to carry out grading processing to the reaction slurry; returning the reaction slurry provided with small grain calcium sulfate to the mother liquid for thoroughly removing the calcium, and feeding the reaction slurry provided with large grain calcium sulfate to the calcium sulfate for filtering; and III) filtering and washing the filtering reaction slurry of calcium sulfate by a filter, feeding the primary filtrate and the primary lavage fluid into the working procedure of neutralizing, and returning the secondary lavage fluid to the filter. The invention has the advantage of using middle-low quality phosphorite to prepare the high-concentration nitric phosphate.
Owner:TIANJI COAL CHEM IND GROUP +1

Method for preparing high-alkali value (TBN400) synthesized calcium alkyl benzene sulfonate

The invention provides a method for preparing high base number (TBN400) synthetic calcium alkyl-benzene sulfonate. The method comprises the following steps of: adopting a mixed acid of long-chain linear alkyl-benzene sulfonic acid and high-boiling heavy alkyl-benzene sulfonic acid, calcium oxide and/or calcium hydroxide, low-carbon alcohol, alkaline-earth metal halide or nitrate, and a mixture of alkaline-earth metal alkylphenol or alkaline-earth metal alkylphenate and polyisobutylene succinic anhydride for a neutralization reaction in the presence of a solvent and cutback oil at a temperature of between 40 and 80 DEG C; then, passing through carbon dioxide to a product of the neutralization reaction at a temperature of between 40 and 60 DEG C for a carbonation reaction; and producing high base synthetic alkyl-benzene sulfonate with a total base number (TBN) of 400mgKOH/g by adopting a process of a one-step method. The product is divided into high-base number (TBN400) synthetic alkyl-benzene sulfonate containing chlorine and high-base number (TBN400) synthetic alkyl-benzene sulfonate without the chlorine. The product produced by adopting the method with low viscosity, small turbidity, easy filtration, light color and no skin formation has the advantages of excellent high-temperature detergency, excellent anti-foaming property and excellent heat storage stability.
Owner:JINZHOU DPF TH CHEM CO LTD

High basic value (TBN400) sulfurized calcium alkyl and preparation method thereof

The invention relates to high base number (TBN400) vulcanized alkyl phenol calcium and a preparation method thereof. The vulcanized alkyl phenol calcium has a chemical structure as right. The preparation method is as follows: in a system containing solvent and diluent oil, alkyl phenol compound, shielded phenol compound, calcium oxide and / or calcium hydroxide and sulfur are subjected to sulfonation / neutralization reaction at a temperature of between 60 and 180 DEG C to generate phenolate intermediate; balanced calcium oxide and / or calcium hydroxide are added into the mixture, carbon dioxide is introduced, and the mixture is subjected to carbonation reaction; and alkyl polylol is added into the mixture at the sulfonation / neutralization reaction or respectively at the sulfonation / neutralization reaction and the carbonation reaction to participate in the reaction, long-chain carboxylic acid is added into the mixture at the sulfonation / neutralization reaction or respectively at the sulfonation / neutralization reaction and the carbonation reaction to participate in the reaction, and products are obtained through refining. The vulcanized alkyl phenol calcium has the characteristics of high base number, low viscosity, low precipitation number, good heat storage stability, and the like, and has excellent combination property, does not cause environmental protection problem during use, and belongs to an environment-friendly product, and adopts a one-stage process, has mild reaction conditions, and is easy to filter.
Owner:JINZHOU DPF TH CHEM CO LTD

Rolling oil composition for 12-roller reversing mill

The invention relates to a rolling oil composition used for a twelve-high reversing cluster mill; the rolling oil composition belongs to the field of metallurgical steel rolling oil products, and comprises the components according to weight percent as follows: 60-70 percent of compound neopentyl polyol ester, 14-28 percent of mineral oil, 1-5 percent of phosphorus-containing extreme-pressure and anti-wear agent, 1-5 percent of sulfur-containing extreme-pressure and anti-wear agent, 2-12 percent of compound emulsifier, 1-3 percent of anti-rust agent, 1-3 percent of antioxidant and 0.01-0.5 percent of defoamer; the rolling oil composition takes the compound neopentyl polyol ester synthetic ester with excellent lubricating performance as the lubricating basic component; an oiliness agent main body with high lubricating performance and high extreme-pressure and anti-wear performance is composed by adding the scientific components of the phosphorus-containing and the sulfur-containing extreme-pressure and anti-wear agents; and the anti-rust performance and the emulsion stability are ensured by adopting the mineral oil, the anti-rust oil, the emulsifier and the antioxidant with the appropriate proportion for coordination, thereby creatively solving the contradiction between the lubricating performance and the detergence, ensuring the requirements on the lubricating performance of the quality when rolling steel plates with thin specifications, protecting the lubricating requirements of back-up bearings and ensuring the volatility and the annealing detergence under the cleaning-free condition.
Owner:WUHAN TONGSHENG FINE CHEM TECH DEV
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