Novel reverse osmosis membrane and preparation method thereof
A reverse osmosis membrane, a new type of technology, applied in reverse osmosis, semi-permeable membrane separation, chemical instruments and methods, etc., can solve problems such as short service life, chlorine oxidation, flux and desalination rate limitations, etc.
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Embodiment 1
[0108] (1) Configuration solution 1: add to the stirrer and account for each component of following mass fraction: the dimethyl sulfoxide of 75%, the polyaryl sulfone of 20% and the ethylene glycol of 5%, under the vacuum of 10mbar Stir at a speed of 200r / min for 24 hours to obtain solution 1;
[0109] (2) Scrape coating support layer: cast solution 1 on the surface of the non-woven fabric, scrape off the solution layer on both sides of the non-woven fabric with a scraper, and then form a support on the surface of the non-woven fabric through gel phase inversion in a 10°C cold water bath layer, and then formed by pretreatment with hot water at 90°C to form a support layer with a thickness of 120 μm to obtain a film containing the support layer;
[0110] (3) Configure solution 2: add water and triethylamine to the agitator, stir evenly at a speed of 200r / min, then add m-phenylenediamine, continue stirring at the original speed until completely dissolved, and obtain solution 2; ...
Embodiment 2
[0119] (1) Configuration solution 1: add to the stirrer and account for each component of following mass fraction: the dimethyl sulfoxide of 75%, the polyaryl sulfone of 20% and the ethylene glycol of 5%, under the vacuum of 10mbar Stirring at a speed of 200r / min and vacuum stirring for 24 hours to obtain solution 1;
[0120] (2) Scrape coating support layer: cast solution 1 on the surface of the non-woven fabric, scrape off the solution layer on both sides of the non-woven fabric with a scraper, and then form a support on the surface of the non-woven fabric through gel phase inversion in a 10°C cold water bath layer, and then formed by pretreatment with hot water at 90°C to form a support layer with a thickness of 120 μm to obtain a film containing the support layer;
[0121] (3) Configure solution 2: add water and triethylamine to the agitator, stir evenly at a speed of 200r / min, then add m-phenylenediamine, continue stirring at the original speed until completely dissolved,...
Embodiment 3
[0130] (1) Configuration solution 1: add to the stirrer and account for each component of following mass fraction: the dimethyl sulfoxide of 75%, the polyaryl sulfone of 20% and the ethylene glycol of 5%, under the vacuum of 10mbar Stirring at a speed of 200r / min and vacuum stirring for 24 hours to obtain solution 1;
[0131] (2) Scrape coating support layer: cast solution 1 on the surface of the non-woven fabric, scrape off the solution layer on both sides of the non-woven fabric with a scraper, and then form a support on the surface of the non-woven fabric through gel phase inversion in a 10°C cold water bath layer, and then formed by pretreatment with hot water at 90°C to form a support layer with a thickness of 120 μm to obtain a film containing the support layer;
[0132] (3) Configure solution 2: add water and triethylamine to the agitator, stir evenly at a speed of 200r / min, then add m-phenylenediamine, continue to stir at the original speed until completely dissolved, ...
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