Method for producing nano zinc oxide by utilizing zinc-containing raw ore
A nano-zinc oxide and raw ore technology, which is applied in the direction of zinc oxide/zinc hydroxide, nanotechnology, etc., can solve the problems of poor comprehensive economic benefits, inability to handle, unsatisfactory leaching rate, etc., and achieve process recovery rate and high-quality goods grade problems, realize economic and environmental protection utilization, and avoid the effect of water treatment pressure
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Embodiment 1
[0125] In a zinc mine in Yunnan, the zinc content is 5.6%, and the oxidation rate of the raw ore is 96.3%. The main form of zinc in this mine is zinc carbonate.
[0126] Get 300 grams of zinc-containing raw ore, put into 900 milliliters of ammonia-ammonium bicarbonate mixed solution (10% of total ammonia mass concentration, 3% of carbonate root mass concentration) and carry out stirring and leaching, the leaching temperature is normal temperature, and the stirring time is 2 hours, Then filter, the filtered liquid contains 1.632% zinc (in zinc oxide equivalent), and the carbonate mass concentration in the liquid is 4.23%, and the increased part is brought in by the zinc carbonate in the raw ore. According to the test data, the recovery rate of soluble zinc in the raw ore during the leaching process is 90.79%, and the recovery rate of total zinc is 87.43%.
[0127] The filtered leachate containing zinc ammonium ions is purified.
[0128] Take 600 ml of purified leaching solutio...
Embodiment 2
[0133] In a zinc mine in Chongqing, the zinc content is 4.7%, and the oxidation rate of the raw ore is 95.52%. The main form of zinc in this mine is zinc silicate.
[0134] Get 300 grams of zinc oxide raw ore, put into 900 milliliters of ammonia-ammonium bicarbonate mixed solution (10% of total ammonia mass concentration, 3% of carbonate root mass concentration) and carry out stirring and leaching, leaching temperature is normal temperature, stirring time is 2 hours, Then filter, after filtering, the zinc oxide in the liquid is 1.367%, the mass concentration of carbonate in the liquid is 3.54%, and the increased part is brought in by the zinc carbonate in the raw ore. According to the test data, the recovery rate of soluble zinc in the raw ore during the leaching process is 91.53%, and the recovery rate of total zinc is 87.26%.
[0135] The filtered leachate containing zinc ammonium ions is purified.
[0136] Take 600 ml of purified leaching solution, add 12.18 g of calcium o...
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