High Adhesion Primer Coatings
A high-adhesion, primer technology, used in primers, polyester coatings, coatings, etc., can solve the problem that coatings cannot be sprayed with other types of coatings
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[0033] Preferably, the preparation method of hyperbranched modified polyester resin comprises the following steps:
[0034] S1, trimethylolpropane and 2,2-dimethylolpropionic acid monomer react under the action of a catalyst to obtain aliphatic hyperbranched polyester;
[0035] S2, the terminal graft anhydride of the aliphatic hyperbranched polyester obtained in step S1, obtain the hyperbranched polyester containing terminal carboxyl group;
[0036] S3. Add carboxylamine heterocyclic alcohol to the hyperbranched polyester containing carboxyl-terminated polyester obtained in step S2, and obtain a hyperbranched modified polyester resin through esterification.
[0037] The above method for preparing the hyperbranched modified polyester resin has mild reaction conditions, few reaction steps, short preparation time, and the obtained hyperbranched modified polyester resin has high purity. In the above preparation method, the carbon amine heterocyclic alcohol can be 1-(2-hydroxyethy...
Embodiment 1
[0048] In the present embodiment, the preparation method of hyperbranched modified polyester resin is as follows:
[0049] S1. Trimethylolpropane and 2,2-dimethylolpropionic acid monomers with a molar ratio of 1:1 were used as raw materials, and p-toluenesulfonic acid was used as a catalyst to react at 150°C for 5 hours to obtain aliphatic hyperbranched polyester ;
[0050] S2, grafting succinic anhydride at the end of the above-mentioned aliphatic hyperbranched polyester, the molar ratio of the raw materials is 1: 12, the reaction temperature is 90 ° C, DMF is used as a solvent, and the progress of the reaction is confirmed by acid value titration. When the acid value Stop reaction when being half of the initial value, obtain the hyperbranched polyester containing terminal carboxyl group;
[0051] S3, using the above-mentioned hyperbranched polyester containing carboxyl groups as raw materials, add 1-(2-hydroxyethyl)-4-methyl-2-imidazolidinone, the molar ratio of the two is ...
Embodiment 2
[0066] In the present embodiment, the high adhesion primer paint comprises the following components in parts by weight: 50 parts by weight of modified weak hydroxyl acrylic resin, 30 parts by weight of hyperbranched modified polyester resin prepared in Example 1, 2 parts by weight Parts of fumed silica, 30 parts by weight of diacetone alcohol. The above coatings are transparent high adhesion primer coatings.
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