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Method for preparing alloy-ceramic lamellar coating through atmospheric plasma spraying

An alloy ceramic and plasma technology, which is applied in metal material coating process, coating, melting spray plating, etc., can solve the problems that powder cannot be fully mixed, cannot be mass-produced, destroy original powder, etc., and achieve high temperature corrosion resistance. Excellent, the effect of improving high temperature wear resistance and corrosion resistance, high fracture toughness

Inactive Publication Date: 2018-11-23
扬州睿德石油机械有限公司 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The traditional atmospheric plasma spraying alloy-ceramic composite coating technology is to pre-mix the alloy powder and ceramic powder by ball milling. Practice shows that when the density or particle size of the alloy powder and ceramic powder is greatly different, the two powders cannot be fully mixed together. The original powder will be destroyed during the ball milling process, and the powder waste is serious during spraying
Another method is to use agglomerated powder, although the spraying effect is better, but the cost is high, and it cannot be used for mass production

Method used

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  • Method for preparing alloy-ceramic lamellar coating through atmospheric plasma spraying
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  • Method for preparing alloy-ceramic lamellar coating through atmospheric plasma spraying

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0046] 1. Use acetone to ultrasonically clean the surface of the substrate to be sprayed, and then place it in an oven at 80-100°C for 2 hours.

[0047] 2. Use brown corundum with a particle size of 20 mesh to carry out sandblasting roughening treatment on the surface of the substrate to be sprayed, so that many tiny pits appear on the surface of the substrate, and the surface roughness of the roughened substrate is not lower than Ra7.0.

[0048] 3. Weigh 2000 g of NiCrBSi powder with a particle size range of -75~+40 μm, and the weight percentage of each component is: 15~20% chromium, 3~4.5% boron, 3.5~5.5% silicon, and 0.5~1.1% carbon , iron <5%, and the balance is nickel. 2000 g of YSZ powder with a particle size ranging from -53 to +15 μm was placed in an oven at 80 to 100 °C for 2 h to ensure good fluidity of the powder during the spraying process.

[0049] 4. The alloy powder and ceramic powder are fed into the plasma arc at the same time by means of two-way powder feedi...

Embodiment 2

[0056] The difference between this embodiment and Embodiment 1 is that in step 5, the powder feeding rate of the metal powder feeder 1 is 29.8 g / min, and the powder feeding amount of the ceramic powder feeder 2 is 3.4 g / min. Adjust the plasma spraying process current to 517 A, voltage to 58 V, flow of plasma generating gas Ar to 50 L / min, H 2 The flow rate is 8 L / min, the spraying distance is 120 mm, the gun translation speed is 300 mm / s, the gun translation distance is 3 mm, the number of spraying repetitions is 5, and the cooling method is 0.3 Mpa air cooling.

[0057] Hardness test was done on the prepared NiCrBSi-YSZ coating, coating hardness HV 0.1 The Vickers hardness can reach 742.

[0058] The reciprocating friction and wear test was carried out on the prepared coating, in which the load was 20 N, the frequency was 4 Hz, the wear scar length was 8 mm, the duration was 1 h, and the total sliding distance was 72 m. The wear rate of the sprayed NiCrBSi-YSZ coating was 4....

Embodiment 3

[0060] The difference between this embodiment and Embodiment 1 is that in step 5, the powder feeding rate of the metal powder feeder 1 is 29.8 g / min, and the powder feeding amount of the ceramic powder feeder 2 is 8.2 g / min. Adjust the plasma spraying process current to 517 A, voltage to 58 V, flow of plasma generating gas Ar to 50 L / min, H 2 The flow rate is 8 L / min, the spraying distance is 120 mm, the gun translation speed is 300 mm / s, the gun translation distance is 3 mm, the number of spraying repetitions is 5, and the cooling method is 0.3 Mpa air cooling.

[0061] Hardness test was done on the prepared NiCrBSi-YSZ coating, coating hardness HV 0.1 The Vickers hardness can reach 754.

[0062] The reciprocating friction and wear test was carried out on the prepared coating, in which the load was 20 N, the frequency was 4 Hz, the wear scar length was 8 mm, the duration was 1 h, and the total sliding distance was 72 m. The wear rate of the sprayed NiCrBSi-YSZ coating was 4....

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Abstract

The invention relates to a method for preparing an alloy-ceramic lamellar coating through atmospheric plasma spraying. The atmospheric plasma spraying manner is adopted for directly spraying alloy andceramic powder to the surface of a matrix, and the high-temperature wear-resisting and anti-corrosion coating is prepared. The method is simple in process and low in cost, the problems that the ceramic coating is large in brittleness and insufficient in toughness are effectively solved, and the service life of the coating is longer.

Description

technical field [0001] The invention relates to the technical field of surface coatings, in particular to a method for preparing an alloy-ceramic layered coating by atmospheric plasma spraying. Background technique [0002] With the rapid development of modern industrial technology, high-temperature equipment is widely used in metallurgy, chemical industry, energy, military and other fields, especially in high-temperature, high-pressure and complex corrosive media. If the anti-corrosion problem of these equipment is not solved, it will not only cause Huge economic losses will also bring many hidden dangers to safe production. Therefore, doing a good job of high-temperature anti-corrosion work on equipment can not only ensure safe production, but also prolong the service life of equipment and save money. The alloy-ceramic layered coating prepared by the invention has good high temperature corrosion resistance, can protect the substrate from wear and corrosion under high tempe...

Claims

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Application Information

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IPC IPC(8): C23C4/134C23C4/06
CPCC23C4/06C23C4/134
Inventor 张超黄博任永先肖金坤
Owner 扬州睿德石油机械有限公司