High barrier polyethylene film and preparation method thereof
A polyethylene film, high barrier technology, applied in the field of polyethylene film, can solve the problems of difficult film process, poor water resistance, difficult to control the amount of paint, etc., to achieve the effect of reducing operation difficulty and production cost
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Embodiment 1
[0022] Embodiment 1: Preparation 1 of filling
[0023] The filling preparation steps of the present embodiment are as follows:
[0024] Weigh raw materials according to the following mass percentages: 10% of 304 stainless steel powder, 15% of nano-titanium, 20% of silver nitrate, 5% of urea, 0.2% of polyvinylpyrrolidone, 0.2% of ammonium carbamate, 30% of Aqua, 10% of 50wt% nitric acid solution, 304 stainless steel powder with a particle size of 80nm, and nano-titanium with a particle size of 15nm;
[0025] Prepare urea into a saturated urea aqueous solution, then add nano-grade 304 stainless steel, heat to 40°C, keep warm for 20 minutes, take out, filter and wash, then add to 50wt% nitric acid solution, soak at 90°C for 10 hours, take out, brush and wash Clean, obtain pretreated nano-scale 304 stainless steel, stand-by;
[0026] Add silver nitrate into the ethanol solution to prepare a 30wt% silver nitrate ethanol solution, add polyvinylpyrrolidone and stir evenly, then add...
Embodiment 2
[0027] Embodiment 2: the preparation two of filler
[0028] The filling preparation steps of the present embodiment are as follows:
[0029] Weigh the raw materials according to the following mass percentages: 8% 304 stainless steel powder, 13% nano-titanium, 18% silver nitrate, 3% urea, 0.2% polyvinylpyrrolidone, 0.2% ammonium carbamate, 25% sulfuric acid Aqueous solution, 10% 55wt% nitric acid solution, 304 stainless steel powder with a particle size of 60nm, and nano-titanium with a particle size of 12nm;
[0030] Prepare urea into a saturated urea aqueous solution, then add nano-grade 304 stainless steel, heat to 40°C, keep warm for 20 minutes, take out, filter and wash, then add to 55wt% nitric acid solution, soak at 90°C for 13 hours, take out, brush and wash Clean, obtain pretreated nano-scale 304 stainless steel, stand-by;
[0031] Add silver nitrate into the ethanol solution to prepare a 20wt% silver nitrate ethanol solution, add polyvinylpyrrolidone and stir evenly...
Embodiment 3
[0032] Embodiment 3: the preparation three of filler
[0033]The filling preparation steps of the present embodiment are as follows:
[0034] Weigh the raw materials according to the following mass percentages: 9% 304 stainless steel powder, 15% nano-titanium, 20% silver nitrate, 4% urea, 0.2% polyvinylpyrrolidone, 0.2% ammonium carbamate, 20% sulfuric acid Aqua, 9% of 55wt% nitric acid solution, 304 stainless steel powder with a particle size of 50nm, and nano-titanium with a particle size of 10nm;
[0035] Prepare urea into a saturated urea aqueous solution, then add nano-grade 304 stainless steel, heat to 50°C, keep warm for 20 minutes, take out, filter and wash, then add to 60wt% nitric acid solution, soak at 90°C for 16 hours, take out, brush and wash Clean, obtain pretreated nano-scale 304 stainless steel, stand-by;
[0036] Add silver nitrate into the ethanol solution to prepare a 10wt% silver nitrate ethanol solution, add polyvinylpyrrolidone and stir evenly, then ad...
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