A kind of preparation method of reconstituted tobacco leaf coating liquid

A technology for reconstituted tobacco leaves and coating solution, which is applied in the preparation of tobacco, tobacco, and tobacco treatment, etc. It can solve the problems of affecting the application effect of coating solution, insufficient fragrance of coating solution, single aroma of coating solution, etc., and achieve good physical Adsorption performance and stability, improvement of fine fiber retention rate, low cost effect

Active Publication Date: 2021-08-03
HUBEI CHINA TOBACCO IND
View PDF26 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This method only performs a simple Maillard reaction on the extract, and the resulting coating solution has insufficient aroma and is insufficient in improving the aroma of cigarettes; the invention patent (application number: 201711070249.X) is to combine stem paste, The leaf paste and tobacco flavors and fragrances are blended in a mass ratio of 30:65:5 to make a coating liquid with a solid content of 40%-46%, and the stem paste and leaf paste are blended in a mass ratio of 25:75 to make a solid content of 20%-35% % spray liquid, or use a single leaf paste or a single stem paste to prepare a spray liquid with a solid content of 20%-35%
This method only mixes different pastes or flavors and fragrances, and does not use physical or chemical methods to treat the extract itself. The obtained coating liquid has a relatively single aroma and poor application effect; the invention patent (application number: 201510332704.3 ) is to add yeast and protease to the tobacco extract to ferment, then concentrate alcohol and alcohol into a clear paste, add hot water, reducing sugar, amino acid, and carry out Maillard reaction
Although this method decomposes the macromolecules in the extract by adding yeast and protease, the above strains and enzymes can only process part of the macromolecules, which affects the application effect of the coating solution to a certain extent.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • A kind of preparation method of reconstituted tobacco leaf coating liquid

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] A kind of preparation method of reconstituted tobacco leaf coating liquid provided in embodiment 1 is characterized in that concrete steps comprise:

[0022] (1) Add 15 times of tap water to the mixture of tobacco stems, tobacco powder and secondary tobacco leaves, and after mixing evenly, conduct dynamic countercurrent extraction at 40°C for 1.2 hours, and obtain insoluble slurry and extract after the extraction is completed;

[0023] (2) Utilize the 300nm aperture inorganic ceramic filter membrane to filter the extract to obtain filtrate A and retentate A;

[0024] (3) Use potassium dihydrogen phosphate to adjust the pH value of the retentate A to 4.5, and add 0.6% glucosidase to the retentate A after adjusting the pH value, place it at 75° C., and perform enzymatic hydrolysis for 60 minutes;

[0025] (4) add its weight 6% chitosan aqueous solution (chitosan content is 7.0% in its chitosan aqueous solution) to the enzymolysis solution that step (3) obtains, stir and m...

Embodiment 2

[0029] A kind of preparation method of reconstituted tobacco leaf coating liquid provided in embodiment 2 is characterized in that concrete steps comprise:

[0030] (1) Add 9 times of tap water to the mixture of tobacco stems, tobacco powder and secondary tobacco leaves, and after mixing evenly, conduct dynamic countercurrent extraction at 55°C for 0.5h, and obtain insoluble slurry and extract after the extraction is completed;

[0031] (2) Utilize the 300nm aperture inorganic ceramic filter membrane to filter the extract to obtain filtrate A and retentate A;

[0032] (3) Use potassium dihydrogen phosphate to adjust the pH value of the retentate A to 6.1, and add 1.2% glucosidase to the retentate A after adjusting the pH value, place it at 58° C., and perform enzymatic hydrolysis for 50 minutes;

[0033] (4) add its weight 10% chitosan aqueous solution (chitosan content is 4.5% in its chitosan aqueous solution) in the enzymolysis solution that step (3) obtains, stir and mix, l...

Embodiment 3

[0037] Embodiment 3, a kind of preparation method of reconstituted tobacco leaf coating liquid is characterized in that concrete steps comprise:

[0038] (1) Add 7 times of tap water to the mixture of tobacco stems, tobacco powder and secondary tobacco leaves, and after mixing evenly, conduct dynamic countercurrent extraction at 65°C for 1.2 hours, and obtain insoluble slurry and extract after the extraction is completed;

[0039](2) Utilize the 300nm aperture inorganic ceramic filter membrane to filter the extract to obtain filtrate A and retentate A;

[0040] (3) Use potassium dihydrogen phosphate to adjust the pH value of the retentate A to 5.3, and add 0.9% glucosidase to the retentate A after adjusting the pH value, place it at 60° C., and perform enzymatic hydrolysis for 45 minutes;

[0041] (4) add its weight 12% chitosan aqueous solution (chitosan content is 3.5% in its chitosan aqueous solution) in the enzymolysis solution that step (3) obtains, stir and mix, leave st...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

The invention provides a method for preparing a reconstituted tobacco leaf coating solution. The method is to add tap water to the mixture of tobacco stalks, tobacco powder and secondary tobacco leaves and mix them evenly, then dynamically countercurrent extract to obtain insoluble slurry and extract; filter the extract to obtain filtrate A and retentate A; use potassium dihydrogen phosphate Adjust the pH value of the retentate solution A, and add glycosidase to the retentate solution A after adjusting the pH value for enzymolysis, then add chitosan aqueous solution to the enzymolysis solution, stir and mix evenly, and take the supernatant after standing still. Filter to obtain filtrate B; combine filtrate A and filtrate B, concentrate under reduced pressure to obtain concentrate A, add sodium glutamate for Maillard reaction, add liquid fructose, stir evenly, and centrifuge to collect the filtrate. Coating solution for reconstituted tobacco leaves. The method in the present invention is energy-saving and environment-friendly, and the prepared reconstituted tobacco leaf coating liquid has a strong aroma, can enhance aroma quality, increase the fluttering feeling of smoke, reduce throat irritation, and improve oral aftertaste.

Description

technical field [0001] The invention belongs to the field of manufacturing and processing of the tobacco industry, and in particular relates to a method for preparing a coating liquid for reconstituted tobacco leaves. Background technique [0002] Reconstituted tobacco leaves, also known as reconstituted tobacco leaves and tobacco sheets, are made by reorganizing tobacco stems, tobacco dust, and some secondary tobacco leaves produced during the production and processing of tobacco or cigarettes by physical or chemical methods, and can be used as a substitute for cigarette raw materials Taste. The use of reconstituted tobacco leaves in cigarettes can effectively reduce the tar and CO content and improve the smoking quality of cigarettes. The reconstituted tobacco leaf coating solution is a liquid substance obtained after a series of treatments of the water-soluble part in the extraction process of tobacco raw materials, and is an important factor for imparting aroma style to...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Patents(China)
IPC IPC(8): A24B3/14A24B15/24
CPCA24B3/14A24B15/24
Inventor 喻世涛唐向兵高颂程书锋刘志昌
Owner HUBEI CHINA TOBACCO IND
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products