Stepwise removing method of phosphate and sulfate radicals in iron phosphate wastewater
A technology of iron phosphate and phosphate radicals, which is applied in chemical instruments and methods, preparation/separation of ammonia, water pollutants, etc. It can solve the problems that phosphate radicals and sulfate radicals cannot be removed and recovered step by step, and achieve a high degree of resource utilization Effect
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[0064] Example 1
[0065] The step-by-step removal of phosphate and sulfate in ferric phosphate wastewater is as follows:
[0066] 1) Take iron phosphate production wastewater, test the concentration of phosphate and sulfate, and add lye to adjust the pH of the wastewater = 6-9;
[0067] 2) According to the test phosphate concentration, add ferric sulfate solid with the number of moles of iron ion 0.5 times that of phosphate ion, and stir the reaction for 30 minutes;
[0068] 3) Add lye again to adjust pH=3-3.5, stir for 2min;
[0069] 4) Add 5% PFC, and the volume ratio of iron phosphate wastewater is 1:2000, stir the reaction for 10 minutes, let the precipitation stand for 30 minutes, and filter to obtain a solid containing iron phosphate and the filtrate. The filtrate is analyzed for the sulfate concentration and phosphate concentration. ;
[0070] 5) Determine the sulfate concentration in the filtrate in step 4), and add calcium hydroxide solid at a molar ratio of calcium to sulfate...
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[0077] Example 2
[0078] The step-by-step method for removing phosphate and sulfate in iron phosphate wastewater, the specific steps are as follows:
[0079] 1) Take iron phosphate production wastewater, test the concentration of phosphate and sulfate, and add lye to adjust the pH of the wastewater = 6-9;
[0080] 2) According to the concentration of test phosphate, add iron sulfate solid with the number of moles of iron ion as 2 times of phosphate ion, and stir for 2h;
[0081] 3) Add lye again to adjust pH=7-8, and stir for 2min;
[0082] 4) Add 3% PAS and stir and react for 2 minutes, and the volume ratio to iron phosphate wastewater is 1:500. The precipitate is left standing for 5 minutes and filtered to obtain a solid containing iron phosphate and a filtrate. The filtrate is analyzed for the concentration of sulfate and phosphate;
[0083] 5) Determine the sulfate concentration in the filtrate in step 4), and add calcium hydroxide solid at a molar ratio of calcium to sulfate of 1.2...
Example Embodiment
[0090] Example 3
[0091] The step-by-step method for removing phosphate and sulfate in iron phosphate wastewater, the specific steps are as follows:
[0092] 1) Take iron phosphate production wastewater, test the concentration of phosphate and sulfate, and add lye to adjust the pH of the wastewater = 6-9;
[0093] 2) According to the test phosphate concentration, add ferric sulfate solid with the number of moles of iron ions 1.2 times that of phosphate ions, and stir the reaction for 30 minutes;
[0094] 3) Add lye again to adjust pH=3.5-4.5 and stir for 2min;
[0095] 4) Add 0.5% PFS and stir and react for 5 min, and the volume ratio to ferric phosphate wastewater is 1:1500. The precipitate is allowed to stand for 30 min and filtered to obtain a solid containing ferric phosphate and a filtrate. The filtrate is analyzed for the concentration of sulfate and phosphate;
[0096] 5) Determine the sulfate concentration in the filtrate in step 4), and add calcium hydroxide solid at a molar ra...
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