Fresh keeping material for eggs of hens
A technology of fresh-keeping materials and eggs, which is applied in the field of fresh-keeping materials for grass chicken eggs. It can solve the problems of high quality preservation cost, limited storage time of grass eggs, and difficulty in egg circulation, and achieve excellent mechanical properties, excellent biodegradability, and extended storage time. Effect
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Embodiment 1
[0017] A fresh-keeping material for grass chicken eggs, which is made of the following ingredients in parts by weight: 120 parts of polyvinyl alcohol, 45 parts of ethyl orthosilicate, 20 parts of methyl triethoxysilane, 15 parts of stearic acid, 10 parts of hydrochloric acid solution, 50 parts of ethanol, 6 parts of phosphate buffer solution, 0.2 parts of nano-zinc oxide, 200 parts of deionized water, and its preparation method comprises the following steps:
[0018] (1) Dissolve polyvinyl alcohol in deionized water under stirring, heat up to 50°C, add methyltriethoxysilane dropwise, reflux and stir for 2.5 hours under the protection of nitrogen, after the reaction, cool down to 15°C, Add nano-zinc oxide, ultrasonically disperse for 30 minutes, the ultrasonic power is 320 watts, and stand for 5 hours after ultrasonic;
[0019] (2) Dissolve ethyl orthosilicate in ethanol solvent, stir and mix, add hydrochloric acid solution, heat up to 80°C, add stearic acid, stir to dissolve, ...
Embodiment 2
[0027] A fresh-keeping material for grass chicken eggs, which is made of the following ingredients in parts by weight: 125 parts of polyvinyl alcohol, 48 parts of ethyl orthosilicate, 22 parts of methyl triethoxysilane, 18 parts of stearic acid, 11 parts of hydrochloric acid solution, 55 parts of ethanol, 7 parts of phosphate buffer solution, 0.25 parts of nano-zinc oxide, 205 parts of deionized water, and its preparation method comprises the following steps:
[0028] (1) Dissolve polyvinyl alcohol in deionized water under stirring, heat up to 53°C, add methyltriethoxysilane dropwise, reflux and stir for 2.8 hours under the protection of nitrogen, after the reaction, cool down to 18°C, Add nano-zinc oxide, ultrasonically disperse for 33 minutes, ultrasonic power is 325 watts, and stand still for 5.5 hours after ultrasonic;
[0029] (2) Dissolve ethyl orthosilicate in ethanol solvent, stir and mix, add hydrochloric acid solution, heat up to 82°C, add stearic acid, stir to disso...
Embodiment 3
[0037] A fresh-keeping material for grass chicken eggs, which is made of the following ingredients in parts by weight: 130 parts of polyvinyl alcohol, 50 parts of ethyl orthosilicate, 25 parts of methyl triethoxysilane, 20 parts of stearic acid, 12 parts of hydrochloric acid solution, 60 parts of ethanol, 8 parts of phosphate buffer solution, 0.3 parts of nano-zinc oxide, 210 parts of deionized water, and its preparation method comprises the following steps:
[0038] (1) Dissolve polyvinyl alcohol in deionized water under stirring, heat up to 55°C, add methyltriethoxysilane dropwise, reflux and stir for 3.0 hours under the protection of nitrogen, after the reaction, cool down to 20°C, Add nano-zinc oxide, ultrasonically disperse for 35 minutes, the ultrasonic power is 330 watts, and stand for 6 hours after ultrasonic;
[0039] (2) Dissolve ethyl orthosilicate in ethanol solvent, stir and mix, add hydrochloric acid solution, heat up to 85°C, add stearic acid, stir to dissolve, ...
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