Method for preparing conductive solution of conductive electrode and method for preparing conductive electrode
A technology of conductive electrodes and conductive solutions, which is applied in equipment for manufacturing conductive/semiconductive layers, conductive layers on insulating carriers, conductive materials, etc., can solve device failure, low adhesion of flexible substrates, and limited applications and other problems to achieve the effect of preventing water failure and avoiding short circuits
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Embodiment 1
[0033] The preparation method of the conductive solution of the conductive electrode of the present embodiment, its steps are as follows:
[0034] S1. Polymerize styrene sulfonate and acrylate to form a polymer:
[0035] Put sodium styrene sulfonate and pentyl acrylate with a ratio of parts by weight of 6:4 into a three-necked flask, then add solvent and initiator, and react the resin monomer at 90°C for 12 hours for polymerization. Wherein, the sodium styrene sulfonate and pentyl acrylate are resin monomers, the solvent is selected from N.N-dimethylacetamide, and the initiator is selected from BPO. The added amount of the resin monomer, solvent and initiator is as follows: the resin monomer accounts for 15% of the total weight, the solvent accounts for 84% of the total weight, and the initiator accounts for 1% of the total weight. After the end of the polymerization reaction, distill under reduced pressure for 5 hours to evaporate most of the solvent; then use deionized wate...
Embodiment 2
[0048] The preparation method of the conductive solution of the conductive electrode of the present embodiment, its steps are as follows:
[0049] S1. Polymerize styrene sulfonate and acrylate to form a polymer:
[0050] Put sodium styrene sulfonate and butyl acrylate with a ratio of parts by weight of 5:3 into a three-necked flask, and then add solvent and initiator to react the resin monomer at a temperature of 80°C for 14 hours for polymerization. Wherein, the sodium styrene sulfonate and butyl acrylate are resin monomers, the solvent is selected from N.N-dimethylformamide, and the initiator is selected from LPO. The added amount of the resin monomer, solvent and initiator is as follows: the resin monomer accounts for 14% of the total weight, the solvent accounts for 85% of the total weight, and the initiator accounts for 1% of the total weight. After the end of the polymerization reaction, distill under reduced pressure for 4 hours to evaporate most of the solvent; then u...
Embodiment 3
[0063] The preparation method of the conductive solution of the conductive electrode of the present embodiment, its steps are as follows:
[0064] S1. Polymerize styrene sulfonate and acrylate to form a polymer:
[0065] Put calcium styrene sulfonate and butyl acrylate with a ratio of parts by weight of 7:5 into a three-necked flask, then add a solvent and an initiator to react the resin monomer at 100°C for 10 hours for polymerization. Wherein, the calcium styrene sulfonate and butyl acrylate are resin monomers, the solvent is selected from N.N-dimethylacetamide, and the initiator is selected from LPO. The added amount of the resin monomer, solvent and initiator is as follows: the resin monomer accounts for 15% of the total weight, the solvent accounts for 83% of the total weight, and the initiator accounts for 2% of the total weight. After the end of the polymerization reaction, distill under reduced pressure for 6 hours to evaporate most of the solvent; then use deionized ...
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