Extracting method of melaleuca alternifolia tea tree essential oil
A technology of Melaleuca alternifolia and tea tree essential oil, which is applied in the field of extraction of Melaleuca alternifolia tea tree essential oil, can solve problems such as the loss of active components of essential oil, easy mold growth of tea tree essential oil, and reduce the use value of spices, etc., and achieve rapid extraction Effect
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Embodiment 1
[0027] (1) Take 500 g of fresh stems and leaves of Melaleuca alternifolia, the measured water content is 52%, and pulverize to 20 mesh after removing impurities;
[0028] (2) Use a certain amount of solvent to moisten the stems and leaves of Melaleuca alternifolia, and let it stand for 2 hours. A certain proportion of the solvent is a mixed solvent of propanol and ethanol, and extract it twice;
[0029] (3) Heat the mixture after standing to reflux for extraction for 2 h; after cooling, filter to obtain the extract;
[0030] (4) Distilling the extract obtained above under reduced pressure, recovering the solvent propanol and ethanol at 60°C, recovering water and active ingredients of tea tree with low boiling point at 80°C, and obtaining tea tree essential oil at 160°C;
[0031] (5) The obtained Melaleuca alternifolia tea tree essential oil was analyzed by GC-MS, from figure 1 It can be seen that the obtained tea tree essential oil is determined to contain terpinene 4-ol, and...
Embodiment 2
[0033] (1) Take 400 g of fresh stems and leaves of Melaleuca alternifolia tea tree, the measured water content is 33%, and grind to 20 mesh after removing impurities;
[0034] (2) Select a certain amount of solvent to moisten the stems and leaves of Melaleuca alternifolia, and let it stand for 2 hours, in which the solvent is a mixed solvent of ethyl acetate and ethanol, and extract twice;
[0035] (3) Heat the mixture after standing to reflux at 60°C for 2 h; after cooling, filter to obtain the extract;
[0036] (4) Distilling the extract obtained above under reduced pressure, recovering the solvent propanol and ethanol at 60°C, recovering water and active ingredients of tea tree with low boiling point at 80°C, and obtaining tea tree essential oil at 160°C;
[0037] (5) The obtained Melaleuca alternifolia tea tree essential oil was analyzed by GC-MS, from figure 2 It can be seen that the obtained tea tree essential oil definitely contains terpinene 4-ol, and the content is ...
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