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Extracting method of melaleuca alternifolia tea tree essential oil

A technology of Melaleuca alternifolia and tea tree essential oil, which is applied in the field of extraction of Melaleuca alternifolia tea tree essential oil, can solve problems such as the loss of active components of essential oil, easy mold growth of tea tree essential oil, and reduce the use value of spices, etc., and achieve rapid extraction Effect

Inactive Publication Date: 2019-01-04
ANHUI UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] 1. Fat adsorption method, which uses oil to absorb the essential oil in tea tree. Although the process is simple, it is difficult to separate the essential oil and oil in the follow-up
[0004] 2. Supercritical extraction method, using supercritical carbon dioxide fluid extraction to obtain tea tree essential oil, this method has the advantages of high yield and high product quality; but because supercritical carbon dioxide fluid is too soluble, non-essential oil components in tea tree are also extracted out, and the water in the tea tree is not easy to separate, making the tea tree essential oil easy to grow mold during storage, which limits the application range of the obtained product
This method has simple equipment, easy operation, low cost, large output, and no pollution. However, after a long period of heating and distillation, the essential oil is likely to cause thermal decomposition of heat-sensitive components and hydrolysis of easy-to-hydrolyze components, resulting in the loss of active components in the essential oil and aromatic odor. changes, thereby reducing the use value as a spice

Method used

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  • Extracting method of melaleuca alternifolia tea tree essential oil
  • Extracting method of melaleuca alternifolia tea tree essential oil

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] (1) Take 500 g of fresh stems and leaves of Melaleuca alternifolia, the measured water content is 52%, and pulverize to 20 mesh after removing impurities;

[0028] (2) Use a certain amount of solvent to moisten the stems and leaves of Melaleuca alternifolia, and let it stand for 2 hours. A certain proportion of the solvent is a mixed solvent of propanol and ethanol, and extract it twice;

[0029] (3) Heat the mixture after standing to reflux for extraction for 2 h; after cooling, filter to obtain the extract;

[0030] (4) Distilling the extract obtained above under reduced pressure, recovering the solvent propanol and ethanol at 60°C, recovering water and active ingredients of tea tree with low boiling point at 80°C, and obtaining tea tree essential oil at 160°C;

[0031] (5) The obtained Melaleuca alternifolia tea tree essential oil was analyzed by GC-MS, from figure 1 It can be seen that the obtained tea tree essential oil is determined to contain terpinene 4-ol, and...

Embodiment 2

[0033] (1) Take 400 g of fresh stems and leaves of Melaleuca alternifolia tea tree, the measured water content is 33%, and grind to 20 mesh after removing impurities;

[0034] (2) Select a certain amount of solvent to moisten the stems and leaves of Melaleuca alternifolia, and let it stand for 2 hours, in which the solvent is a mixed solvent of ethyl acetate and ethanol, and extract twice;

[0035] (3) Heat the mixture after standing to reflux at 60°C for 2 h; after cooling, filter to obtain the extract;

[0036] (4) Distilling the extract obtained above under reduced pressure, recovering the solvent propanol and ethanol at 60°C, recovering water and active ingredients of tea tree with low boiling point at 80°C, and obtaining tea tree essential oil at 160°C;

[0037] (5) The obtained Melaleuca alternifolia tea tree essential oil was analyzed by GC-MS, from figure 2 It can be seen that the obtained tea tree essential oil definitely contains terpinene 4-ol, and the content is ...

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Abstract

The invention discloses an extracting method of melaleuca alternifolia tea tree essential oil, and belongs to the technical field of plant extraction. The method includes the following steps of selecting fresh melaleuca alternifolia tea tree stems and leaves for cleaning and smashing; mixing a certain amount of different-polarity solvent according to a certain ratio to obtain a mixed solvent, andwetting the tea tree steams and leaves for standing for a certain period of time; conducting heating, backflowing, extracting and filtering on the standing mixture; decompressing and distilling the filtered liquid mixture for recovering the solvent and tea tree essential oil; conducting GC-MS analysis on the obtained melaleuca alternifolia tea tree essential oil and determining the content of a main active component (terpine-4 alcohol) in the obtained tea tree essential oil. The method is simple, the tea tree essential oil is extracted from melaleuca alternifolia to the maximum extent, production benefits are directly improved, the obtained tea tree essential oil is extremely low in water content, and storage is facilitated.

Description

technical field [0001] The invention belongs to the field of essential oil extraction technology, and in particular relates to an extraction method of Melaleuca alternifolia tea tree essential oil. Background technique [0002] Melaleuca alternifolia, also known as tea oil tree, is the main raw material of tea tree essential oil. The tea tree essential oil extracted from the fresh branches and leaves of Melaleuca alternifolia is a natural oil, rich in pine oil, lemon olein, and eucalyptol , anisole, etc., have the effects of sterilization and anti-inflammation, astringent pores, treatment of colds, coughs, rhinitis, asthma, improvement of dysmenorrhea and genital infections. Suitable for oily and acne-prone skin, it can treat purulent wounds and burns, sunburn and dandruff. Widely used in many fields such as skin care products, cosmetics, medicines, food spices, etc. The extraction method of existing tea tree essential oil mainly contains: [0003] 1. Fat adsorption metho...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/02
CPCC11B9/027
Inventor 宋吉明吴江敏牛和林毛昌杰陈京帅
Owner ANHUI UNIVERSITY
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