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High-temperature-resistant polyester lubricating oil base oil and preparation method thereof

A technology of lubricating oil base oil and high temperature resistant type, applied in the fields of lubricating oil base oil and its preparation, high temperature resistant polyester lubricating oil base oil and its preparation, can solve the problem of high temperature stability, low non-toxicity, high temperature resistance General, easy to degrade carbon deposits and other problems, to achieve the effect of good lubricating performance and wear resistance, moderate viscosity index, and easy-to-obtain raw materials

Active Publication Date: 2019-01-18
上海新纳克合成材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

With the rapid development of modern industry and the increasingly prominent environmental problems, the requirements for lubricant performance, operational reliability and service life, high temperature stability, low or non-toxicity, etc. are getting higher and higher. Traditional minerals are made of Base oils have been difficult to meet these stringent requirements
Due to the small molecular weight of synthetic ester compounds, the high temperature resistance is average, and it is easy to degrade and generate carbon deposits under high temperature.

Method used

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  • High-temperature-resistant polyester lubricating oil base oil and preparation method thereof
  • High-temperature-resistant polyester lubricating oil base oil and preparation method thereof
  • High-temperature-resistant polyester lubricating oil base oil and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] A kind of high temperature resistant type polyester lubricating oil base oil, is made by following raw material, and described parts are all molar percentages:

[0029]

[0030] A preparation method of high-temperature-resistant polyester lubricating oil base oil, comprising the following steps:

[0031] A. Add 1,3,5-cyclohexanetrimethanol, diethyl fluoromalonate, xylene, and catalyst into the reactor, start stirring and mix thoroughly, and heat up to 140-160°C for reflux and water separation reaction 2~4h;

[0032] B. Add 12-benzoyl stearic acid, 2,2-difluoropropionic acid, and 3-fluoro-4-hydroxybenzoic acid into the reactor for full esterification reaction, and continue the water separation reaction at 150-160°C for 3 ~6h;

[0033] C. Then add perfluoroheptanoic acid and tris(trimethylsilyl) phosphate in the prescribed amount, heat up to 160-170°C for 2-4 hours, and stop the reaction when the acid value is less than 1mgKOH / g;

[0034] D. Add water to wash the ca...

Embodiment 2

[0038] A kind of high temperature resistant type polyester lubricating oil base oil, is made by following raw material, and described parts are all molar percentages:

[0039]

[0040]

[0041] Its preparation method etc. are the same as embodiment 1.

Embodiment 3

[0043] A kind of high temperature resistant type polyester lubricating oil base oil, is made by following raw material, and described parts are all molar percentages:

[0044]

[0045] Its preparation method etc. are the same as embodiment 1.

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Abstract

The invention discloses high-temperature-resistant polyester lubricating oil base oil and a preparation method thereof, and belongs to the field of fine chemical engineering. The base oil is preparedfrom 1,3,5-cyclohexane trimethyl alcohol, diethyl fluoromalonate, 12-benzoyl stearic acid, 2,2-difluoropropionic acid, 3-fluoro-4-hydroxybenzoic acid, perfluoroheptanoic acid and tris(trimethylsilyl)phosphate; fluorine-contained carboxylic acid and the 1,3,5-cyclohexane trimethyl alcohol with high heat resistance are used as main raw materials, the 12-benzoyl stearic acid and the 3-fluoro-4-hydroxybenzoic acid are introduced to adjust the viscosity index of the base oil, and the tris(trimethylsilyl) phosphate is used as a high-temperature-resistant antioxidant; through fluorinated compounds in the raw materials, the high temperature resistance and the carbon deposition resistance of the product are guaranteed. The preparation method has the advantages that the raw materials are easy to obtain, and the method is simple and convenient to operate; the prepared lubricating oil base oil has good high-temperature resistance, a moderate viscosity index, good lubricating performance and wearresistance, can be applied to lubrication of most automotive engines, and is especially applicable to high temperature environments.

Description

technical field [0001] The invention relates to a lubricating oil base oil and a preparation method thereof, in particular to a high-temperature-resistant polyester lubricating oil base oil and a preparation method thereof, belonging to the field of fine chemicals. Background technique [0002] Lubricating oil is an indispensable chemical for mechanical operation and is widely used in various fields of national economy. With the further promotion of economic globalization, especially the rapid development of the automobile industry, and the strengthening of environmental protection and energy saving requirements, although the total demand for lubricating oil has not increased significantly, the demand for high-grade lubricating oil has gradually increased. [0003] Lubricating oil is mainly composed of base oil and additives. Base oil is the main component of lubricating oil, accounting for more than 85%, and plays an important role in the basic properties of lubricating oil...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10M111/02C10N30/06C10N30/08
CPCC10M111/02C10N2030/06C10N2030/08
Inventor 李海云王永垒邢楠楠张雅文魏文静朱梦泽许涛
Owner 上海新纳克合成材料有限公司
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