Method for preparing two-phase manganese-bismuth permanent magnet material
A permanent magnet material, dual-phase manganese-bismuth technology, applied in the direction of magnetic materials, magnetic objects, inductance/transformer/magnet manufacturing, etc., can solve the problem of MnBi/FeCo hysteresis curve collapse, dual-phase composite material remanence and magnetic energy product Improve and affect MnBi/FeCo and other issues, and achieve the effect of simple and easy preparation method, stable permanent magnetic performance and excellent magnetic performance
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Embodiment 1
[0019] The composition chemical formula of the main body of the permanent magnet material in this embodiment is Mn 57 Bi 42 Al 1 .
[0020] Weigh each element according to the chemical formula of the above ingredients for batching; put the batching in the smelting furnace, and vacuumize the furnace to at least 5×10 -3 Pa; Then, pass helium gas until the pressure in the furnace is 50kPa; heat up to 1300°C to melt, stir, refine and cast into water-cooled copper molds for use.
[0021] The obtained alloy ingot is crushed, put into the quartz tube in the vacuum belt throwing machine, the diameter of the nozzle at the bottom of the quartz tube is 0.5 mm, after the chamber of the vacuum belt throwing machine is evacuated, the cavity is filled with protective gas; Turn on the power supply of the vacuum strip machine to heat and melt the alloy in the quartz tube. At the same time, control the distance from the nozzle at the bottom end of the quartz tube to the surface of the copper...
Embodiment 2
[0024] The composition chemical formula of the main body of the permanent magnet material in this embodiment is Mn 52 Bi 45 Al 3 .
[0025] Weigh each element according to the chemical formula of the above ingredients for batching; put the batching in the smelting furnace, and vacuumize the furnace to at least 5×10 -3 Pa; Then, pass helium gas until the pressure in the furnace is 80kPa; heat up to 1450°C to melt, stir, refine, and then cast it into a water-cooled copper mold for use.
[0026] The obtained alloy ingot is crushed and put into the quartz tube in the vacuum strip machine. The diameter of the nozzle at the bottom of the quartz tube is 0.8mm. After the cavity of the vacuum strip machine is vacuumed, fill the cavity with protective gas; Turn on the power supply of the vacuum strip machine to heat and melt the alloy in the quartz tube. At the same time, control the distance from the nozzle at the bottom of the quartz tube to the surface of the copper roller to be 1...
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