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Method for preparing luminous coating water-repellent synthetic leather base cloth by grafting, softening and filling modification

A technology of synthetic leather base cloth and luminous coating, which is applied in the field of synthetic leather, can solve the problems of poor hygienic performance of superfine fiber synthetic leather, shorten the service life of luminous coating fabric, and easy moisture absorption of luminous coating fabric. Good mechanical properties, high washing fastness, and increased specific surface area

Inactive Publication Date: 2019-04-02
蚌埠星烁新材料科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Synthetic leather is a focus of research in recent years because of its wide source of raw materials and high mechanical strength, but the active group content of synthetic leather base cloth is small, so that water vapor cannot be effectively absorbed and transmitted between the fiber and the outside world. As a result, the hygienic performance of microfiber synthetic leather is poor
[0003] At present, luminous coated fabrics have been widely used in clothing, luminous toys, luminous embroidery, luminous slippers, etc., but due to the influence of some luminescent materials themselves and external factors, the surface stability of such products is not very ideal. Exposure to the air for a long time, even the moisture in the air can make it hydrolyze to a certain extent, and most of the coating agents used are hydrophilic, which makes the surface of the luminous coating fabric more prone to moisture absorption and moisture, resulting in luminous brightness and afterglow time are greatly reduced, and even lose the characteristics of luminescence-luminescence, which seriously shortens the service life of luminous coating fabrics and limits its application fields

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] A method for grafting-softening-filling modification to prepare luminous coating water-repellent synthetic leather base cloth, is characterized in that it comprises the following steps:

[0026] (1) Pretreatment of synthetic leather base cloth:

[0027] The synthetic leather base cloth is pretreated in formic acid with a liquid ratio of 30:1. After being treated at 50-60°C for 30 minutes, it is fully washed with water, and then the liquid ratio is 50:1 with 15% sulfuric acid at 50-55 After hydrolysis at ℃ for 3 hours, the synthetic leather base cloth was washed with water at 70-75 °C for 20 min, and fully dried to obtain the pretreated synthetic leather base cloth;

[0028] (2) Using epoxy resin crosslinking agent to graft collagen to modify synthetic leather base fabric:

[0029] Put the pretreated synthetic leather base cloth obtained in (1) into a small infrared dyeing machine with a liquid ratio of 30:1, add a cross-linking agent, hydrolyze and open the ring at 35-...

Embodiment 2

[0040] A method for grafting-softening-filling modification to prepare luminous coating water-repellent synthetic leather base cloth, is characterized in that it comprises the following steps:

[0041] (1) Pretreatment of synthetic leather base cloth:

[0042] The synthetic leather base cloth is pretreated in formic acid with a liquid ratio of 30:1. After being treated at 50-60°C for 40 minutes, it is fully washed with water, and then the liquid ratio is 50:1 with 15% sulfuric acid at 50-55 After hydrolysis at ℃ for 4 hours, the synthetic leather base cloth was washed with water at 70-75 °C for 30 min, and fully dried to obtain the pretreated synthetic leather base cloth;

[0043] (2) Using epoxy resin crosslinking agent to graft collagen to modify synthetic leather base fabric:

[0044]Put the pretreated synthetic leather base cloth obtained in (1) into a small infrared dyeing machine with a liquid ratio of 30:1, add a cross-linking agent, hydrolyze and open the ring at 35-4...

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Abstract

The invention discloses a method for preparing a luminous coating water-repellent synthetic leather base cloth by grafting, softening and filling modification. The method includes putting the pretreated synthetic leather base cloth into an infrared dyeing small prototype, adding a cross-linking agent for hydrolysis ring opening, fully washing with water, adding collagen graft reaction, fully washing with water, and drying in the air to obtain the grafted modified synthetic leather base cloth; filling the grafted modified synthetic leather base cloth with a filler, softening with a softening agent, fixing with formic acid, cross-linking with an aluminum tanning agent, alkali extracting with sodium bicarbonate, fully washing with water, hanging and drying to obtain the soft-filled modified synthetic leather base cloth; dipping the soft-filled modified synthetic leather base cloth into a luminous coating finishing agent, drying, dipping into a sodium hydroxide solution, preforming alkalireduction, fully washing with water, pre-baking and baking to obtain the luminous coating-finished synthetic leather base cloth; dipping the luminous coating-finished synthetic leather base fabric ina fluorine-containing water repellent finishing agent, pre-baking and baking to obtain the luminous coating water-repellent synthetic leather base cloth.

Description

technical field [0001] The invention belongs to the field of synthetic leather, and in particular relates to a method for preparing a luminous coating water-repellent synthetic leather base cloth through grafting-softening-filling modification. Background technique [0002] Synthetic leather is a focus of research in recent years because of its wide source of raw materials and high mechanical strength, but the active group content of synthetic leather base cloth is small, so that water vapor cannot be effectively absorbed and transmitted between the fiber and the outside world. Thereby causing the hygienic performance of superfine fiber synthetic leather is relatively poor. [0003] At present, luminous coated fabrics have been widely used in clothing, luminous toys, luminous embroidery, luminous slippers, etc., but due to the influence of some luminescent materials themselves and external factors, the surface stability of such products is not very ideal. Exposure to the ai...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06N3/00D06N3/14D06M15/15D06M13/188D06M11/55
CPCD06M11/55D06M13/188D06M15/15D06N3/0059D06N3/0061D06N3/0077D06N3/142D06N2209/103D06N2209/126D06N2209/1685D06N2211/28
Inventor 郭艳
Owner 蚌埠星烁新材料科技有限公司
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