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A Glycol-Water Based Coolant with Low Corrosion and Low Conductivity

A water-based coolant and ethylene glycol technology, applied in heat exchange materials, chemical instruments and methods, etc., can solve the problems of serious corrosion, complex structure, complicated electrochemical mechanism, etc., so as to reduce usage and corrosion. Effect

Active Publication Date: 2020-07-14
BEIJING UNIV OF CHEM TECH +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The liquid cooling system not only has a complex structure, but also has various changes in the fluid mechanical behavior of the heat exchange medium, and is composed of different metals such as carbon steel, cast aluminum, anti-rust aluminum, brass, etc. The corrosion potential of different metals is different, so that each There are differences in the corrosion of the two materials, and constitute galvanic corrosion, especially the synergistic effect between electrochemical corrosion and hydrodynamic factors, which leads to the complexity of the electrochemical mechanism of the system materials in the heat exchange working fluid, and the corrosion is relatively more serious

Method used

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Examples

Experimental program
Comparison scheme
Effect test

example 1

[0014] Example 1 When in 1 liter of ethylene glycol-water-based (volume ratio 65 / 35) solution, first add corrosion inhibitors: namely, ethanolamine phosphate 150mg / L, benzothiazole 150mg / L, mercaptobenzothiazole 150mg / L , 150 mg / L of polyvinylpyrrolidone compound, 100 mg / L of sodium borate, and 10 mg / L of +3-valent cerium nitrate were stirred and mixed. Second, hydroxymethylaminomethane was used as a buffer to adjust the pH of the ethylene glycol-water-based solution until the pH reached 8.5. Finally, 1.0 ml of methyl orange indicator solution was added, and the solution changed from colorless to bright brownish yellow, thus obtaining a cooling liquid. The test results show that the conductivity of the coolant is 90-95μS / cm; the average corrosion rate of copper, cast aluminum, aluminum alloy, and stainless steel is less than 0.1g / m when soaked in the coolant at 90°C for 14 days 2 .d. After the test, the pH value of the cooling liquid is 7.8-8.0; the corrosion of brass alloy ...

example 2

[0015] Example 2 In 1 liter of ethylene glycol-water-based (volume ratio 65 / 35) solution, first, add corrosion inhibitors: namely, ethanolamine phosphate 100mg / L, benzothiazole 200mg / L, mercaptobenzothiazole 200mg / L , Polyvinylpyrrolidone compound 100mg / L, sodium borate 200mg / L, +3-valent cerium nitrate 5mg / L. Second, the pH of the glycol-water-based coolant was adjusted using hydroxymethylaminomethane as a buffer until the pH reached 8.5. Finally, 1.0 ml of methyl orange indicator solution was added, and the solution changed from colorless to bright brownish yellow to obtain a cooling solution. The test results show that the conductivity of the coolant is ~90μS / cm; the average corrosion rate of aluminum alloy, solder, and stainless steel is less than 0.1g / m after being soaked in the coolant at 90°C for 14 days 2 .d. Corrosion of brass alloy is less than Example 1, less than 0.1g / m 2 .d; while corrosion pits appear on the surface of cast aluminum, the corrosion rate is 0.2g...

example 3

[0016] Example 3 In the ethylene glycol-water-based (volume ratio 65 / 35) solution, first, add a corrosion inhibitor, that is, ethanolamine phosphate 150mg / L, benzothiazole 200mg / L, polyvinylpyrrolidone compound 100mg / L, boric acid Sodium 150mg / L, +3 valent cerium nitrate 3mg / L. At the same time, change mercaptobenzothiazole to sodium mercaptobenzothiazole, and add at a concentration of 200mg / L. Second, the pH of the glycol-water-based coolant was adjusted using hydroxymethylaminomethane as a buffer until the pH reached 8.5. Finally, 1.0 ml of methyl orange indicator solution was added, and the solution changed from colorless to bright brownish yellow to obtain a cooling solution. The test results show that after changing mercaptobenzothiazole to mercaptobenzothiazole sodium, the amount of hydroxymethylaminomethane added is reduced by 1 / 3, and the conductivity of the coolant is 80-85μS / cm; after the test, the pH value of the coolant is 8.3 -8.4; Copper and its alloys, aluminu...

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Abstract

A low-corrosion and low-conductivity ethylene glycol-water-based liquid coolant belongs to the field of electronic liquid cooling. The liquid coolant is characterized in that the liquid coolant is obtained by adding a corrosion inhibitor to an ethylene glycol-water-based (volume ratio of 65 / 35) solution, and the corrosion inhibitor comprises 50-150 mg / L of ethanolamine phosphate, 100-400 mg / L of amixture of benzothiazole and mercaptobenzothiazole according to a mass ratio 1:1, 50-200mg / L of a polyvinylpyrrolidone compound, 100-200 mg / L of sodium borate and 3-10 mg / L of lanthanum (III) nitrate. Hydroxymethylaminomethane is used as a pH adjuster to adjust the pH of the ethylene glycol-water-based liquid coolant to 8.5. The ethylene glycol-water-based liquid coolant belongs to a cathode-anode hybrid corrosion inhibitor, and an organic basic compound is used as the pH adjuster to prepare the low-corrosion and low-conductivity ethylene glycol-water-based liquid coolant.

Description

technical field [0001] The invention belongs to the use of an anode-cathode hybrid corrosion inhibitor, using an organic basic compound as a pH regulator to prepare a low-corrosion and low-conductivity ethylene glycol-water-based cooling fluid, which is used as a heat exchange working medium for Copper and its alloys, aluminum alloys, stainless steel and other multi-metal materials such as motors, air conditioners, and liquid cooling systems for electrical and electronic equipment. Background technique [0002] Today, with the rapid development of electronic integrated circuit technology and the wide application of electronic chips, the degree of integration of electrical and electronic equipment is getting higher and higher. The heat generated by the heating of electrical and electronic equipment components has seriously affected electrical equipment and electronic devices. Reliability and safety, normal operation. At the same time, with the high-end development and applic...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09K5/20
Inventor 雍兴跃程普强张小明陈振宁杨健何祯潘金杰陈日辉周林张新全齐社红杨文毅王欣笛
Owner BEIJING UNIV OF CHEM TECH