Preparation method of long-acting antifogging agent
An anti-fogging agent, a long-term technology, applied in chemical instruments and methods, other chemical processes, etc., can solve the problems of non-lasting anti-fogging effect and loss of hydrophilicity, and achieve long-term anti-fogging performance and improved hydrophilicity. , the effect of pore size reduction
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[0026]Mix sodium lignosulfonate solution with a mass fraction of 10-12% and formaldehyde in a beaker at a mass ratio of 14:1, and add sodium sulfite 1 to 4 times the mass fraction of formaldehyde to the beaker, with a mass fraction of 5-10% The sodium hydroxide solution adjusts the pH of the material in the beaker to 10-11, and after stirring and reacting for 2-3 hours at a temperature of 90-95°C and a rotation speed of 300-320r / min, the pretreated sodium lignosulfonate is obtained. Solution, mix the pretreated sodium lignosulfonate solution and potassium iodide in a three-necked flask at a mass ratio of 90:1 to 100:1, and add 1 , 6-dibromohexane solution, control the adding rate of 1,6-dibromohexane solution to be 8-10mL / min, and at the same time control the pH of the material in the three-necked flask with a sodium hydroxide solution with a mass fraction of 5-12% 11.0 to 11.5, and stirred and reacted for 4 to 5 hours at a temperature of 80 to 85°C and a rotational speed of 2...
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