A mouth-dissolving film composition
A technology of composition and mouth-dissolving film, which is applied in the field of mouth-dissolving film composition and its preparation, can solve problems such as aggregation of active substances, affecting the mouthfeel and dissolution of the film, and poor treatment effect, so as to improve compliance and film-forming Good appearance and taste, uniform distribution of active ingredients
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Embodiment 1
[0047] Example 1: Ondansetron Oral Dissolving Film
[0048] The dosage of each prescription is shown in Table 1, and the prescription evaluation is shown in Table 2.
[0049] Table 1:
[0050]
[0051] The raw material of ondansetron was pulverized by a mechanical pulverizer (the aperture of the screen mesh was 0.5 mm). Place the prescribed amount of ondansetron in the main tank of the homogenizer, add poloxamer (not added in preparation D), absolute ethanol and water, and stir evenly. The polydextrose, the aqueous solution of polyoxyethylene and the aqueous solution of hydroxypropyl methylcellulose were added to the main tank, stirred in vacuum, and sheared at high speed for 15 minutes to obtain a glue solution. The glue liquid is scraped on a continuous coating machine, dried and formed, cut into a film with a specified area, and packaged and sealed.
[0052] Table 2:
[0053]
[0054] Based on the analysis of the dissolution time, mouthfeel, breaking force and 180...
Embodiment 2
[0055] Example 2: Entecavir Oral Dissolution Film
[0056] The dosage and evaluation of each prescription are shown in Table 3.
[0057] table 3
[0058]
[0059] Entecavir was dispersed in absolute ethanol. Add the aqueous poloxamer solution and stir until the entecavir is completely dissolved. Add maltitol, lemon essence, tartrazine, polydextrose, polyoxyethylene, and hypromellose aqueous solution to it and stir evenly. High-speed shearing and standing to obtain glue. The glue liquid is scraped on a continuous coating machine, dried and formed, cut into a film with a specified area, and packaged and sealed.
[0060] After experimental analysis, polydextrose can improve the mouthfeel and texture of the dissolving film.
Embodiment 3
[0061] Example 3 Dissolution test:
[0062] According to the dissolution test method (the fourth method of the four general rules of the Chinese Pharmacopoeia in 2015), take the film preparation 2*3cm obtained from the ondansetron mouth-dissolving film preparation A after being coated by a continuous coating machine, and fix it on a two-layer disc. Place the mesh plate in the lower part of the dissolution vessel, making it parallel to the rotating surface of the paddle bottom, with a distance of 25 ± 2 mm, for measurement, the dissolution temperature is 37 ± 0.5 °C, the volume of the dissolution medium is 900 ml, and the rotation speed is 50 rpm . The dissolution media were 0.1M hydrochloric acid solution, pH4.5 acetate buffer solution, pH6.8 phosphate buffer solution and purified water.
[0063] result (see figure 1 ): there is no obvious difference in the dissolution conditions of the ondansetron oral film-dissolving agent prepared by the present invention in the four medi...
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