Preparation method of nitrification organic matter and prepared nitrification organic matter
A technology of organic matter and nitrating acid solution, which is applied in the preparation of nitro compounds, organic chemistry, chemical instruments and methods, etc. It can solve the problems of affecting the quality of chemical products, poor batch production stability, and high post-processing costs, and achieve large-scale industrial applications. value, improved production environment, and high production efficiency
Pending Publication Date: 2019-07-12
SHANDONG HIMILE CHEM TECH
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The invention discloses a preparation method of nitrification organic matter and the prepared nitrification organic matter, and relates to the technical field of organic synthesis. The preparation method of the nitrification organic substance comprises the following steps: introducing a nitrification acid liquid and molten-state organic matter to be nitrified into a microchannel reactor, and performing a reaction, wherein the organic matter to be nitrified is solid at normal temperature, and solidification and/or dissolution in the nitrification acid liquid does not occur in the organic matterto be nitrified after the organic matter to be nitrified is introduced into the microchannel reactor. According to the preparation method of the nitrification organic matter provided by the invention, the nitrification organic matter prepared by the method has a very good yield and purity without a solvent removal post-treatment process; in the whole process, no solvent participates in the reaction, so that the post-treatment process of solvent removal is avoided; and the method has high safety in the whole reaction process, adopts automation control, has high production efficiency and a greatly-improved production environment, and has larger industrial application value.
Application Domain
Chemical/physical/physico-chemical microreactorsNitro compound preparation
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- Effect test(2)
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