Chemical mechanical pulping process for whole corn stalk

A corn stalk and chemical mechanical technology, which is applied in the field of corn stalk chemical mechanical pulping process, can solve the problems of low-efficiency physical separation of bark and leaves, poor physical properties of pulping, and large consumption of liquid medicine, etc., to reduce equipment Investment, less chemical consumption, and the effect of reducing consumption

Active Publication Date: 2019-08-02
CHINA NAT PULP & PAPER RES INST CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] The purpose of the present invention is to provide a pure corn stalk chemical-mechanical pulping process, which avoids the low-efficiency physical separation of bark and leaves, retains most of the fiber components in raw materials, and solves the problem of corn stalk pulping. Low pulp yield, large consumption of chemical solution, and poor physical properties of pulp. At the same time, hot water pre-extraction waste liquid and pre-impregnation waste liquid can also be used as raw materials for other processes, which is conducive to realizing high-value utilization of all components.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0037] (1) Whole corn stalks are used as raw materials, and the corn stalks are first cut into small sections with a size of 3-10 cm by a grass cutter.

[0038] (2) Put the cut corn stalks into a cooking pot or an extraction tank, add tap water, the mass is 20 times the mass of the dry corn stalks, the extraction temperature is 98°C, and the holding time is 60 minutes.

[0039] (3) After separating the extracted corn stalks from the hot water, put them into a twin-screw extruder for extruding, and add tap water at the rear of the extruder to wash the stalks. 5 times the dry mass.

[0040] (4) Put the dehydrated corn stalks into a cooking pot or a prepreg, add sodium hydroxide, the quality is 8% of the absolute dry mass of the crushed corn stalks, and the amount of tap water added is the absolute dry weight of the crushed corn stalks. 20 times the dry mass, the impregnation temperature is 80°C, and the holding time is 60 minutes.

[0041] (5) The pre-impregnated corn stalks w...

Embodiment 2

[0046] (1) Whole corn stalks are used as raw materials, and the corn stalks are first cut into small sections with a size of 3-10 cm by a grass cutter.

[0047] (2) Put the cut corn stalks into a cooking pot or an extraction tank, add tap water, the mass is 20 times the mass of the dry corn stalks, the extraction temperature is 98°C, and the holding time is 60 minutes.

[0048] (3) After separating the extracted corn stalks from the hot water, put them into a twin-screw extruder for extruding, and add tap water at the rear of the extruder to wash the stalks. 5 times the dry mass.

[0049] (4) Put the dehydrated corn stalks into a cooking pot or a pre-soaker, add sodium hydroxide, the mass is 5.5% of the absolute dry mass of the crushed corn stalks, and the amount of tap water added is the absolute dry mass of the crushed corn stalks. 10 times the dry mass, the impregnation temperature is 98°C, and the holding time is 40 minutes.

[0050] (5) The pre-impregnated corn stalks w...

Embodiment 3

[0055] (1) Whole corn stalks are used as raw materials, and the corn stalks are first cut into small sections with a size of 3-10 cm by a grass cutter.

[0056] (2) Put the cut corn stalks into a cooking pot or extraction tank, add the hot water extract separated from the previous cycle, and add squeezing and washing water. The number of cycles is 4 times, and the mixing water The quality is 10 times that of the dry corn stalks, the extraction temperature is 98° C., and the holding time is 60 minutes.

[0057] (3) After separating the extracted corn stalks from the hot water, put them into a twin-screw extruder for extruding, and add tap water at the rear of the extruder to wash the stalks. 5 times the dry mass.

[0058] (4) Put the dehydrated corn stalks into a cooking pot or a pre-soaker, add sodium hydroxide, the quality is 6% of the absolute dry mass of the crushed corn stalks, and the added liquid is separated from the previous cycle For the pre-soaking solution, the am...

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Abstract

The invention relates to a chemical mechanical clean pulping process with whole corn stalk as a raw material. Firstly, the cut corn stalk is subjected to pre-extraction in hot water, after solid-liquid separation, the stalk is squeezed, ground and washed, the washed stalk is subjected to three-section high-concentration normal-pressure slurry grinding after being subjected to pre-impregnating treatment, and high-yield and high-strength chemical mechanical pulp is obtained, wherein the corn stalk is cut in a conventional hay cutter; extraction in hot water is chemical-free heating autocatalyticextraction under normal pressure; the extrusion and grinding process is performed in a double-screw extrusion and grinding machine; pre-impregnation is impregnation with sodium hydroxide under normalpressure; three-section high-concentration normal-pressure slurry grinding is performed in a high-concentration normal-pressure disc mill. The process has the benefits that compared with conventionalcorn stalk pulping processes, the process does not require physical separation of stalks and leaves of the corn stalk and is applicable to pulping of the whole corn stalk, part of non-fiber components are separated while fiber components in raw materials are almost completely reserved, a few chemicals are consumed in the pulping process, the obtained pulp is high in yield and good in strength, and high-pressure environment is avoided in the whole process. Produced waste liquids can be directly used as raw materials for other procedures.

Description

technical field [0001] The invention relates to the technical field of chemical mechanical pulping, in particular to a whole stalk chemical mechanical pulping process of corn stalks. Background technique [0002] my country's fiber resources are in short supply, and the import of waste paper is limited. How to use existing resources to alleviate the huge pressure of raw material shortage is imminent. The development of non-wood pulping can effectively solve the current dilemma. However, the annual output of crop stalks in my country is huge, and corn stalks account for more than one-third of the proportion, but most of them are directly burned, causing serious pollution and waste. There have been some studies on the use of corn stover for pulping. [0003] Chinese patent 200310124000.4 discloses a chlorine-free bleaching pulping process of depilled corn stalks as raw materials, which uses the pith-removed and leaf-removed corn stalk husks as raw materials, cooks and bleac...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D21D1/02
CPCD21D1/02
Inventor 江骁雅刘文孟凡锦
Owner CHINA NAT PULP & PAPER RES INST CO LTD
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