Inorganic quick-setting perfusion blasting pore sealing material for mining, and preparation method thereof
A sealing material and inorganic technology, which is applied in the field of mineral inorganic quick-setting perfusion blasting sealing material and its preparation field, can solve the problems of long strength time, large gap between clay materials and low efficiency, and achieves low production cost and high production efficiency. short cycle effect
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preparation example Construction
[0049] In order to further understand the mine inorganic quick-setting perfusion blasting sealing material of the present invention, the present invention also provides a preparation method of the mine inorganic quick-setting perfusion blasting sealing material. The preparation method includes the following steps:
[0050] Step 1, weighing the water reducing agent, sodium sulfate, sodium metaaluminate and gas generating agent and putting them into the first container, mixing and stirring evenly to obtain the composite admixture powder;
[0051] Step 2, weighing the raw materials of sulphoaluminate cement clinker, gypsum, lime and fly ash and putting them into the second container, then adding composite admixture powder, mixing and stirring evenly to obtain the sealing material powder;
[0052] Step 3: Add water to the sealing material powder prepared in step 2, stir and mix evenly to obtain the sealing material.
[0053] The raw materials used in the examples of the present in...
Embodiment 1
[0055] A mine-used inorganic quick-setting perfusion blasting sealing material provided in the embodiment of the present invention has a formula in parts by weight: 35 parts of sulphoaluminate cement clinker, 25 parts of gypsum, 8 parts of lime, powdered coal 30 parts of ash, 2 parts of composite admixture, and 90 parts of water; wherein, the parts by weight of the composite admixture are: 60 parts of water reducer, 20 parts of sodium sulfate, 15 parts of sodium metaaluminate, and 5 parts of gas-generating agent.
[0056] In this embodiment, the preparation method of the mine-used inorganic quick-setting perfusion blasting sealing material is as follows:
[0057] In the first step, add 600g of naphthalene-based water reducer, 200g of sodium sulfate, 150g of sodium metaaluminate, and 50g of aluminum powder paste into the mixer and mix evenly. After passing the test, a composite admixture is obtained;
[0058] In the second step, weigh 3500g of sulphoaluminate cement clinker, 25...
Embodiment 2
[0064] In this embodiment, the amount of water added in the second step of the preparation method is changed to 8000 g, and the other method steps and raw material amounts are the same as those in Example 1, and will not be repeated here.
[0065] The fluidity, initial setting time, 1.5h compressive strength, maximum reaction temperature and vertical expansion rate of the sealing material slurry prepared in this example were tested, and the test standards and methods were the same as those in Example 1.
[0066] The fluidity of the sealing material slurry prepared in the embodiment of the present invention is 260 mm.
[0067] The test block was prepared by grouting pump, the initial setting time was 25min, the compressive strength was 3.95MPa in 1.5h, the highest reaction temperature was 44.6℃, and the vertical expansion rate after hardening was 8.9%.
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