Recombinant adenovirus capable of displaying neutralization antigenic epitope of EV71 virus and CVA16 virus simultaneously
A technology of recombinant adenovirus and CVA16, applied in the field of genetic engineering to achieve the effect of preventing hand, foot and mouth disease
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Embodiment 1
[0025] Example 1: Construction of recombinant adenovirus
[0026] First, the human type 3 adenovirus backbone plasmid pBRAd△E3GFP (constructed by the laboratory according to the conventional genetic engineering technology in this field, the E3 region nt27 ,737–30,900 (SEQ ID NO: 10) was knocked out and replaced with the CMV-EGFP gene (SEQ ID NO: 11)) as a template, and the primer pairs HexU / hr1-sp70R and HexD / hr1-sp70U were used for PCR amplification (General reaction conditions) 1L fragment (nt16,764-21,140) (SEQ ID NO: 12) and 1R fragment (nt 21125-24569) (SEQ ID NO: 13) of pBRAd△E3GFP were obtained. After gel recovery and purification, 1L and 1R 50 ng of each mixture was used as a template, and Hexon upstream and downstream primers were added for PCR amplification of HexU and HexD (conventional reaction conditions) to obtain the hexon fragment R1SP70 in which the SP70 sequence was embedded in the HVR1 region.
[0027] Use the same method to insert the PEP55 antigen epitope...
Embodiment 2
[0034] Example 2: Biological Characteristic Test of Recombinant Adenovirus
[0035] 2.1 Thermal stability test of recombinant adenovirus.
[0036] Place the recombinant adenovirus in a 45°C water bath for 5, 10, 20, and 40 minutes respectively, and then inoculate the recombinant adenovirus with different heat exposure times into 293 cells. After 48 hours of virus infection, take the virus supernatant to test the TCID50 data , comparing the thermal stability curves of recombinant adenovirus with non-recombined type 3 adenovirus as a control. Thermal stability curve see image 3 .
[0037] It was found through experiments that the difference between the recombinant adenovirus and type 3 adenovirus was not significant, indicating that the chimeric neutralizing antigen gene fragments of EV71 virus and CVA16 virus had no effect on the heat stability of the recombinant adenovirus.
[0038] 2.2 ELISA data test of neutralizing epitope of recombinant adenovirus.
[0039] The recomb...
Embodiment 3
[0045] Example 3: Neutralizing antibody test of recombinant adenovirus
[0046] The above-mentioned recombinant adenovirus is purified by ion exchange adsorption.
[0047] The operation steps are as follows: repeatedly freeze-thaw the culture of the recombinant adenovirus three times, put the freeze-thaw product into a centrifuge tube, centrifuge at a high speed of 6000g, and centrifuge at 4°C for 30min. The centrifuged supernatant is concentrated by ultrafiltration, and a 500KD molecular weight cut-off ultrafiltration column (GE) is selected for ultrafiltration concentration of the adenovirus particle suspension. The concentrated recombinant adenovirus was purified with DEAE SepharoseFF (GE Company), the loading buffer was 10mM NaCl+10mM PBS (PH7.4), the elution buffer was 1.2MNaCl+10mM PBS (PH7.8), and the protein was collected The eluents with high concentration were mixed, and the protein concentration of the purified recombinant adenovirus was tested by BCA method, and s...
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