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Preparation method of ferrite/reducing metal composite particles and method for preparing high-temperature stealth coating based on laser 3D printing

A 3D printing and metal composite technology, applied in metal processing equipment, process efficiency improvement, additive manufacturing, etc., can solve problems such as insufficient bonding force, difficult to control microstructure, and inability to guarantee electromagnetic performance, and achieve good fusion and coating. Strong temperature/weather resistance, good combination effect

Active Publication Date: 2022-01-11
HARBIN INST OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] The present invention provides a method for preparing a high-temperature stealth coating based on laser 3D printing technology to solve the problems of insufficient coating / substrate bonding force of the existing high-temperature wave-absorbing coating, difficulty in controlling the microstructure, and unguaranteed electromagnetic properties; the present invention is based on 3D Ferromagnetic / dielectric composite coating obtained by laser-induced in situ thermite reaction by printing technology
[0005] The invention integrates high temperature resistance and electromagnetic absorption performance organically, and prepares the coating in an in-situ autogenous manner, which meets the service requirements of the high temperature stealth coating and simultaneously solves the problem of the film layer / substrate binding force

Method used

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  • Preparation method of ferrite/reducing metal composite particles and method for preparing high-temperature stealth coating based on laser 3D printing
  • Preparation method of ferrite/reducing metal composite particles and method for preparing high-temperature stealth coating based on laser 3D printing
  • Preparation method of ferrite/reducing metal composite particles and method for preparing high-temperature stealth coating based on laser 3D printing

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Embodiment 1

[0035] Embodiment 1: The preparation method of the ferrite / reducing metal composite particles used in this example is prepared by a mixing and granulation process, and the specific preparation method is completed through the following steps:

[0036] Step 1, the particle size diameter is 80nm, spherical Fe 3 o 4 Particles, particle size diameter of 50nm, spherical Al particles and polyvinyl alcohol (PVA) additives according to Fe 3 o 4 The mass ratio to Al is 3.2:1, and the additive dosage is 0.5% of the total mass of the ferrite powder and the reducing metal powder to uniformly mix to obtain a slurry;

[0037] Step 2. The obtained slurry is granulated by centrifugal spray drying and granulation; the spray drying process parameters are as follows: the inlet temperature of the spray drying tower is 220°C, the outlet temperature of the spray drying tower is 100°C, and the spray drying tower is atomized The rotational speed of the disk was 20000r / min. After the granulation is...

Embodiment 2

[0052] Embodiment 2: In this embodiment, the method for preparing a high-temperature stealth coating based on laser 3D printing is carried out according to the following steps:

[0053] The preparation method of the ferrite / reducing metal composite particles used in this example is prepared by a mixing and granulation process, and the specific preparation method is completed through the following steps:

[0054] Step 1, the particle size diameter is 100nm, spherical BaFe 12 o 19 Particles, particle size diameter of 50nm, spherical Al particles and additives (methyl cellulose (CMC)) according to BaFe 12 o 19 The mass ratio of particles to Al particles is 3.2:1, the amount of additives is 1% of the total mass of ferrite powder and reducing metal powder, and the slurry is obtained after uniform mixing;

[0055] Step 2. The obtained slurry is granulated by centrifugal spray drying and granulation; the spray drying process parameters are: the inlet temperature of the spray dryin...

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Abstract

A method for preparing ferrite / reducible metal composite particles and a method for preparing a high-temperature stealth coating based on laser 3D printing belong to the technical field of wave-absorbing coating preparation. The invention aims to solve the problems that existing high-temperature wave-absorbing coatings have insufficient coating / substrate bonding force, difficult control of coating microstructure, and unguaranteed electromagnetic properties. In the present invention, nano-scale ferrite powder and nano-scale reductive metal powder are mixed and granulated to prepare composite particles; in the closed preparation chamber of 3D printing equipment, composite particles are produced on the surface of the substrate by laser-induced in-situ reaction. Obtain high temperature stealth coating. The invention is applied to the high-temperature stealth of components and the prevention and control of electromagnetic pollution.

Description

technical field [0001] The invention belongs to the technical field of preparation of wave-absorbing coatings; in particular, it relates to a preparation method of ferrite / reducing metal composite particles and a method for preparing high-temperature stealth coatings based on laser 3D printing; it can be applied to high-temperature stealth of components and prevention and control of electromagnetic pollution . Background technique [0002] In the field of national defense technology, the demand for radar stealth of high-temperature components such as engines is rapidly increasing; in the field of civilian technology, with the explosive growth of the power level and application scale of radar technology and wireless communication technology, electromagnetic leakage and electromagnetic leakage caused by stray electromagnetic waves The problem of pollution has become increasingly prominent. It is shown that the application of wave-absorbing coatings on components can effective...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B22F1/00B22F9/10B22F3/105B33Y10/00B22F1/052B22F1/065
CPCB22F9/10B22F3/1039B33Y10/00B22F10/00B22F1/052B22F1/065C22C1/058Y02P10/25B22F10/25B33Y80/00B22F2998/10B33Y70/10B22F7/008B22F9/026B33Y40/10B22F9/20B22F2301/35B22F2304/10C22C1/053
Inventor 姜建堂管振杰杨勇甄良邵文柱
Owner HARBIN INST OF TECH
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