49 results about "Thermite" patented technology

The invention relates to the technical field of thermite, in particular to a thermite system of an ultralow condensed phase combustion product and a preparation method of the thermite system. The preparation method of the aluminothermic system comprises the following steps: S1, synthesizing nanoscale BiF3 particles; s2, immersing a mixed oxidizing agent into a copper nitrate solution, dropwise adding ammonia water into a system, reacting for a period of time, standing and aging the reaction system, performing centrifugal separation, washing, and performing vacuum freeze drying to obtain BiF3-coated TACN core-shell structure particles; and S3, adding the acid-activated nano aluminum powder and the BiF3-coated TACN core-shell structure particles into an n-hexane medium, carrying out ultrasonic treatment, and drying to obtain thermite powder. Through the high reaction interface of the nano-scale bismuth-based fluoride and the activation strategy of the high-energy gas production compound on the interface, the output of ultralow condensed phase combustion products and the efficient release of system energy are realized.

The invention provides a preparation method of a thermite, which comprises the following steps: taking CuN (CN) 2 and aluminum powder as raw materials, adding an organic solvent, mixing, and carrying out vacuum drying to obtain the thermite, the mass ratio of the CuN (CN) 2 to the aluminum powder is (1: 1)-(1: 4). According to the method for preparing the thermite through CuN (CN) 2, a new thought for applying other oxides to an energetic material of the thermite is provided, the thermite can provide the heat of 1528.9 J / g and the gas production pressure of 50 KPa, and it is detected that a high-temperature-resistant material aluminum nitride is generated in a product obtained after combustion.

The invention provides a gas phase change rock breaking device and method based on an aluminothermic reaction, and belongs to the technical field of rock blasting. The rock breaking device comprises a graphite excitation pipe, a liquefied air bag and a sealing cover, the excitation pipe is filled with thermite, and thermite reaction can be carried out to release heat; the liquefied air bag is hermetically sleeved outside the excitation tube, is filled with liquid oxygen or liquid nitrogen and is changed into gas under the action of heat released by the excitation tube, and rock mass fracture is realized by volume expansion. By arranging a multi-section excitation pipe serial connection structure, adopting the industrial graphite excitation pipe, designing a liquid oxygen or liquid nitrogen double-medium system and using the polyethylene degradable material bag body, the safety, the economical efficiency and the environmental adaptability of open-air rock mining are remarkably improved.

A layered thermite composite includes alternating layers of metal oxide and reducing metal deposited upon a substrate. A fuzzy interface layer between each metal oxide layer and reducing metal layer includes reducing metal, reducing metal oxide, and metal oxide at least partially intermixed therein. The fuzzy interface layer forms while moving between chambers in a multi-chamber deposition process which minimizes exposure of the reducing metal to oxygen while moving between chambers. The fuzzy interface layer is not expected to grow in thickness after deposition. The combination of the relative thinness of the fuzzy interface layer as well as the presence of reactants as well as reducing metal oxide maintains the sensitivity of the layered thermite structure to mechanical ignition if the structure is used within a primer.

The present invention discloses a method for controlling the yield of vanadium-aluminum alloy, which specifically comprises the following steps: (1) using a copper crucible and a graphite furnace body as a thermite reaction vessel; (2) mixing flaky vanadium pentoxide, aluminum particles and a slag-forming agent uniformly and adding the mixture to the thermite reaction vessel; (3) placing the reaction vessel filled with the mixed raw materials in a cooling pool with circulating water and installing a furnace cover; (4) igniting a magnesium strip to initiate the thermite reaction; (5) removing the furnace cover and the furnace body 5 to 8 minutes after the thermite reaction ends; (6) stopping the cooling water supply when the alloy ingot cools to 950°C and installing a heat-insulating furnace cover on the copper crucible; (7) cooling the alloy ingot naturally for 24 to 48 hours, and finishing the alloy after cooling to obtain a vanadium-aluminum alloy product. The present invention can increase the yield of vanadium-aluminum alloy to more than 86%.

The invention provides a low-oxygen low-nitrogen aluminum-niobium intermediate alloy and a preparation method thereof, and belongs to the technical field of intermediate alloys. The preparation method of the low-oxygen low-nitrogen aluminum-niobium intermediate alloy comprises the following steps that a niobium source, an aluminum source and an oxidizing agent are mixed, then charging is conducted under the argon and vibration conditions, and a mixture is obtained; and the mixture is sequentially subjected to a thermit reaction and cooling under the vibration condition, and the low-oxygen low-nitrogen aluminum-niobium intermediate alloy is obtained. According to the method, charging is carried out under the argon and vibration conditions, air remaining in gaps of mixture particles can be eliminated, introduction of oxygen and nitrogen in the thermit reaction process is reduced, and therefore the oxygen and nitrogen content of the aluminum-niobium intermediate alloy is reduced; and the thermit reaction and cooling are carried out under the vibration condition, so that thick dendritic crystals formed in the alloy solidification process can be crushed, the purpose of grain refinement is achieved, fine grain strengthening is achieved, and the obdurability of the aluminum-niobium intermediate alloy is improved.

The invention provides a method for preparing a high-purity niobium ingot by utilizing multistage refining and the high-purity niobium ingot, and the method comprises the following steps: (1) taking aluminum particles, niobium pentoxide, a heat generating agent and a slag former as raw materials, preparing an aluminum-niobium alloy ingot by adopting an exothermic method outside a furnace, and then carrying out surface treatment and crushing treatment to obtain aluminum-niobium alloy particles; (2) the aluminum-niobium alloy particles are subjected to horizontal electron beam smelting, and a smelted niobium plate is obtained; (3) stacking a plurality of smelting niobium plates, and then sequentially performing vacuum diffusion welding and vacuum arc smelting to obtain a primary niobium ingot; and (4) the primary niobium ingot is placed in a double-gun electron beam smelting furnace to be smelted, and the high-purity niobium ingot is obtained. The stable production of the high-RRR value high-purity niobium is realized by adopting a multi-stage refining process coupling system of an aluminothermy method, horizontal electron beam melting, diffusion welding, electric arc melting and double-gun electron beam melting, and the technical problems of high energy consumption, high cost, low production efficiency and the like in the traditional process are effectively solved.

A method and cascade reactor system for producing elemental rare earth metals and rare earth-aluminum alloys via aluminothermic reduction are disclosed. The method involves combining rare earth oxides or halide salts with aluminum powder, initiating a thermite-type reaction under inert or controlled atmospheric conditions, and recovering the molten metal product. Fluxing agents may be used to enhance slag fluidity and phase separation. The cascade reactor comprises multiple thermite zones with staged ignition, thermal transfer mechanisms, and slag separation interfaces, enabling sequential reduction of mixed feedstocks. The system supports both batch and continuous formats and achieves high recovery yields, reduced aluminum contamination, and compatibility with alloying and post-purification processes. The invention is adaptable to individual rare earth species and mixed oxide concentrates, offering a scalable, energy-efficient, and environmentally favorable route to rare earth metal and alloy production.

Disclosed herein are exothermic reaction mixtures that can be used for copper-based thermite reactions. The disclosed exothermic reaction mixtures can be advantageously formulated with synthetically made copper oxide(s), which can improve consistency and stability of thermite reactions. An example exothermic reaction mixture includes an alloy comprising copper and aluminum and a metal oxide comprising Cu2O and CuO. Also disclosed are methods of preparing the exothermic reaction mixture and methods of welding that include the exothermic reaction mixture.

This invention discloses a fluoride-modified liquid metal thermite and its preparation method, belonging to the field of thermite preparation technology. It utilizes Galinstan eutectic to prepare liquid metal; aluminum powder and liquid metal are synthesized using physical mixing and ultrasonic treatment to obtain liquid metal-modified aluminum; FeCl3·6H2O is added to a perfluorooctanoic acid aqueous solution and stirred, followed by a hydrothermal reaction; the resulting product is washed to obtain Fe(PFO)3; the liquid metal-modified aluminum is mixed with iron perfluorooctanoate and ultrasonically treated to obtain Fe(PFO)3@LM-Al; Fe(PFO)3@LM-Al and iron oxide are added to anhydrous ethanol and ultrasonically stirred to obtain Fe(PFO)3@LM-Al@Fe2O3. This invention, using the above method, raises the high-temperature thermal oxidation reaction temperature of aluminum powder to before the melting point of 660℃, achieving a breakthrough in the thermal mass transfer process of aluminum powder.

The invention discloses an energy-gathered cutting device for directional forcible entry of a collapsed building, and belongs to the technical field of building forcible entry, the energy-gathered cutting device for directional forcible entry of the collapsed building comprises a double-layer shaped charge liner, and the double-layer shaped charge liner is formed by nesting an outer-layer shaped charge liner made of steel and an inner-layer shaped charge liner made of red copper; the outer-layer shaped charge liner is in an inverted frustum shape, and the inner-layer shaped charge liner is in an inverted frustum shape and comprises a high-detonation-velocity charge section, a thermite particle section and a low-detonation-velocity charge section which are sequentially connected in series; the detonating cord is connected with a high-detonation-velocity charge section, a thermite particle section and a low-detonation-velocity charge section in series, the delay detonator is arranged at the front end of the high-detonation-velocity charge section, and an outer-layer steel shaped charge crushes a concrete matrix through high impact toughness of steel to form an initial radial crack; the inner-layer red copper shaped charge liner generates high-speed energy-gathered jet flow by virtue of ductility of copper, the steel bars are efficiently cut off, and the inner-layer red copper shaped charge liner and the steel bars work cooperatively to improve the breaking efficiency and quality.

The present disclosure teaches a system and method for generating power by a thermal power plant. The system and method includes a fuel heating chamber configured to receive a nano-thermite fuel, an induction assembly configured to inductively heat the fuel in the fuel heating chamber, and an electricity generating subsystem configured to convert heat from the heated nano-thermite fuel into electricity.

This invention provides a method for producing a chromium-aluminum-iron alloy, including steps such as raw material mixing. The raw materials used in the mixing process are chromium oxide, aluminum powder, lime, and sodium chlorate. The process employs a two-step smelting method: first, an aluminothermic reduction reaction is used, and second, an electric heating method is employed in a refining furnace. This process homogenizes the molten iron, chromium, and aluminum alloys with different specific gravities, preventing heavier iron and chromium from sinking and lighter aluminum from floating, thus avoiding alloy segregation. The chromium oxide yield produced by this method reaches 93.97%, which is 5-6 percentage points higher than the yield of metallic chromium produced by the conventional aluminothermic method. The metallic aluminum yield reaches 98%-99%, with low aluminum burn-off.

The invention is a multi-layer thermite block, encased in an exterior protective shield with one face exposed. The exposed face is carved out to accommodate a target device such that the block encompasses the target device when placed atop the device. When receiving a data-destruction signal, the block is ignited producing a short-duration blast of heat sufficient to severely damage or destroy all physical data-storing facilities of the target device.

The invention discloses an experimental device for realizing oil and gas well plugging by simulating an underground thermite to melt bismuth alloy, which comprises a pressure container, a combustion system, a data acquisition system, a gas supply system and a power supply system, and is characterized in that the combustion system is arranged in the pressure container and comprises an electric ignition experiment table, an experimental sleeve and an electric ignition wire; the outer surface of the experiment sleeve is coated with bismuth alloy, the experiment sleeve is placed on the electric ignition experiment table, the electric ignition wire extends into the experiment sleeve in the using state, the power supply system is connected with the electric ignition wire, the gas supply system is communicated with the pressure container, and a heating device is arranged in the pressure container. The data acquisition system comprises a high-speed camera and a thermocouple signal collector, and the thermocouple signal collector is connected with the thermocouple through a signal line penetrating through the pressure container. According to the invention, by adding the pressure container, the gas supply system and the heating device, the experiment of melting the bismuth alloy by the thermite in the underground environment is simulated, and data support is provided for oil-gas well plugging.

The invention provides a preparation method of a low-cost CuCr25 contact material, and relates to the technical field of preparation of electrical materials, and the preparation method comprises the following steps: preparing and weighing CuCr25 contact raw materials, mixing the CuCr25 contact raw materials, carrying out compression molding on the CuCr25 contact raw materials, sintering a green body, processing and preparing a CuCr25 contact, and cleaning and inspecting the CuCr25 contact. The water atomized copper powder and the aluminothermy chromium powder are adopted as main raw materials, quantitative recycled powder is innovatively added, the cost of the raw materials is successfully and greatly reduced, the optimized solid-phase sintering process ensures that the material forms a uniform and compact microscopic structure, meanwhile, the production energy consumption of the material is effectively reduced, and the production cost is reduced. The key performance of the prepared CuCr25 contact material completely meets the application standard of low-voltage electrical appliances, the conductivity and strength are perfectly balanced, the product advantages of low cost and high performance are constructed, the green manufacturing concept is reflected through waste recycling, and collaborative improvement of economic benefits and product performance is effectively achieved.

A method and associated system of energy production, the method including providing core-shell thermite particles and combusting the core-shell thermite particles in a dispersed group to produce heat. The combustion of the core-shell thermite particles may proceed according to various core-shell thermite group combustion modes.

A thermite composition for a process of plugging and abandoning a petroleum well comprises a tube-scaling composition and a gas leakage-preventing composition. The tube-scaling composition comprises aluminium and a metal oxide, and the gas leakage-preventing composition comprises a metal or an alloy with a melting point ranging from 100-300° C. The tube-scaling composition is arranged at the bottom, followed by the gas leakage-preventing composition. The thermite composition further comprises a tube-opening composition comprising aluminium and a metal oxide. The process of plugging and abandoning a petroleum well using the thermite composition involves introducing the thermite composition which is arranged in layers in the petroleum well to be plugged and abandoned, and initiating an ignition to trigger a thermite reaction, which melts the metal for tube sealing and prevents gas leakage.

A method and associated system of energy production, the method including providing core-shell thermite particles and combusting the core-shell thermite particles in a dispersed group to produce heat. The combustion of the core-shell thermite particles may proceed according to various core-shell thermite group combustion modes.

A method creates and verifies a thermite-based downhole well barrier in a well. The method includes lowering a heat generating mixture to a desired location in the well; and igniting the heat generating mixture, thereby starting a heat generating process. The method further includes measuring a parameter (P(t)) representative of fluid pressure and / or fluid flow at an upper location of the well as a function of time, at least from time of ignition of the heat generating mixture. The method further includes identifying a first peak area of the measured parameter (P(t)); and determining that the integrity of the well barrier is intact by comparing the first peak area with a first peak area of an expected parameter (E(t)).

This invention relates to the field of metallic materials technology, specifically to a method for producing an aluminum-tungsten-tantalum ternary master alloy. The method involves mixing tantalum pentoxide, aluminum powder, and potassium chlorate, placing the mixture in a molten pool, igniting it with a magnesium strip, and cooling it to obtain an aluminum-tantalum alloy ingot. After removing the surface alumina from the ingot, the ingot is machined into chips in a glove box for later use. Tungsten trioxide, aluminum powder, and the chipped aluminum-tantalum alloy are then mixed and placed in a vacuum aluminothermic furnace. The furnace is closed, a vacuum is created, and a mixture of magnesium and potassium permanganate is sprayed in. The mixture is ignited to initiate a vacuum aluminothermic reaction. After the reaction occurs, the vacuum level in the furnace is increased, and the furnace is cooled. The furnace is then opened, and the slag is removed to obtain the aluminum-tungsten-tantalum alloy ingot. This invention combines metallothermic reduction with vacuum aluminothermic processes to prepare the aluminum-tungsten-tantalum ternary alloy, producing an aluminum-tungsten-tantalum alloy with high homogeneity and low gaseous impurities. This solves the problems of high melting point, high density, and high gaseous impurity content in traditional aluminothermic reaction production methods.

The invention provides a molten alloy packer which comprises a central pipe of a tubular structure. The bismuth-based alloy ring is arranged on the central pipe, and the bismuth-based alloy ring is heated, melted and solidified by adopting a thermite so as to plug formation gaps and annuluses; the prefabricated fastening structure is arranged on the central pipe, and the molten bismuth-based alloy ring is pushed to be directionally solidified after the prefabricated fastening structure is started; wherein the bismuth-based alloy ring is heated and melted through a tripping-in ignition heating tool. After heating, directional solidification packing after bismuth-based alloy melting is achieved, the beneficial effects of being easy to operate, reliable in sealing, good in durability and the like are achieved, the construction efficiency is effectively improved, and finally long-acting packing under various well conditions such as casing damage wells and well cementation is achieved.

Provided is a blast-free alternative tool for breaching operations for the intended purpose of cutting metal, including rebar, steel cables, I-beams, thin walled containers, welding doors, and the like. The apparatus includes a flexible and cuttable tube containing metal oxide / metal (thermite) mixture, capable of being formed around a target material and of NONEL ignition. The apparatus can be used to cut, weld, or ignite target material. Protective caps are included with provisions to insert shock tube or time fuse to transmit ignition to first fire mix. A fire proof or flame retardant flexible outerwrap with adhesive (such as hydrogel) or malleable retention wires covers the cutting ribbon for heat and slag retention. In the preferred embodiment, the apparatus is issued / manufactured in rolls or precut lengths.

The invention relates to the technical field of metal processing, and discloses an efficient and energy-saving aluminum plate production system which comprises a first supporting frame, a hydraulic pump is rotationally connected to the outer surface of the first supporting frame, an aluminum hot melting furnace is rotationally connected to the outer surface of the hydraulic pump, and a smoke exhaust mechanism is clamped to the upper surface of the aluminum hot melting furnace. A waste heat groove is fixedly connected to the outer surface of the smoke exhaust mechanism, a clamping frame is clamped to the outer surface of the waste heat groove, an aluminum plate is clamped into the clamping frame, a filter screen and a filter screen groove are driven to rotate through a rotating shaft, aluminum ash is blocked and received when smoke is sucked, and deposition of a bent pipe of a heat conduction pipe is reduced; the heat conducting plate heats a waste heat tank water source by using flue gas waste heat to preserve heat of the aluminum plate so as to reduce subsequent energy consumption; the rubber round pad filters smoke by means of a water source when the smoke is exhausted and elastically blocks the outlet to prevent the water source from entering the heat conducting plate; and the scraping plate is pulled by the guide rope to scrape aluminum ash in the bent pipe and then is reset by the spring, so that the heat conduction and smoke exhaust efficiency is guaranteed.

The invention relates to the field of alloy materials, and discloses a high-quality aluminum-vanadium-carbon alloy and a preparation method thereof. Ammonium metavanadate, aluminum particles and carbon powder are used as raw materials, V2O5 powder is prepared through oxidizing roasting of the ammonium metavanadate, vanadium elementary substance powder is prepared through thermal reduction of the V2O5 powder, the vanadium elementary substance powder, the aluminum particles and the carbon powder are evenly mixed to obtain Al-V-C alloy powder, the Al-V-C alloy powder is put into a mold to be subjected to cold pressing to obtain an Al-V-C alloy blank, and the high-quality aluminum-vanadium-carbon alloy is obtained through vacuum sintering and suspension smelting. The alloy comprises the following components in percentage by weight: 50-75wt% of vanadium, 0.4-3.5 wt% of carbon and the balance of aluminum: less than or equal to 0.01 wt% of iron, less than or equal to 0.01 wt% of silicon, less than or equal to 0.005 wt% of oxygen and less than or equal to 0.002 wt% Ammonium metavanadate is used as a vanadium source, the cost is low, compared with an aluminum-vanadium-carbon alloy obtained through an aluminothermy method and a smelting method, the adopted method has the characteristics of high purity and high homogenization, segregation is reduced to the maximum extent, aluminum, vanadium and carbon elements are distributed more uniformly, the content of impurity elements such as oxygen and nitrogen is reduced, element burning loss is reduced, and the service life of the aluminum-vanadium-carbon alloy is prolonged. And a new thought is provided for preparation of the domestic high-quality aluminum-vanadium-carbon alloy.

A micro detonator is provided. The micro detonator is made from thermite consisting of layered metal oxide and reducing metal, separated by gradient interface layers. Oxidation of the reducing metal is resisted during and after deposition of the thermite layers until the exothermic reaction is initiated. Layer thickness can thus be reduced without significantly reducing energy density, resulting in rapid, mechanical propagation of the reaction. The micro detonator can be used as a standalone device or within a projectile containing a second charge.

The invention discloses a production method of a vanadium-iron alloy. The production method comprises the following steps: S1, selecting high-impurity vanadium-aluminum alloy crushed aggregates and polishing wastes, vanadium pentoxide, iron oxide powder, aluminum particles, calcium oxide and a heat generating agent; s2, treating the raw materials treated in the step S1; s3, uniformly mixing the crushed vanadium-aluminum alloy, the polishing waste, vanadium pentoxide, iron oxide powder, aluminum particles, calcium oxide and a heat generating agent to form a mixture; s4, a reaction furnace is selected, and a high-alumina refractory material with the particle size of 1-5 mm is laid at the bottom of a reaction furnace body; s5, filling the mixture into a reaction furnace body, compacting, spreading an ignition agent on the material for ignition, and carrying out aluminothermic reaction; s6, discharging after cooling; according to the method, the crushed vanadium-aluminum alloy with high impurity content and the polished waste are converted into the vanadium-iron alloy through an aluminothermic method, and recycling of the waste is achieved.

The application discloses a kind of nanometer thermite film combustion observation system and its application, it is related to combustion observation platform technical field, including high-speed camera, lens, macro-burning rate observation platform and cross-gap propagation observation platform, macro-burning rate observation platform includes slide holder, slide holder is provided with slide slot, cross-gap propagation observation platform includes guide rail base and the fixed angle platform, adjustable angle platform of being set on guide rail base, guide rail base is horizontally arranged, lens is vertically oriented the gap between fixed angle platform and adjustable angle platform, nanometer thermite film slide is carried on fixed angle platform and adjustable angle platform.The application adopts the structure and step of above-mentioned one kind of nanometer thermite film combustion observation system and its application, the combustion event of micron level nanometer thermite film is recorded, realizes the research demand of thin film combustion cross-gap propagation ability under different distances, different included angle.

This invention relates to the field of intermediate alloy preparation technology for aerospace-grade titanium alloys, and discloses a vanadium-aluminum intermediate alloy for aerospace-grade titanium alloys and its preparation method. The alloy preparation uses high-purity aluminum granules, vanadium pentoxide, calcium oxide, cryolite, and aluminum foil as raw materials. First, a primary alloy is prepared using a vacuum aluminothermic method based on an "aluminum foil-encased powder package" material. Then, the primary alloy undergoes finishing treatment to obtain alloy particles. These particles are then subjected to alkaline washing, filtration, and vacuum heat treatment, ultimately yielding an AlV65 alloy with higher purity, better compositional uniformity, and a purer microstructure. This method effectively addresses the challenges of high vapor phase impurity content, significant component segregation, and numerous microscopic inclusions in existing vanadium-aluminum alloys, and is of great significance for building a more resilient aerospace industry chain and promoting high-quality industrial development.

The application provides an aluminum-molybdenum-chromium intermediate alloy and a preparation method thereof, and the preparation method comprises the following steps: (1) fluidizing roasting molybdenum disulfide and chromium sulfide, and obtaining molybdenum trioxide and chromium oxide after cooling; (2) mixing aluminum powder, potassium chlorate and the molybdenum trioxide and the chromium oxide obtained in the step (1), and then performing vacuum aluminothermic reduction smelting, cooling and refining to obtain the aluminum-molybdenum-chromium intermediate alloy. The preparation method provided by the application utilizes the heat released by the fluidizing roasting of the metal sulfide to dry the aluminum powder and the potassium chlorate, so that the drying process is shortened and the continuous production is facilitated; the vacuum aluminothermic method and the electron beam furnace refining method are adopted to improve the uniformity of the intermediate alloy, reduce the impurity content in the intermediate alloy and facilitate the control of the main component and the impurity content in the TC6, TC17 and TC18 and other grades of titanium alloy.