Compound diesel oil pour point depressant and preparation method and application thereof
A diesel pour point depressant and mixed solution technology, which is applied in the petroleum industry, fuel additives, liquid carbon-containing fuels, etc., can solve the problems of poor low-temperature fluidity of diesel oil and unsatisfactory pour point depressing effect, and achieve enhanced pour point depressing effect  , improve pour point depressing effect, simple and easy preparation method
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Embodiment 1
[0026] The measurement method of cold filter point in the present invention is carried out according to "SH / T0248-2006 Determination method of cold filter point of diesel oil and civil heating oil", and the measurement method of condensation point is carried out according to "GB510-83 Determination of freezing point of petroleum products".
[0027] Raw materials used in the following examples:
[0028]
[0029] The preparation method of polybenzyl methacrylate-tetradecyl methacrylate used in this example and other examples is: mix 0.02mol maleic anhydride and 0.02mol myristyl methacrylate, add 25mL solvent toluene, 0.0685 g of initiator benzoyl peroxide was added, and the reaction was carried out at 120° C. for 8 hours to obtain polytetradecyl methacrylate-maleic anhydride. The molecular Mw of the polymer tested by GPC is 54623g / mol, Mn is 21326g / mol, and Mw / Mn is 2.561, and the product benzyl methacrylate-tetradecyl methacrylate is characterized by NMR as figure 1 shown. ...
Embodiment 2
[0036] Composite diesel pour point depressant in the present embodiment, it is made up of following mass percent components:
[0037]
[0038] The preparation method of the above-mentioned composite diesel oil pour point depressant is: mixing and stirring polytetradecyl methacrylate-maleic anhydride, methyl acetate, ethyl acetate, triethylamine and dicyclohexylamine in proportion at a temperature of 25°C Evenly, ultrasonically disperse for 15 minutes to obtain a composite diesel pour point depressant.
[0039] The application of the above-mentioned composite diesel pour point depressant in diesel fuel pour point depressant, the ratio of composite diesel pour point depressant:diesel, calculated by mass ratio, is preferably 1:200, and the composite diesel pour point depressant is added to diesel at a temperature of 40°C After mixing and stirring evenly, ultrasonically disperse for 25 minutes to obtain diesel oil containing the composite diesel pour point depressant.
[0040]...
Embodiment 3
[0042] Composite diesel pour point depressant in the present embodiment, it is made up of following mass percent components:
[0043]
[0044] The preparation method of the above-mentioned composite diesel oil pour point depressant is: mixing and stirring polytetradecyl methacrylate-maleic anhydride, methyl acetate, ethyl acetate, triethylamine and dicyclohexylamine in proportion at a temperature of 25°C Evenly, ultrasonically disperse for 15 minutes to obtain acetate diesel composite diesel pour point depressant.
[0045] The application of the above-mentioned composite diesel pour point depressant in diesel fuel pour point depressant, the ratio of composite diesel pour point depressant:diesel, calculated by mass ratio, is preferably 1:200, and the composite diesel pour point depressant is added to diesel at a temperature of 40°C After mixing and stirring evenly, ultrasonically disperse for 25 minutes to obtain diesel oil containing the composite diesel pour point depressa...
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