A method for improving the electrochemical performance of anion intercalation electrode materials
An electrode material and anion technology, applied in the field of improving the electrochemical performance of anion-embedded electrode materials, can solve the problems of unfavorable battery portability, miniaturization development, reduction of actual loading of active materials, reduction of volumetric energy density, etc., so as to improve cycle stability. performance, improved magnification performance, and the effect of less usage
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Embodiment 1
[0041] Based on the organic positive electrode material with reversible intercalation / extraction of perchlorate anion, the method of the present invention is used to improve its electrochemical performance, and it is necessary to prepare a covalent organic framework compound containing perchlorate anion. The specific process is as follows:
[0042] Preparation of additives:
[0043] Add 42 mg of 1,3,5-triformylphloroglucinol and 118 mg of ethidium bromide into a 15 mL quartz tube, then add 2 mL of a mixed solution of dioxane and mesitylene (volume ratio 1:1), 0.2mL 6.0mol / L acetic acid solution. The quartz tube was cooled with liquid nitrogen, evacuated, and degassed. After repeating three times, the quartz tube was sealed and reacted in an oven at 120° C. for three days. After the reaction was completed, the quartz tube was taken out, cooled to room temperature, and the seal was broken to obtain a deep red precipitate, which was filtered with suction, and the filter cake wa...
Embodiment 2
[0047] When adding a small amount of specific additives, such as 1%, the performance of the battery is also improved. At this time, the battery assembly method is similar to that of Embodiment 1. Such as Figure 5 It is shown that the performance of the battery can also be improved when the proportion of certain kinds of additives is 1.0%. The stable discharge capacity is 94mAh / g at a current density of 100mA / g, and the average discharge voltage and coulombic efficiency are the same as in Example 1. In terms of cycle stability, after 200 cycles, the specific capacity of the battery decays to 60mAh / g.
[0048] In addition, gradually increasing the proportion of specific types of additives, when it reaches 10%, can obtain better effects; and, when the amount of specific types of additives is further increased, the effect remains basically unchanged. Considering that too many additives affect the energy density and cost factors of the battery, a small amount of specific additi...
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