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Water-based sizing agent for all-cotton spinning and preparation method thereof

A cotton textile, water-based technology, applied in the field of cotton textile water-based slurry and its preparation, can solve the problems of general cotton fiber adhesion, easy breakage of molecular chains, poor adhesion effect, etc., and improve antistatic performance. , Improve the sizing rate, the effect of clear opening

Inactive Publication Date: 2019-12-24
桐乡市星邦科技发展股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] The sizing of high-density fabrics in cotton textiles generally uses acrylic acid-based ternary copolymerization slurry, which has a low viscosity and high solid content, but due to the presence of a certain amount on the molecular chain of the copolymer molecule in the slurry The carboxylic acid groups in the slurries are not neutralized, and it is easy to increase the viscosity during the pulping process. In addition, these sizings also have a relatively general adhesion of the copolymer molecules to the cotton fibers, and the molecular chains are easily stretched. broken problem
The publication date is 20171110, and the Chinese patent with the publication number CN107338641A discloses a water-based slurry for textile fabrics. The slurry in this invention has poor adhesion to cotton yarn and is easy to break when stretched

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] The water-based slurry for cotton textiles in this embodiment includes the following components in parts by weight: 35 parts of butyl acrylate, 15 parts of methyl acrylate, 15 parts of methyl methacrylate, 20 parts of acrylonitrile, lauryl acrylate 15 parts of ester, 4 parts of divalent alkaline earth metal compound, 3.5 parts of emulsifier, 4 parts of initiator, 0.4 part of antistatic agent, 1.5 parts of penetrating agent; the dosage ratio of antistatic agent and penetrating agent is 4:15; emulsifier consists of Sodium lauryl sulfate, fatty alcohol polyoxyethylene ether, acryloxypropyl alkylphenol polyether ammonium sulfate compounded according to the ratio of 2:1:1; the initiator is 3% ammonium persulfate aqueous solution .

[0025] The preparation method of the all-cotton textile water-based size in the present embodiment comprises the steps:

[0026] S1: Weigh a specified amount of emulsifier, butyl acrylate, methyl acrylate, methyl methacrylate, and acrylonitrile,...

Embodiment 2

[0033] The all-cotton textile water-based slurry in the present embodiment comprises the following components in parts by weight: 30 parts of butyl acrylate, 10 parts of methyl acrylate, 10 parts of methyl methacrylate, 15 parts of acrylonitrile, lauryl acrylate 10 parts of ester, 3 parts of divalent alkaline earth metal compound, 3 parts of emulsifier, 3 parts of initiator, 0.3 part of antistatic agent, 1.1 part of penetrating agent.

[0034] The preparation method of the all-cotton textile water-based size in the present embodiment comprises the steps:

[0035] S1: Weigh a specified amount of emulsifier, butyl acrylate, methyl acrylate, methyl methacrylate, and acrylonitrile, and add them to the reactor for mixing, raise the temperature to 55°C, stir and emulsify for 30 minutes to obtain a mixed emulsion; then The temperature of the mixed emulsion is raised to 70°C;

[0036] S2: Add the initiator dropwise to the mixed emulsion at a uniform speed, and the dropping time is co...

Embodiment 3

[0042] The water-based slurry for cotton textiles in this embodiment includes the following components in parts by weight: 40 parts of butyl acrylate, 20 parts of methyl acrylate, 20 parts of methyl methacrylate, 25 parts of acrylonitrile, lauryl acrylate 20 parts of ester, 5 parts of divalent alkaline earth metal compound, 4 parts of emulsifier, 5 parts of initiator, 0.5 part of antistatic agent, and 1.9 parts of penetrating agent.

[0043] The preparation method of the all-cotton textile water-based size in the present embodiment comprises the steps:

[0044] S1: Weigh a specified amount of emulsifier, butyl acrylate, methyl acrylate, methyl methacrylate, and acrylonitrile, and add them to the reactor for mixing, raise the temperature to 55°C, stir and emulsify for 30 minutes to obtain a mixed emulsion; then The temperature of the mixed emulsion is raised to 70°C;

[0045] S2: Add the initiator dropwise to the mixed emulsion at a uniform speed, and the dropping time is cont...

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Abstract

The invention relates to a water-based sizing agent for all-cotton spinning and a preparation method thereof. The problems that in the prior art, surface adhesion between water-based sizing agents forall-cotton spinning and cotton fibers is poor, and the tensile property of sizing agents is poor are solved. According to a technical scheme, the water-based sizing agent for all-cotton spinning comprises the following components in parts by weight: 30-40 parts of butyl acrylate, 10-20 parts of methyl acrylate, 10-20 parts of methyl methacrylate, 15-25 parts of acrylonitrile, 10-20 parts of lauryl acrylate, 3-5 parts of a divalent alkaline earth metal compound, 3-4 parts of an emulsifier, 3-5 parts of an initiator, 0.3-0.5 part of an antistatic agent and 1.1-1.9 parts of a penetrant. The acrylonitrile is introduced into a sizing agent monomer, so that the surface adhesive force between the sizing agent and cotton fibers is greatly improved, the sizing rate of the sizing agent is high, andthe antistatic property is good.

Description

technical field [0001] The invention relates to a slurry and a preparation method thereof, in particular to a cotton textile water-based slurry and a preparation method thereof. Background technique [0002] The sizing of high-density fabrics in cotton textiles generally uses acrylic acid-based ternary copolymerization slurry, which has a low viscosity and high solid content, but due to the presence of a certain amount on the molecular chain of the copolymer molecule in the slurry The carboxylic acid groups in the slurries are not neutralized, and it is easy to increase the viscosity during the pulping process. In addition, these sizings also have a relatively general adhesion of the copolymer molecules to the cotton fibers, and the molecular chains are easily stretched. Fracture problem. The publication date is 20171110, and the Chinese patent with the publication number CN107338641A discloses a kind of water-based slurry for textile fabrics. The slurry in this invention h...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08F220/18C08F220/14C08F220/46C08F2/26C08F2/30D06M15/263D06M15/31D06M11/00D06M13/00D06M15/00D06M101/06
CPCC08F2/26C08F2/30C08F220/18D06M11/00D06M13/00D06M15/00D06M15/263D06M15/31D06M2101/06D06M2200/40
Inventor 吴建英吴建伟
Owner 桐乡市星邦科技发展股份有限公司
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