A preparation method of ag-supported quasi-three-dimensional structure embedded flexible electrode material
A flexible electrode and embedded technology, applied in the field of preparation of Ag-supported quasi-three-dimensional embedded flexible electrode materials, can solve problems such as hindering large-scale application, high cost and scarcity, and achieve novel morphology, simple preparation process, The effect of large specific surface area
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0033] (1) Dissolve 1 mmol of silver nitrate in 10 mmol of deionized water, stir magnetically for 30 min at a stirring speed of 700 r / min, and mix well to obtain solution A.
[0034] (2) Dissolve 1 mmol of ammonia water in 20 mmol of deionized water, stir magnetically for 30 min at a stirring speed of 700 r / min, and mix well to prepare solution B.
[0035] (3) Dissolve 0.5 mmol of dodecylamine in 5 mmol of ethanol solution, and after it is completely dissolved, add 0.3 mmol of sodium dodecyl sulfate and 0.2 mmol of polyvinylpyrrolidone to prepare solution C. Mix A and B, slowly pour into solution C, and ultrasonically treat for 30 minutes; let stand to obtain solution D.
[0036] (4) 20mmol of NiCl 2 ·6H 2 O was dissolved in 40 mmol of deionized water, and 1.2 times NiCl was added 2 ·6H 2 The thiourea of 0 molar quantity, magnetic stirring, after mixing uniformly, makes solution E.
[0037] (5) Carbon cloth (1cm×1cm) was used as the working electrode, the Pt electrode w...
Embodiment 2
[0040] (1) Dissolve 1 mmol of silver nitrate in 20 mmol of deionized water, stir magnetically for 60 min at a stirring speed of 800 r / min, and mix well to obtain solution A.
[0041] (2) Dissolve 3 mmol of ammonia water in 20 mmol of deionized water, stir magnetically for 60 min at a stirring speed of 800 r / min, and mix well to prepare solution B.
[0042] (3) Take 1 mmol of dodecylamine and dissolve it in 5 mmol of methanol solution. After it is completely dissolved, add 0.5 mmol of sodium dodecyl sulfate and 0.5 mmol of polyvinylpyrrolidone to prepare solution C. Mix A and B, slowly pour into solution C, and ultrasonically treat for 30 minutes; let stand to obtain solution D.
[0043] (4) 50mmol of NiCl 2 ·6H 2 O was dissolved in 40 mmol of deionized water, and 1.2 times NiCl was added 2 ·6H 2 The thiourea of 0 molar quantity, magnetic stirring, after mixing uniformly, makes solution E.
[0044] (5) Carbon cloth (1cm×1cm) was used as the working electrode, the Pt elec...
Embodiment 3
[0048] (1) Dissolve 1 mmol of silver nitrate in 20 mmol of deionized water, stir magnetically for 30 min at a stirring speed of 800 r / min, and mix well to obtain solution A.
[0049] (2) Dissolve 2 mmol of ammonia water in 20 mmol of deionized water, stir magnetically for 30 min at a stirring speed of 800 r / min, and mix well to prepare solution B.
[0050] (3) Dissolve 0.8 mmol of dodecylamine in 5 mmol of butanol solution, and after it is completely dissolved, add 0.4 mmol of sodium dodecyl sulfate and 0.4 mmol of polyvinylpyrrolidone to prepare solution C. Mix A and B, slowly pour into solution C, and ultrasonically treat for 30 minutes; let stand to obtain solution D.
[0051] (4) 30mmol of NiCl 2 ·6H 2 O was dissolved in 40 mmol of deionized water, and 1.2 times NiCl was added 2 ·6H 2 The thiourea of 0 molar quantity, magnetic stirring, after mixing uniformly, makes solution E.
[0052] (5) Carbon cloth (1cm×1cm) was used as the working electrode, the Pt electrode w...
PUM
Login to View More Abstract
Description
Claims
Application Information
Login to View More