Filtering type electrochemical reactor and method for removing antibiotics from water mass
An electrochemical and filtering technology, applied in chemical instruments and methods, inorganic chemistry, water pollutants, etc., can solve problems such as limiting the application range of electrochemical oxidation, failing to meet practical application requirements, and failing to obtain removal effects. Good use value and application prospect, good strength, good removal effect
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[0035] Example 1
[0036] A filter type electrochemical reactor, such as figure 1 As shown, it includes a pool body 1 and a filter device 2 located in the pool body 1. The filter device 2 includes a cathode 21 at the water inlet end and an anode 24 at the water outlet end. A sealing septum 21 is provided between the cathode 21 and the anode 24, Used to separate the cathode 21 and the anode 24 while also sealing the filter device 2 to avoid water leakage; a sealing septum 21 is provided between the cathode 22 and the cell body 1 to separate the cathode 22 and the cell body 1 At the same time, the filter device 2 is sealed to avoid water leakage.
[0037] In this embodiment, the anode 24 is a carbon nanotube film, and the carbon nanotube film is used as the anode material to be arranged at the water outlet end of the filter device 2, which can not only adsorb more pollutants (such as antibiotics), but also in the electrochemical oxidation reaction process. It can also produce more f...
Example Embodiment
[0043] Example 2
[0044] A method for removing antibiotics in water bodies, using the filtering electrochemical reactor in Example 1 to process antibiotics, including the following steps:
[0045] (1) Mixing sulfamethoxazole wastewater with an initial concentration of 5 mg / L and a pH of 7 with sodium chloride to obtain a mixed solution, wherein the concentration of sodium chloride in the mixed solution is 20 mmol / L.
[0046] (2) Connect the filter type electrochemical reactor to the power supply, set the external DC voltage to 0; according to the feed rate of 1.5 mL / min, continuously feed the mixed solution in step (1) into the filter type electrochemical reactor The electrochemical oxidative degradation is carried out at a temperature of 25°C, and the feeding time is 1h, specifically: the mixed solution in step (1) is continuously fed into the reactor through the water inlet of the filter electrochemical reactor, and passes through At the cathode and anode, adsorption reaction and...
Example Embodiment
[0050] Example 3
[0051] A method for removing antibiotics in water bodies, using the filtering electrochemical reactor in Example 1 to process antibiotics, including the following steps:
[0052] (1) Mix sulfamethoxazole wastewater with an initial concentration of 50 mg / L and a pH of 7 with sodium chloride to obtain a mixed solution, wherein the concentration of sodium chloride in the mixed solution is 20 mmol / L.
[0053] (2) Connect the filter type electrochemical reactor to the power supply, set the external DC voltage to 3V; according to the feed rate of 1.5mL / min, continuously feed the mixed solution in step (1) into the filter type electrochemical reactor The electrochemical oxidative degradation is carried out at a temperature of 25℃, and the feeding time is 1h. Specifically, the mixed solution in step (1) is continuously fed into the reactor through the water inlet of the filter electrochemical reactor, and then passes through the cathode. With the anode, adsorption reactio...
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