Wear-resistant packing and preparation method thereof
A technology of packing and nano-boron fiber, which is applied in the field of wear-resistant packing and its preparation, and sealing materials, which can solve the problems of creep resistance, wear resistance, high temperature resistance, poor acid and alkali resistance and sealing performance, and low equipment dependence , short service life and other problems, to achieve the effects of poor acid and alkali resistance, poor sealing performance, low equipment dependence, and short service life
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Embodiment 1
[0032] A wear-resistant packing prepared from the following raw materials in parts by weight: 10 parts of surface-modified nano-boron fiber / chromium boride composite material, 15 parts of ionic anthracenedione-based fluorine-containing polycondensate, and 25 parts of aminophenyl silicone oil , 30 parts of epichlorohydrin rubber, 1 part of N,N'-m-phenylene bismaleimide, 1 part of compatibilizer PE-g-ST.
[0033] The preparation method of the surface-modified nano-boron fiber / chromium boride composite material comprises the following steps: dispersing 30 g of nano-boron fiber and 30 g of chromium boride in 200 g of N,N-dimethylformamide, and then adding 3 -23.4g of methacryloyloxypropyl tri(methoxyethoxy)silane, stirred and reacted at 60°C for 4 hours, then added trans,trans-1,3-butadiene-1 , 10g of 4-dicarboxylic acid, under nitrogen atmosphere, reflux and stir at 125°C for 15 hours, then centrifuge, wash with ethyl acetate three times, and dry in a vacuum oven at 80°C to const...
Embodiment 2
[0042] A wear-resistant packing prepared from the following raw materials in parts by weight: 11 parts of surface-modified nano-boron fiber / chromium boride composite material, 16 parts of ionic anthracenedione-based fluorine-containing polycondensate, and 26 parts of aminophenyl silicone oil , 32 parts of epichlorohydrin rubber, 2 parts of 2,5-dithio-1,3,4-thiadiazole, 2 parts of compatibilizer PP-g-ST.
[0043] The preparation method of the surface-modified nano-boron fiber / chromium boride composite material comprises the following steps: dispersing 35 g of nano-boron fiber and 30 g of chromium boride in 210 g of N,N-dimethylformamide, and then adding 3 -23.4g of methacryloyloxypropyltri(methoxyethoxy)silane, stirred and reacted at 65°C for 4.5 hours, then added trans,trans-1,3-butadiene-1 , 10g of 4-dicarboxylic acid, under a helium atmosphere, reflux and stir at 127°C for 16 hours, then centrifuge, wash with ethyl acetate for 4 times, and dry in a vacuum oven at 82°C to con...
Embodiment 3
[0052] A wear-resistant packing prepared from the following raw materials in parts by weight: 13 parts of surface-modified nano-boron fiber / chromium boride composite material, 18 parts of ionic anthracenedione-based fluorine-containing polycondensate, and 27 parts of aminophenyl silicone oil , 36 parts of epichlorohydrin rubber, 2 parts of sulfur, 1 part of compatibilizer ABS-g-MAH.
[0053] The preparation method of the surface-modified nano-boron fiber / chromium boride composite material comprises the following steps: dispersing 40 g of nano-boron fiber and 30 g of chromium boride in 230 g of N,N-dimethylformamide, and then adding 3 -23.4g of methacryloyloxypropyl tri(methoxyethoxy)silane, stirred and reacted at 70°C for 5 hours, then added trans,trans-1,3-butadiene-1 , 10g of 4-dicarboxylic acid, under a neon atmosphere, reflux and stir at 130°C for 18 hours, then centrifuge, wash with ethyl acetate 4 times, and dry in a vacuum oven at 86°C to constant weight.
[0054] The ...
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