Method for efficiently preparing large-volume semi-solid thick liquid through compounding process

A semi-solid slurry and composite process technology, applied in the field of metal semi-solid processing, can solve the problems of unsuitable large-volume semi-solid slurry preparation, unstable pulping process, and difficult industrialization promotion, and achieve stable and reliable pulping process. Easy to promote and apply in industrialization, high pulping efficiency

Pending Publication Date: 2020-04-14
UNIV OF SCI & TECH BEIJING
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0006] The purpose of the present invention is to solve the problems of instability, low efficiency, unsuitability for the preparation of large-volume semi-solid slurry and difficulty in industrialization of the existing pulping process, and provides a composite process for efficiently preparing large-volume semi-solid slurry, that is, in During the solidification process of the alloy melt, while directly stirring the alloy melt in the container and indirect treatment of the melt near the crucible wall to cause disturbance, a certain amount of alloy particles is quickly scattered into the interior of the alloy melt; Under the synergistic effect of the stirring device, the melt disturbance device and the melting and heat absorption of alloy particles, the alloy melt cools down rapidly and nucleates a large number of nuclei inside it, and dissociates inside the melt under the convection generated by stirring and disturbance. The synergistic effect makes the internal temperature field and composition field of the alloy uniform, and inhibits the growth of grain dendrites, thereby preparing a large-volume semi-solid slurry with a certain volume fraction of spherical or near-spherical primary solid phases uniformly distributed in the liquid phase matrix

Method used

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  • Method for efficiently preparing large-volume semi-solid thick liquid through compounding process
  • Method for efficiently preparing large-volume semi-solid thick liquid through compounding process
  • Method for efficiently preparing large-volume semi-solid thick liquid through compounding process

Examples

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Effect test

Embodiment 1

[0047] A356 aluminum alloy (liquidus 615 ℃, solidus 555 ℃) semi-solid slurry with a quality of 40 kg prepared by the present invention, the schematic diagram of the composite process for preparing large-volume semi-solid slurry is as follows figure 2 shown.

[0048] The preparation works as follows:

[0049] The container 1 is a crucible, and the A356 aluminum alloy melt 2 (40kg) with a temperature of 660° C. is scooped out with the crucible;

[0050] The melt stirring device adopted is a mechanical stirring device 8, and the melt disturbing device adopted is a three-phase AC induction electromagnetic stirring coil 7. The specific mechanical stirring parameters are a stirring rod with an outer diameter of 80 mm, made of graphite, and a stirring speed of 600 r / min. The electromagnetic disturbance parameters are 380V three-phase alternating current, power 2.2KW, and current 20A; start the mechanical stirring 8 and the three-phase alternating current induction electromagnetic s...

Embodiment 2

[0053] Embodiment 2: Adopt the semi-solid slurry of AlSi8 aluminum alloy (liquidus line 625 ℃, solidus line 563 ℃) that the mass of the present invention is prepared to be 62kg, the schematic diagram of compound process preparation large-volume semi-solid slurry is as follows image 3 shown. Proceed as follows:

[0054] (1-1) The container 1 is a crucible, and 50 kg of AlSi8 aluminum alloy melt 2 at a temperature of 670° C. is scooped out from the crucible and placed inside the melt disturbance device 4 .

[0055] (1-2) The melt stirring device 3 adopted is an ultrasonic stirrer 10, and the number of the ultrasonic stirrer 10 is 3, and the melt disturbing device 4 adopted is an electromagnetic stirrer 9, and the number of the electromagnetic stirrer 9 is 4, specifically The ultrasonic stirring parameters are ultrasonic power 1.5KW, ultrasonic frequency is 20kHz, the specific electromagnetic disturbance parameters are power 12KW, frequency 15Hz; start the ultrasonic stirring a...

Embodiment 3

[0058] Embodiment 3: adopt the present invention to prepare the ZnAl9Cu2 zinc alloy (liquidus line 405 ℃, solidus line 345 ℃) semi-solid slurry that adopts the present invention to prepare quality, the synoptic diagram of composite process preparation large-volume semi-solid slurry is as follows Figure 4 shown. Proceed as follows:

[0059] (1-1) Container 1 is a crucible, and 95 kg of ZnAl9Cu2 zinc alloy melt 2 at a temperature of 480° C. is scooped out from the crucible and placed inside the melt disturbance device 4 .

[0060] (1-2) The melt stirring device 3 used is mechanical stirring, the number of mechanical stirring rods 8 is 3, the melt disturbing device 4 adopted is a vibrator 11, and the specific mechanical stirring parameters are a stirring speed of 1000r / min, specifically The vibration parameter is a vibration frequency of 50 Hz; start the mechanical stirring rod 8 and the vibrator 11 to directly stir the zinc alloy melt 2 in the crucible 1 and indirectly stir th...

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Abstract

The invention relates to a method for efficiently preparing a large-volume semi-solid thick liquid through a compounding process. The method comprises the following steps that a large-volume alloy melt in a container is stirred, meanwhile, in order to enable the alloy melt of the edge part to be sufficiently stirred to avoid adhering materials and quickly cooling the melt, the melt disturbance andthe particles of the same alloy composition are added in the alloy melt on the outer wall of the container, so that the purpose of rapidly and uniformly melting a component field and a temperature field and rapidly cooling is achieved. According to the compounding process, when the melt falls to a preset semi-solid temperature, the treating is stopped, the large-volume semi-solid thick liquid with a solid phase rate of 20%-60% is obtained, and the thick liquid is sent to a forming device for rheoforming. The method solves the problem that when the large-volume semi-solid thick liquid is prepared by a single process, the structure is not uniform, the edge of a crucible is adhered due to insufficiently stirring or disturbing, and the cooling of the melt is slow; and the process is strong incontrollability and good in industrialization prospect, and is particularly suitable for preparing the large-volume semi-solid thick liquid with the weight of more than 10 kg.

Description

technical field [0001] The invention belongs to the technical field of metal semi-solid processing, and in particular relates to a method for efficiently preparing large-volume semi-solid slurry with a mass of more than 10 kg through a composite process. Background technique [0002] In the 1970s, Professor M.C.Flemings of the Massachusetts Institute of Technology and others invented metal semi-solid processing technology. The preparation of semi-solid slurry is the core and key of semi-solid processing technology. There are various methods for preparing metal semi-solid slurry, such as double helix stirring method, bubble stirring method, serpentine sprue method, low superheat casting and weak mechanical stirring method, electromagnetic stirring method, turbulent flow effect method, ultrasonic treatment method, forced convection stirring method, spray deposition method, cooling chute method, rotating enthalpy balance method, etc. However, the above method has the problems ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B22D17/00B22D27/08B22D27/02B22D27/04B22D18/02C22C21/02C22C18/04
CPCB22D17/007B22D18/02B22D27/02B22D27/04B22D27/08C22C18/04C22C21/02
Inventor 祁明凡李静媛乌拉别克·朱玛别克徐玉昭陈雨来康永林
Owner UNIV OF SCI & TECH BEIJING
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